CN2113274U - Intort magnetic excitation type fractionating at distiller - Google Patents
Intort magnetic excitation type fractionating at distiller Download PDFInfo
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- CN2113274U CN2113274U CN 91220663 CN91220663U CN2113274U CN 2113274 U CN2113274 U CN 2113274U CN 91220663 CN91220663 CN 91220663 CN 91220663 U CN91220663 U CN 91220663U CN 2113274 U CN2113274 U CN 2113274U
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Abstract
The utility model relates to an intort magnetic excitation type fractionating at distiller for processing the plants aromatic oil, mainly comprising a boiler, a distiller, a condenser, an oil-water separator, an oil barrel and a water tank. The utility model controls to fractionate by the temperature and makes ingredients with different boiling points of the volatile oil carried out by the steam. The utility model makes materials of the distiller impact mutually by adopting a strengthen device (31), a millstones type fluted disc (30), high strength magnet (29) and a spiral plate (10) and causes the external to be scratched badly, the interior cells to be vibrated and blind spots of materials to be reduced. The utility model activates molecules of the aromatic oil through the high strength magnet, increases the activity, increases the rate of accepting more than 20% and is capable of controlling the production quality.
Description
A kind of inward turning excitation type fractionation distiller that relates to is used for the distillation of essential oil volatile oil, belongs to agricultural results product processing units.
The deep processing of development essential oil volatile oil is an importance that promotes spices production and improve the agricultural byproducts economic benefit.Because the boiling temperature scope of essential oil volatile oil is at 190 ℃～230 ℃, boiling range temperature broad.Various perfume oil volatile oil are different molecular structures mixture of ingredients in this oil kind similar compound.Because molecular structure and density difference, the boiling point and the boiling range of each composition are different, even same oil is planted kind and place of production soil property and weather condition difference because of raw material, its boiling point boiling range still has difference, so the crude oil of general perfume oil does not have definite boiling point.
Essential oil volatile oil molecule generally all is stored in root, stem, leaf, flower, fruit, seed, the trunk of plant, the special secretory tissue of bark, and transporting and depot organ in glandular hairs, oil pipe, grease chamber or cell walls, mostly exist with the oil droplet shape.Therefore bring difficulty to processing.Distillation temperature is too low, and then the higher composition of boiling point can't distillate, and influences recovery rate and quality.Distillation temperature is too high, and then low boiling point component is again by pyrolysis, and unwanted material composition also distills, the quality of same influence oil.
In the prior art, the method of extracting perfume oil has large distillation tower and field distiller, all is to continue to use constant temperature level pressure one to heat up in a steamer on earth method, and the shortcoming of this method is the low boiling point component pyrolysis, and high boiling point becomes fractionation not go out, and causes the low and oily bad of recovery rate.The method of another kind of middle-size and small-size factory is to adopt the multilayer string to steam, and indivedual oil are planted and carried out stepwise distillation; The oil kind that also has is pressurization again after the air distillation, and back two kinds of methods are near fractionating technology, but does not enter meticulous fractionating technology field.The typical structure of these methods is shown in Figure 1A and Figure 1B.
Figure 1A is a multilayer string distiller, and multilayer material and clearance space are arranged in the device, is used for medium and small factory and processes plant processing such as Herba Cymbopogonis Citrari, Caulis Miscanthis floriduli, Wrinkled Gianthyssop Herb, Salvia Sclare L. in batches.It from the bottom by the multihole nozzle steam supply.Its advantage is that energy consumption is low, and low boiling point component is distillated, and pressurization back recovery rate improves, but raw material is subjected to the vapour pressure dead angle big, and objectionable constituent are also followed and distillated, the difficult quality guarantee of oil.Third generation field distiller adopts water distillation.Figure 1B is the water distillation structure iron, vapour pipe is become single hole by porous concentrate spray vapour, and raw material can roll in device and collision mutually, and the raw material crust can abrade, and oil yield improves.With the Persea cubeba raw material is example, and recovery rate improves 20～25% than water flowing steaming process, and its shortcoming is that distillation temperature is below 100 ℃, high boiling point becomes to fractionate out few, and the product aldehyde value is on the low side, in the prior art, do not see as yet and excite the perfume oil molecule, improve the technology of water vapor carrying capacity.
In view of above-mentioned, the purpose of this utility model is to provide a kind of temperature control fractionation, utilizes steam (intensifier) vibration, and magnetic force intensifies the inward turning excitation type fractionation distiller of perfume oil molecular activity.
The utility model adopts the oblique rotation of raw material, circulation up and down, solution is subjected to the vapour dead angle, destroy the storage dead angle of perfume oil molecule in raw material with raw material bump fluted disc, dwindle multicomponent boiling point dead angle in the perfume oil with the temperature control fractionation, spray the activity of shake the frequency ripple and the magnetic excitation perfume oil molecule of vapour formation again with intensifier, improve the carrying capacity of water vapor, reduction distillates temperature required, accelerate the speed that distillates, reduce energy consumption.Concrete structure ties up in the cylindrical inner-rotary type distiller that two ends are taper, side in the distiller bottom is provided with steam-supply pipe, and pipe end installing intensifier designs an abrasive disk type fluted disc at the awl end, fluted disc bottom outer rim is equipped with high strong magnet, is used for intensifying raising perfume oil molecular activity.Fluted disc inner edge one side is equipped with the curved shape charging guide plate that is welded into steel plate, and slag-drip opening is installed between steam-supply pipe and the fluted disc.In distiller inner chamber lower inner wall the volution blocking material plate is arranged.One side of cylindrical top of distiller and upper cone junction is provided with charging scffold, and a side of upper cone is provided with charging opening, and the vertex of a cone is provided with filter screen.The upper cone top is connected with steam outlet pipe, in the steam outlet pipe head pipe throttling valve is housed, and steam outlet pipe afterbody and condenser steam inlet pipe link, oil vapour mixed steam enters water-and-oil separator after condensation, by separating, oil flow to respectively in separately the container with water, realizes above-mentioned purpose with this.
Below in conjunction with accompanying drawing and most preferred embodiment in detail, principle of work of the present utility model and constitutional features are described in detail.
Description of drawings
Figure 1A steams the formula distiller for the multilayer string
Figure 1B is a water distillation formula distiller
Fig. 2 is the utility model structural system figure
Fig. 3 is the utility model A-A sectional view
Fig. 4 is the slag-drip opening structure iron
Figure 1A and 1B are representative distiller in the prior art, and Figure 1A steams distiller for the multilayer string, the porous steam supply, and promptly a layered material, a sheaf space exist ventilation property poor, the distillation problem that the dead angle is big, pyrolysis is high, recovery rate is low.Figure 1B is a third generation field water material mixing distiller, single hole steam supply, but undue anti-partially pyrolysis, and the high boiling point volatile oil component is difficult for distillating, and the perfume oil quality is difficult to guarantee.
Fig. 2 is the utility model structural system figure, it overcomes the prior art shortcoming, utilize the temperature control fractionation, steam intensifier and fluted disc make the outside severe scratch of raw material, inner cell is given a shock, and forces the perfume oil molecule to ooze out from the storage dead angle, intensifies the perfume oil molecule with high strong magnet, improve its activity, impel recovery rate to increase.Simultaneously at the top of distiller filter screen is set, prevents that particle from entering condenser tubes, the steam outlet pipe mouth is provided with throttling valve, and control gas mixture flow velocity is regulated the pressure in the retort.
Referring to Fig. 2-Fig. 4, the utility model is made of boiler, distiller, condenser, water-and-oil separator, oil drum, water tank.Boiler (1) is a conventional utility boiler, and its pressure and steam output decide according to the actual conditions of production site.Pressure can change in 0.08～0.25Mpa scope, and steam output determines that by throughput promptly per hundred kg feed material need consume 50～60 kilograms of calculating of steam.Stop valve (2) is housed on boiler (1), gives distiller (3) through vapour pipe (35) steam supply.Distiller (3) mainly is made up of thermometer (4), tensimeter (5), filter screen (6), throttling valve (7), steam outlet pipe (8), charge cavity (9), helical baffle (10), charging scffold (11), charging guide plate (28), high strong magnet (29), abrasive disk type fluted disc (30), steam intensifier (31), steam supply pipe clamp (32), steam-supply pipe (33), distiller support (34), mud hole (36).Distiller (3) is the complex body that cylinder is connected with circular cone, lower cone and right cylinder welding, the upper cone bottom is connected with screw with flange with right cylinder, side in the flange junction is provided with charging scffold (11), the top of platform (11) is fixed in upper cone base flange place, and the bottom of platform (11) is connected with right cylinder.Thermometer (4) is housed on the right cylinder top of distiller (3) and tensimeter (5) is used for measuring the interior temperature and pressure of distiller (3), so that the temperature control fractionation.At cylindrical cavity, around inner chamber, be welded with volution blocking material plate (10), this plate is a long strip shape steel plate, about 10～15 centimetres of its width, raw material splashes and hand of spiral cyclic motion in order to block.One filter screen of top of chamber setting in the upper cone stops material to enter pipeline, and upper cone is equipped with charging opening (9) near a side of charging scffold (11), and its structure is as the hand-hole on the boiler, and inner lid bends arm and screw rod and seals.Upper cone top and steam outlet pipe (8) welding, steam outlet pipe (8) head cavity is equipped with throttling valve (7), and its valve block of throttling valve (7) is a round steel sheet that small gap is arranged, and is screwed on valve shaft, can rotate in 90 ° of scopes around valve shaft.Afterbody at steam outlet pipe (8) is equipped with stopping valve (13), and valve (13) joins with prolong (15), and steam outlet pipe (8) is a tapered tube and oblique to condenser one square neck, in order to the outflow of oily vapour gas mixture.Condenser (12) is by steam outlet pipe (8) and distiller (3) UNICOM.
The lower cone inner chamber of distiller (3) (referring to Fig. 3 A-A sectional view) is provided with steam-supply pipe (33), is fixed on the internal chamber wall of lower cone with pipe clamp (32).Intensifier (31) is a tubular, and vibrating reed is housed in the pipe, and the size and the structure of reed determine that according to throughput intensifier (31) links to each other with gas thread with steam-supply pipe (33).Abrasive disk type fluted disc (30) is installed in the bottom of lower cone, and the tooth bar of fluted disc two is formed squares and arranged, it is 1～1.5 millimeter sawtooth that the degree of depth is arranged on the tooth bar, and the tooth bar spacing is 1.5～2 millimeters.Top, the right angle bisector that goes out vapour medullary ray and fluted disc tooth bar group of intensifier (31) is on same straight line.The tail end of intensifier (31) is 20～30 centimetres apart from the edge of fluted disc (30).(opposite that is intensifier (31) is welded with a charging guide plate (28) to one side of fluted disc (30), and material is flowed by certain orientation, and impels raw material by the turn of spiral plate (10) guiding, therefore is called inner-rotary type.Middle at steam-supply pipe (33) and fluted disc (30), be mud hole (36).The structure of mud hole (36) as shown in Figure 4, it is positioned at lower cone bottom one side, mainly by pin (36A), tighten up bow arm (36B), handwheel screw (36C), cover plate (36D), return spring (36E), hook arm (36F), arm pin (36G) and form.During deslagging, only need the hook arm up one is struck to make and tightens up bow arm (36B) and cover plate (36D) is thrown off deslagging.Lower cone bottom outer rim is equipped with high strong magnet (29), by the effect in magnetic field, make perfume oil molecule and water molecules magnetic to, magnetic moment changes, and improves its activity, thereby recovery rate is improved, and distillates temperature required reduction, speeds up, energy consumption reduces.
The oily vapour gas mixture that comes out from steam outlet pipe (8), enter condenser (12), condenser is made up of posticum (14), spiral coil cooling tube (15), water injection pipe (16), water pipe folder (17), A-frame (18), tubing (19), wash water valve (20), foot rest (21).It is a cylindrical container, and the bottom is slightly tapered, and wash water valve (20) is equipped with at the awl end, and the silt particle in the water coolant from then on valve is discharged.The inner chamber installing spiral coil cooling tube (15) of condenser (12), coil pipe is wrapped on the tripod (18), a termination stopping valve (13) of coil pipe, another termination mixed solution tubing (19) is equipped with a stopping valve equally on the pipe.One side of condenser (12) is equipped with a water coolant water injection pipe (16), and the upper end is a funnel, and is fixed on the condenser wall by water pipe folder (17).Posticum (14) is left on the top of condenser (12), and water coolant flows out thus.Condenser (12) is supported by foot rest (21).
Deliver to columnar water-and-oil separator (16) by the mixed solution that tubing (19) comes out by bend pipe (27), utilize the difference of oil, water-mass density, above perfume oil floats over, flow to oil drum (24) through transition pipeline (22), oily(waste)water then flow to water tank (25) by water pipe (23).Water tank can adopt different materials to make according to local condition, as long as its capacity can satisfy (23) two hours flows of water pipe.
The utility model can be used for the production of large, medium and small type factory essential oil, according to the throughput needs, selects boiler and distiller capacity, especially is fit to middle-size and small-size station-service.With 0.6m
3Distiller is an example: about 1 ton of day processing raw material ability, annual 40 days production times in season meter, only need 6000～7000 yuan of investments, then except that recouping capital outlay, still there are thousands of first profits to get, and the quality of product and recovery rate are higher than existing all distillers, are processing unitss of aromatic oil plant producing region township and village enterprises and farmer richness.
Claims (6)
1, a kind of inward turning excitation type fractionation distiller that relates to, be used for the processing of essential oil, rotation and high strong magnet by material in the device intensify the perfume oil molecule, improve the recovery rate of oil, it is characterized in that, it is by boiler, distiller, condenser, water-and-oil separator, oil drum, water tank constitutes, boiler [1] is a conventional utility boiler, stop valve [2] is housed on it, supply with distiller steam, the pressure of boiler [1] is in 0.08～0.25Mpa scope, steam output is by 50～60 kilograms of selections of per hundred kg feed material consumption steam, distiller [3] is mainly by thermometer [4], tensimeter [5], filter screen [6], throttling valve [7], steam outlet pipe [8], charge cavity [9], helical baffle [10], charging scffold [11], charging guide plate [28], high strong magnet [29], abrasive disk type fluted disc [30], steam intensifier [31], steam supply pipe clamp [32], steam-supply pipe [33], distiller support [36] is formed, distiller [3] is the complex body that cylinder is connected with circular cone, lower cone and right cylinder welding, the upper cone bottom is connected with screw with flange with right cylinder, side in the flange junction is provided with charging scffold [11], the top of platform [11] is fixed in the flange place of upper cone bottom, the bottom of platform [11] is connected with right cylinder, distiller [3] is by steam outlet pipe [8] and condenser [12] UNICOM, condenser [12] is a cylindrical container, the bottom is slightly tapered, it is by posticum [14], spiral coil cooling tube [15], water injection pipe [16], water pipe folder [17], A-frame [18], tubing [19], wash water valve [20], foot rest [21] is formed, the oil-water mixture of condensation in spiral coil cooling tube [15], by tubing [19] and water-and-oil separator [26] UNICOM, water-and-oil separator [26] utilizes oil, the difference of water-mass density, after carrying out oily water separation, through oil pipe [22], water pipe [23] flow in oil drum [24] and the water tank [25].
2, inward turning excitation type fractionation distiller according to claim 1 is characterized in that the side that top of chamber in the upper cone of distiller (3) is provided with filter screen (7), upper cone is provided with charging opening (9).
3, inward turning excitation type fractionation distiller according to claim 1, it is characterized in that a throttling valve (7) being housed at steam outlet pipe (8) head cavity, its valve block is a round steel sheet that small gap is arranged, and is fixed on the valve shaft with screw, can rotate in 90 ° of scopes around valve shaft.
4, inward turning excitation type fractionation distiller according to claim 1 is characterized in that the distiller cylindrical cavity is welded with a volution blocking material plate (10), is equipped with thermometer (4) and tensimeter (5) in right cylinder top outer rim.
5, inward turning excitation type fractionation distiller according to claim 1 is characterized in that, the lower cone inner chamber is equipped with steam-supply pipe (33), abrasive disk type fluted disc (30), charging guide plate (28), lower cone bottom outer rim is equipped with high strong magnet (29).
6, inward turning excitation type fractionation distiller according to claim 1, the afterbody that it is characterized in that steam-supply pipe (33) is equipped with intensifier (31), intensifier (31) is a tubular, vibrating reed is housed in the pipe, intensifier (31) is connected with gas thread with steam-supply pipe (33), the bisector on the top, right angle of the steam outlet medullary ray of intensifier (31) and fluted disc tooth bar group is on same straight line, and intensifier (31) tail end is 20～30 centimetres apart from the distance at fluted disc (30) edge.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 91220663 CN2113274U (en) | 1991-08-10 | 1991-08-10 | Intort magnetic excitation type fractionating at distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 91220663 CN2113274U (en) | 1991-08-10 | 1991-08-10 | Intort magnetic excitation type fractionating at distiller |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2113274U true CN2113274U (en) | 1992-08-19 |
Family
ID=4927725
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 91220663 Granted CN2113274U (en) | 1991-08-10 | 1991-08-10 | Intort magnetic excitation type fractionating at distiller |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2113274U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106350227A (en) * | 2016-09-14 | 2017-01-25 | 梧州市西江林产化工技术设备研究所 | Energy-saving high-efficiency adjustable temperature plant essential oil distillation kettle and distillation process thereof |
| CN107794121A (en) * | 2017-10-05 | 2018-03-13 | 曹建华 | Process equipment for cosmetics |
| CN108926020A (en) * | 2018-06-12 | 2018-12-04 | 贾文玉 | A kind of animal husbandry feed processing and storing unit |
-
1991
- 1991-08-10 CN CN 91220663 patent/CN2113274U/en active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106350227A (en) * | 2016-09-14 | 2017-01-25 | 梧州市西江林产化工技术设备研究所 | Energy-saving high-efficiency adjustable temperature plant essential oil distillation kettle and distillation process thereof |
| CN107794121A (en) * | 2017-10-05 | 2018-03-13 | 曹建华 | Process equipment for cosmetics |
| CN107794121B (en) * | 2017-10-05 | 2023-10-10 | 曹建华 | Processing equipment for cosmetics |
| CN108926020A (en) * | 2018-06-12 | 2018-12-04 | 贾文玉 | A kind of animal husbandry feed processing and storing unit |
| CN108926020B (en) * | 2018-06-12 | 2021-10-19 | 贾文玉 | Feed treatment and storage device for animal husbandry |
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| CX01 | Expiry of patent term |