CN211676394U

CN211676394U - Closed organic synthetic extraction all-in-one

Info

Publication number: CN211676394U
Application number: CN201921777205.5U
Authority: CN
Inventors: 陈霞; 吴涛涛; 羊一峰; 陈佳
Original assignee: Taizhou Biomedical Industry Research Institute Co Ltd
Current assignee: Taizhou Biomedical Industry Research Institute Co Ltd
Priority date: 2019-10-22
Filing date: 2019-10-22
Publication date: 2020-10-16
Anticipated expiration: 2029-10-22

Abstract

The utility model discloses a closed organic synthesis extraction all-in-one machine in the technical field of chemical experimental devices, which comprises a case, universal wheels, a front case door, a top case door, a controller, a push rod, an electric lifting column, a device mounting frame and an organic synthesis extraction tank, wherein the top wall of the case is screwed with the universal wheels, the front wall of the case is hinged with the front case door, the top wall of the case is hinged with the top case door, the top wall of the top case door is screwed with the controller, the rear wall of the case is screwed with the push rod, the left side wall and the right side wall of the case are both fixedly provided with the electric lifting column, the inner bottom wall of the case is screwed with the device mounting frame, the device mounting frame is provided with the organic synthesis extraction tank, the device integrates the organic synthesizer device and the extraction device, thereby leading the synthesis and extraction processes to be coherent, the device is suitable for synthesis and extraction equipment with different sizes, is convenient to move and can enhance the stability in the experimental process.

Description

Closed organic synthetic extraction all-in-one

Technical Field

The utility model discloses a closed organic synthesis extraction all-in-one specifically is chemical experiment device technical field.

Background

Organic synthesis refers to a process of chemically preparing simple substances, simple inorganic substances or simple organic substances into more complex organic substances. Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extraction, is a unit operation that utilizes the different solubilities of components in a system in a solvent to separate a mixture, i.e., a method that utilizes the difference in solubility or partition coefficient of a substance in two immiscible (or slightly soluble) solvents to transfer solute substances from one solvent to the other.

Organic synthesis and extraction are two important processes in a chemical experiment, the two processes are in front of each other, but in the current experimental method, after synthesis, synthetic liquid needs to be extracted, and the synthetic liquid needs to be transferred in the middle, so that the loss of the synthetic liquid is inevitably caused, and therefore a machine integrating organic synthesis and extraction functions is needed.

Disclosure of Invention

An object of the utility model is to provide a closed organic synthesis extraction all-in-one to solve the present experimental method who proposes in the above-mentioned background art, need draw out the synthetic fluid after synthesizing and just can extract, the centre needs shift the synthetic fluid, the problem of the loss of difficult the leading to the fact the synthetic fluid.

In order to achieve the above object, the utility model provides a following technical scheme: a closed organic synthesis extraction all-in-one machine which is characterized in that: including quick-witted case, universal wheel, anterior chamber door, top chamber door, controller, push rod, electronic lift post, device mounting bracket and organic synthetic extraction jar, open the lateral wall of quick-witted case has the vent, the roof spiro union of quick-witted case has the universal wheel, the antetheca of quick-witted case articulates there is anterior chamber door, the roof of quick-witted case articulates there is the top chamber door, the roof spiro union of top chamber door has the controller, the back wall spiro union of quick-witted case has the push rod, the equal fixed mounting of lateral wall has electronic lift post about the machine case, the interior diapire spiro union of quick-witted case has the device mounting bracket, install organic synthetic extraction jar on the device mounting bracket.

Preferably, the front wall of the front box door is in threaded connection with a first handle, and the top wall of the top box door is in threaded connection with a second handle.

Preferably, the device mounting bracket includes support body, mounting hole, screw rod, hand wheel, fixed plate and bearing frame, open at the top of support body has the mounting hole, the inner chamber of support body is equipped with the screw hole, and threaded hole is equipped with the screw rod, the hand wheel has been cup jointed to the one end outer wall that the screw rod is located the support body outside, the other end of screw rod runs through the support body and extends into the mounting hole, and its top joint in the bearing frame, the other end of bearing frame is equipped with the fixed plate, the position directly over the screw rod of the roof of support body is from last to having a perfect understanding under to open threaded hole, and threaded hole is.

Preferably, organic synthetic extraction jar is including a jar body, top cap, dropping funnel, motor, stirring rake, ultrasonic transducer, PH sensor, temperature sensor and liquid outlet, the top fixed mounting of the jar body has the top cap, the inner chamber joint of top cap has the dropping funnel, the inner chamber joint of top cap has the motor, the output shaft and the stirring rake fixed connection of motor, the interior diapire fixed mounting of the jar body has ultrasonic transducer, the inside wall fixed mounting of the jar body has the PH sensor, the inside wall fixed mounting of the jar body has temperature sensor, the lateral wall of the jar body is opened there is the liquid outlet.

Compared with the prior art, the beneficial effects of the utility model are that:

1) the device is provided with an organic synthesis extraction tank, which comprises a tank body, a top cover, a dropping funnel, a motor, a stirring paddle and an ultrasonic transducer, experimental liquid is dripped into the tank body through the dripping funnel, the stirring paddle is driven to stir the liquid through the operation of the motor, the liquid is fully synthesized, the ultrasonic transducer is turned on, the rapid mechanical vibration wave is generated by converting the sound energy of the ultrasonic wave into the mechanical energy, and the energy of the ultrasonic wave is utilized, so that the boundary layer of the particles in the liquid becomes thin, the outer surface is peeled off, the particles are cracked, the outer wall of the cell is broken by ultrasonic waves, thereby dissociating the substance in the tissue cell wall into the solution, accelerating the process of dissolving the effective components in the substance into the solvent, reducing the acting force between the target extract and the sample matrix, thereby realizing the extraction and separation of solid and liquid, and achieving the purposes of combining organic synthesis and extraction functions and reducing loss.

2) This device is equipped with quick-witted case, universal wheel, push rod and electronic lift post, and the machine case is except that each device of installation, still plays the guard action to inside organic synthetic extraction jar, promotes the universal wheel through the push rod and can make this device remove, has made things convenient for the transfer of equipment, and the decline of electronic lift post piston rod can prop up quick-witted case, can prevent that it from sliding in the experimentation to strengthen its stability.

3) This device sets up anterior chamber door, top chamber door and device mounting bracket, wherein the device mounting bracket includes the support body, the mounting hole, the screw rod, the hand wheel, fixed plate and fixing bolt, when needs are changed and the maintenance, open anterior chamber door and top chamber door, unscrew fixing bolt, rotate the screw rod through the hand wheel and make it screw out, and drive the fixed plate and remove, make it break away from with the contact of organic synthetic extraction jar, can take out it from anterior chamber door or top chamber door, the convenience that makes equipment change and the flexibility of equipment size are very increased.

Drawings

FIG. 1 is a schematic front view of the closed organic synthesis and extraction integrated machine of the present invention;

FIG. 2 is a schematic axial view of the closed organic synthesis and extraction integrated machine of the present invention;

FIG. 3 is a schematic structural view of the device mounting frame of the present invention;

FIG. 4 is a left side view of the device mounting frame of the present invention;

fig. 5 is a schematic structural view of the organic synthesis extraction tank of the present invention.

In the figure: 100 chassis, 110 ventilation opening, 120 universal wheel, 210 front box door, 211 first handle, 220 fixed part box door, 221 second handle, 300 controller, 400 push rod, 500 electric lifting column, 600 device mounting rack, 610 frame body, 611 mounting hole, 620 screw, 621 hand wheel, 630 bearing seat, 640 fixing plate, 650 fixing bolt, 700 organic synthesis extraction tank, 710 tank body, 720 top cover, 730 dropping funnel, 740 motor, 741 stirring paddle, 750 ultrasonic transducer, 760PH sensor, 770 temperature sensor and 780 liquid outlet.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

The utility model provides a closed organic synthesis extraction all-in-one machine, please refer to fig. 1 and 2, which comprises a case 100, universal wheels 120, a front box door 210, a top box door 220, a controller 300, a push rod 400, an electric lifting column 500, a device mounting rack 600 and an organic synthesis extraction tank 700;

referring to fig. 1 and 2 again, the side wall of the chassis 100 is provided with a vent 110, the vent 110 is used for exhausting harmful gas, the top wall of the chassis 100 is screwed with a universal wheel 120, the universal wheel 120 enables the chassis 100 to move freely, the front wall of the chassis 100 is hinged with a front door 210, the top wall of the chassis 100 is hinged with a top door 220, and the device inside the chassis 100 can be replaced or maintained by opening the front door 210 and the top door 220;

referring to fig. 1 and 2 again, the controller 300 is screwed to the top wall of the top box door 220, a PLC controller is disposed inside the controller 300 and can control the operation of the device, the controller 300 is further provided with a display screen and a button to facilitate data viewing and operation, the push rod 400 is screwed to the rear wall of the case 100, the push rod 400 is used for pushing the case 100 to move through the universal wheel 120, the left and right side walls of the case 100 are fixedly provided with the electric lifting columns 500, and the case 100 can be supported by descending of the piston rods of the electric lifting columns 500, so that the case 100 can be prevented from sliding in the experimental process and the stability of the case can be enhanced;

referring to fig. 1, an apparatus mounting bracket 600 is screwed to an inner bottom wall of a chassis 100, an organic synthesis extraction tank 700 is mounted on the apparatus mounting bracket 600, and the organic synthesis extraction tank 700 is used for integrated operation of organic synthesis and extraction;

referring to fig. 1 and 2, a first handle 211 is screwed on the front wall of the front door 210, a second handle 221 is screwed on the top wall of the top door 220, and the first handle 211 and the second handle 221 are used for opening the front door 210 and the top door 220;

referring to fig. 3 and 4, the device mounting bracket 600 includes a bracket body 610, a mounting hole 611, a screw 620, a hand wheel 621, a fixing plate 640, and a bearing seat 630, wherein the mounting hole 611 is formed at the top of the bracket body 610, a threaded hole is formed in an inner cavity of the bracket body 610, a screw 620 is arranged in the threaded hole, a hand wheel 621 is sleeved on the outer wall of one end of the screw 620, which is positioned outside the frame body 610, the screw 620 can be rotated by holding the hand wheel 621, the other end of the screw 620 penetrates through the frame body 610 and extends into the mounting hole 611, the top end of the bearing block 630 is clamped in the bearing block, the other end of the bearing block 630 is provided with a fixing plate 640, the screw 620 is screwed in and out to drive the fixing plate 640 to move, the fixing plate 640 does not rotate along with the screw 620 when the bearing block 630 rotates the screw 620, so as to avoid the conflict with the frame body 610, the top wall of the frame body 610 is provided with a threaded hole from top to bottom at the position right above the screw 620, a fixing bolt 650 is arranged in the threaded hole, and the fixing bolt 650 is used for fixing the screw 620;

referring to fig. 5, the organic synthesis extraction tank 700 includes a tank 710, a top cover 720, a dropping funnel 730, a motor 740, a stirring paddle 741, an ultrasonic transducer 750, a PH sensor 760, a temperature sensor 770, and a liquid outlet 780, the top cover 720 is fixedly installed on the top of the tank 710, the top cover 720 covers and protects the tank 710, the dropping funnel 730 is fastened to an inner cavity of the top cover 720, the experimental liquid is added into the tank 710 through the dropping funnel 730, the motor 740 is fastened to the inner cavity of the top cover 720, an output shaft of the motor 740 is fixedly connected to the stirring paddle 741, the stirring paddle 741 is driven by the operation of the motor 740 to rotate, thereby stirring the liquid, the ultrasonic transducer 750 is fixedly installed on an inner bottom wall of the tank 710, the ultrasonic transducer 750 generates a fast mechanical vibration wave by converting sound energy of ultrasonic into mechanical energy, solid-liquid extraction separation is achieved by using the energy of the ultrasonic, the, the inside wall fixed mounting of jar body 710 has temperature sensor 770, and on PH sensor 760 and temperature sensor 770 monitored the numerical value in the liquid and transmitted it to the display screen of controller 300, make things convenient for staff's record and monitoring behavior, the lateral wall of jar body 710 is opened has liquid outlet 780, after the extraction is accomplished, can follow liquid outlet 780 and obtain the extract.

When the device is used, a person skilled in the art needs to push the universal wheel 120 to a specific position by the case 100 through the push rod 400, control the electric lifting column 500 to descend and support the case 100 through the controller 300, fix the case 100 on the ground, prevent the case from sliding, open the front case door 210, drop the experimental liquid into the tank 710 through the dropping funnel 730, control the motor 740 to operate through the controller 300, so as to drive the stirring paddle 741 to stir the liquid, so as to fully synthesize the liquid, open the ultrasonic transducer 750, generate a rapid mechanical vibration wave by converting the sound energy of the ultrasonic into mechanical energy, utilize the energy of the ultrasonic to thin the boundary layer of particles in the liquid, peel off the outer surface, break the particles, break the outer wall of the cells by the ultrasonic, so as to make the substances in the tissue cell wall free into the solution, accelerate the process of dissolving the effective components in the substances in the solvent, and reduce the acting force, therefore, solid-liquid extraction separation is realized, the pH sensor 760 and the temperature sensor 770 transmit relevant data in liquid to the display screen of the controller 300, so that a person skilled in the art can clearly see that after extraction is finished, extract liquid can be obtained from the liquid outlet 780, when replacement and maintenance are needed, the front box door 210 and the top box door 220 are opened, the fixing bolt 650 is unscrewed, the screw 620 is rotated through the hand wheel 621 to unscrew the screw, the fixing plate 622 is driven to move, the fixing plate is separated from contact with the organic synthesis extraction tank 700, and the organic synthesis extraction tank can be taken out from the front box door 210 or the top box door 220.

While the invention has been described above with reference to certain embodiments, various modifications may be made and equivalents may be substituted for elements thereof without departing from the scope of the invention. In particular, as long as there is no structural conflict, the various features of the various embodiments disclosed herein can be used in any combination with one another, and the description of such combinations that is not exhaustive in this specification is merely for brevity and resource saving. Therefore, it is intended that the invention not be limited to the particular embodiments disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.

Claims

1. A closed organic synthesis extraction all-in-one machine which is characterized in that: comprises a case (100), universal wheels (120), a front box door (210), a top box door (220), a controller (300), a push rod (400), an electric lifting column (500), a device mounting rack (600) and an organic synthesis extraction tank (700), the side wall of the case (100) is provided with a ventilation opening (110), the top wall of the case is connected with a universal wheel (120) in a threaded manner, the front wall of the case (100) is hinged with a front door (210), the top wall of the case (100) is hinged with a top door (220), the top wall of the top box door (220) is screwed with a controller (300), the rear wall of the case (100) is screwed with a push rod (400), the left side wall and the right side wall of the case (100) are both fixedly provided with electric lifting columns (500), the inner bottom wall of the case (100) is connected with a device mounting rack (600) in a threaded manner, and the device mounting rack (600) is provided with an organic synthesis extraction tank (700).

2. The closed organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: the front wall of the front box door (210) is in threaded connection with a first handle (211), and the top wall of the top box door (220) is in threaded connection with a second handle (221).

3. The closed organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: device mounting bracket (600) is including support body (610), mounting hole (611), screw rod (620), hand wheel (621), fixed plate (640) and bearing frame (630), open at the top of support body (610) has mounting hole (611), the inner chamber of support body (610) is equipped with the screw hole, and threaded hole is equipped with screw rod (620), hand wheel (621) have been cup jointed to the outer one end outer wall that screw rod (620) is located support body (610), the other end of screw rod (620) runs through support body (610) and extends into mounting hole (611), and its top joint in bearing frame (630), the other end of bearing frame (630) is equipped with fixed plate (640), the position that the roof of support body (610) is located directly over screw rod (620) has a perfect understanding the screw hole under from last, and threaded hole is equipped with fixing bolt (650).

4. The closed organic synthesis and extraction all-in-one machine as claimed in claim 1, wherein: the organic synthesis extraction tank (700) comprises a tank body (710), a top cover (720), a dropping funnel (730), a motor (740), a stirring paddle (741), an ultrasonic transducer (750), a PH sensor (760), a temperature sensor (770) and a liquid outlet (780), a top cover (720) is fixedly arranged at the top of the tank body (710), a dropping funnel (730) is clamped in the inner cavity of the top cover (720), the inner cavity of the top cover (720) is clamped with a motor (740), the output shaft of the motor (740) is fixedly connected with a stirring paddle (741), an ultrasonic transducer (750) is fixedly arranged on the inner bottom wall of the tank body (710), a PH sensor (760) is fixedly arranged on the inner side wall of the tank body (710), the inside wall fixed mounting of jar body (710) has temperature sensor (770), the lateral wall of jar body (710) is opened has liquid outlet (780).