CN210964033U - Fullerene separation and purification device - Google Patents
Fullerene separation and purification device Download PDFInfo
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- CN210964033U CN210964033U CN201921367261.1U CN201921367261U CN210964033U CN 210964033 U CN210964033 U CN 210964033U CN 201921367261 U CN201921367261 U CN 201921367261U CN 210964033 U CN210964033 U CN 210964033U
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Abstract
The utility model discloses a separation and purification device of fullerene relates to separation and purification technical field, this separation and purification device of fullerene, including the base, upper surface one side fixed mounting of base has the collector, and the both sides of collector all are provided with the support frame, the one end of the top fixed connection bracing piece of support frame, one side of the other end fixed connection support hand of bracing piece, the lower surface of isolation bucket is connected in the opposite side laminating of support hand, and the upper surface middle part fixed mounting who keeps apart the bucket has the motor, and the inside of keeping apart the bucket is provided with the rotary drum. This separation and purification device of fullerene sets up the backing plate through the inside at the collector, has reached the effect of drainage, makes things convenient for the mixed liquid of fullerene to flow in the silicone tube, through mutually supporting of support frame and bracing piece and support hand, plays the effect of support to keeping apart the bucket, has been convenient for keep apart the dismantlement of bucket and has laid, sets up a plurality of filtration pores through the surface at the rotary drum, can effectively separate the impurity in the mixed liquid of fullerene.
Description
Technical Field
The utility model relates to a separation and purification technical field specifically is a separation and purification device of fullerene.
Background
Fullerene, which is a third allotrope found in elemental carbon, is a substance consisting of carbon, and existing in a spherical, ellipsoidal, or tubular structure, and can be called fullerene, and refers to a class of substances, and is similar to graphite in structure, but has only six-membered rings, and there may be five-membered rings in fullerene, and the fullerene structure is similar to that of Fuller, and is called fullerene.
At present, the existing device for separating and purifying fullerene can not make fullerene and extraction solvent fully contact in the processing process, thereby reducing the efficiency of fullerene purification.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model provides a not enough to prior art, the utility model provides a separation and purification device of fullerene has solved the current device that is used for fullerene separation and purification can't make the fullerene and draw the solvent fully to contact in the course of working to reduce the efficiency of fullerene purification, be unfavorable for the problem of using widely.
(II) technical scheme
In order to achieve the above purpose, the utility model discloses a following technical scheme realizes:
a separation and purification device for fullerene comprises a base, wherein a collector is fixedly arranged on one side of the upper surface of the base, support frames are arranged on two sides of the collector, the top of each support frame is fixedly connected with one end of a support rod, the other end of each support rod is fixedly connected with one side of a support handle, the other side of the support handle is attached to and connected with the lower surface of an isolation barrel, a motor is fixedly arranged in the middle of the upper surface of the isolation barrel, a rotary drum is arranged inside the isolation barrel, filter holes are formed in the surface of the rotary drum, a filter plate is arranged below the rotary drum, and a discharge hole is formed in the middle of the lower surface of;
the lower end of one side of the collector is provided with an interface, one end of the interface is fixedly connected with one end of a silicone tube, the other end of the silicone tube is fixedly connected with one side of the upper surface of a stirring barrel, the other side of the upper surface of the stirring barrel is fixedly connected with a mixed liquid feeding hopper, the middle part of the upper surface of the stirring barrel is fixedly provided with a driving motor, a stirring paddle is arranged in the stirring barrel, and one end of the stirring paddle is fixedly connected with a stirring blade;
the lower surface middle part fixed connection conveying pipeline's of agitator one end, the other end fixed connection of conveying pipeline draws upper surface one side of case, draw inside one side upper end fixedly connected with slide of case, the inside of slide is provided with the heating plate, the lower surface middle part fixed mounting of slide has the condenser.
Optionally, feed hoppers are fixedly mounted on two sides of the upper surface of the isolation barrel;
the motor is fixedly connected with the middle part of the upper surface of the isolation barrel through a fixed seat.
Optionally, a backing plate is arranged at the bottom of the inner cavity of the collector;
and the middle part of the silicone tube is fixedly provided with a material suction pump.
Optionally, a valve is fixedly arranged in the middle of the feed delivery pipe;
a first drainage plate is fixedly arranged in the middle of the other side in the extraction box;
the bottom of the inner cavity of the extraction box is fixedly provided with a second drainage plate.
Optionally, the middle part of the rotary drum is movably connected with the motor through a rotary shaft;
the filter holes are arranged in a plurality and distributed in a rectangular array;
the inside one side of keeping apart the bucket is seted up flutedly, the one end of filter inserts the recess and with recess looks adaptation, the filter other end runs through one side of keeping apart the bucket and is located the surface of keeping apart the bucket.
Optionally, the bottom of the support frame is fixedly connected with the upper surface of the base;
the other end of the stirring paddle penetrates through the upper surface of the stirring barrel and is fixedly connected with the driving motor.
Optionally, a material taking port is fixedly installed at the lower end of one side of the extraction box;
the equal fixed mounting in lower surface both sides of drawing the case has the pillar, the bottom of pillar and the upper surface fixed connection of base.
(III) advantageous effects
The utility model provides a separation and purification device of fullerene possesses following beneficial effect:
(1) this fullerene's separation and purification device, through the inside at the collector setting up the backing plate, the effect of drainage has been reached, make things convenient for fullerene to mix liquid and flow into the silicone tube, through mutually supporting of support frame and bracing piece and support hand, play the effect of support to keeping apart the bucket, the laying of keeping apart the bucket of having convenient for, set up a plurality of filtration pores through the surface at the rotary drum, can effectively separate the impurity in the fullerene mixes liquid, can effectively keep apart the impurity that the rotary drum got rid of through the filter, the purity of fullerene has been improved.
(2) This fullerene's separation and purification device through setting up the silicone tube, has been convenient for install and dismantle to improved the life of device, can effectively mix liquid and extract full contact with fullerene through mutually supporting of stirring rake and stirring leaf, can effectively improve the efficiency and the quality of purification through the heating plate, can guarantee to draw the incasement through the condenser to be the constant temperature state.
Drawings
FIG. 1 is a schematic view of the structure of the present invention;
FIG. 2 is a schematic sectional view of the structure of the present invention;
FIG. 3 is a schematic top view of the isolation tub structure of the present invention;
fig. 4 is a schematic top view of the stirring blade structure of the present invention.
In the figure: 1-base, 2-collector, 3-support frame, 4-support rod, 5-support arm, 6-isolation barrel, 7-motor, 8-rotary drum, 9-filter hole, 10-filter plate, 11-discharge hole, 12-interface, 13-silicone tube, 14-stirring barrel, 15-mixed liquid feed hopper, 16-driving motor, 17-stirring paddle, 18-stirring blade, 19-feed delivery pipe, 20-extraction box, 21-slide plate, 22-heating plate, 23-condenser, 24-backing plate, 25-suction pump, 26-valve, 27-first drainage plate and 28-second drainage plate.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-4, the present invention provides a technical solution:
a device for separating and purifying fullerene comprises a base 1, a collector 2 is fixedly arranged on one side of the upper surface of the base 1, support frames 3 are arranged on two sides of the collector 2, one end of a support rod 4 is fixedly connected to the top of the support frame 3, the other end of the support rod 4 is fixedly connected to one side of a support handle 5, the other side of the support handle 5 is attached to the lower surface of an isolation barrel 6, the isolation barrel 6 is supported by the support frame 3, the isolation barrel 6 is convenient to place, a motor 7 is fixedly arranged in the middle of the upper surface of the isolation barrel 6, a rotary barrel 8 is arranged in the isolation barrel 6, filter holes 9 are formed in the surface of the rotary barrel 8, a plurality of filter holes 9 are formed in the surface of the rotary barrel 8, impurities in a fullerene mixed liquid can be effectively separated, a filter plate 10 is arranged below the rotary barrel 8, and the impurities removed by the rotary barrel 8 can be effectively isolated by the filter plate 10, the purity of the fullerene is improved, and a discharge hole 11 is formed in the middle of the lower surface of the isolation barrel 6;
the lower end of one side of the collector 2 is provided with a connector 12, one end of the connector 12 is fixedly connected with one end of a silicone tube 13, the installation and the disassembly are convenient and the service life of the device is prolonged by arranging the silicone tube 13, the other end of the silicone tube 13 is fixedly connected with one side of the upper surface of a stirring barrel 14, the other side of the upper surface of the stirring barrel 14 is fixedly connected with a mixed liquid feed hopper 15, the middle part of the upper surface of the stirring barrel 14 is fixedly provided with a driving motor 16, a stirring paddle 17 is arranged inside the stirring barrel 14, one end of the stirring paddle 17 is fixedly connected with a stirring blade 18, and the fullerene mixed liquid can be effectively and fully contacted with the extracting solution by the mutual matching of the stirring;
one end of conveying pipeline 19 is fixedly connected to the lower surface middle part of agitator 14, and the other end fixed connection of conveying pipeline 19 draws upper surface one side of case 20, draws inside one side upper end fixedly connected with slide 21 of case 20, and the inside of slide 21 is provided with heating plate 22, through heating plate 22, can effectively improve the efficiency and the quality of purification, and slide 21's lower surface middle part fixed mounting has condenser 23, can guarantee through condenser 23 that it is the constant temperature state to draw inside of case 20.
As an optional technical solution of the utility model: feed hoppers are fixedly arranged on both sides of the upper surface of the isolation barrel 6;
As an optional technical solution of the utility model: a backing plate 24 is arranged at the bottom of the inner cavity of the collector 2, and the backing plate 24 is arranged in the collector, so that the drainage effect is achieved, and the fullerene mixed liquid can conveniently flow into the silicone tube 13;
the middle part of the silicone tube 13 is fixedly provided with a material suction pump 25, and the fullerene solution is conveniently conveyed through the material suction pump 25.
As an optional technical solution of the utility model: a valve 26 is fixedly arranged in the middle of the feed delivery pipe 19;
a first drainage plate 27 is fixedly arranged in the middle of the other side in the extraction box 20;
draw inner chamber bottom fixed mounting of case 20 has second drainage plate 28, through first drainage plate 27 and second drainage plate 28, makes the fullerene after the heating have sufficient time and is cooled down by condenser 23 to the messenger draws the inside homothermal effect that reaches of case 20.
As an optional technical solution of the utility model: the middle part of the rotary drum 8 is movably connected with the motor 7 through a rotating shaft;
a plurality of filtering holes 9 are arranged, and the plurality of filtering holes 9 are distributed in a rectangular array;
keep apart the inside one side of bucket 6 and seted up the recess, the one end of filter 10 insert the recess and with recess looks adaptation, the filter 10 other end runs through one side of keeping apart bucket 6 and is located the surface of keeping apart bucket 6, through the recess, makes filter 10 have good stability.
As an optional technical solution of the utility model: the bottom of the support frame 3 is fixedly connected with the upper surface of the base 1;
the other end of the stirring paddle 17 penetrates through the upper surface of the stirring barrel 14 and is fixedly connected with the driving motor 16, and the stirring blade 18 can be driven to rotate along with the stirring paddle 17 through the driving motor 16.
As an optional technical solution of the utility model: a material taking port is fixedly arranged at the lower end of one side of the extraction box 20;
the lower surface both sides of drawing case 20 all fixed mounting have the pillar, and the bottom of pillar and the upper surface fixed connection of base 1 make through the pillar and draw case 20 to have good stability.
The electrical components presented in the document are all electrically connected with an external master controller and 220V mains, and the master controller can be a conventional known device controlled by a computer or the like.
In summary, when the device for separating and purifying fullerene is used, firstly, the motor 7 is started, the motor 7 drives the rotary drum 8 to rotate through the rotary shaft, a user pours the fullerene mixed liquid into the isolation barrel 6 through the feed hopper, the fullerene mixed liquid flows into the interior of the collector 2 through the rotary drum 8 and the filter plate 10 after being processed by the rotary drum 8 and the filter plate 10, and then the fullerene mixed liquid is guided into the interior of the silicone tube 13 through the backing plate 24, at this time, the material suction pump 25 is started to make the mixed liquid flow into the stirring barrel 14, meanwhile, the extraction solvent is poured into the stirring barrel 14 through the mixed liquid feed hopper 15 and the driving motor 16 is started, the driving motor 16 drives the stirring paddle 17 to rotate, the stirring paddle 17 drives the stirring blade 18 to rotate, after the fullerene mixed liquid is fully contacted with the extraction solvent, the fullerene enters the extraction box 20 by opening the valve 26, and is, then, a buffering process is manufactured through the first flow guiding plate 27 and the second flow guiding plate 28, so that the condenser 23 has sufficient time for temperature control, the purification efficiency and quality of fullerene are improved conveniently, and finally, the fullerene is extracted from a material taking opening, and the production can be completed.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (7)
1. The utility model provides a separation and purification device of fullerene, includes base (1), its characterized in that: a collector (2) is fixedly mounted on one side of the upper surface of the base (1), support frames (3) are arranged on two sides of the collector (2), the top of each support frame (3) is fixedly connected with one end of a support rod (4), the other end of each support rod (4) is fixedly connected with one side of a support handle (5), the other side of each support handle (5) is attached to the lower surface of an isolation barrel (6), a motor (7) is fixedly mounted in the middle of the upper surface of the isolation barrel (6), a rotary barrel (8) is arranged in the isolation barrel (6), filter holes (9) are formed in the surface of the rotary barrel (8), a filter plate (10) is arranged below the rotary barrel (8), and a discharge hole (11) is formed in the middle of the lower surface of the isolation barrel (6);
the lower end of one side of the collector (2) is provided with an interface (12), one end of the interface (12) is fixedly connected with one end of a silicone tube (13), the other end of the silicone tube (13) is fixedly connected with one side of the upper surface of a stirring barrel (14), the other side of the upper surface of the stirring barrel (14) is fixedly connected with a mixed liquid feeding hopper (15), the middle part of the upper surface of the stirring barrel (14) is fixedly provided with a driving motor (16), a stirring paddle (17) is arranged in the stirring barrel (14), and one end of the stirring paddle (17) is fixedly connected with a stirring blade (18);
the one end of lower surface middle part fixed connection conveying pipeline (19) of agitator (14), the other end fixed connection of conveying pipeline (19) draws upper surface one side of case (20), draw inside one side upper end fixedly connected with slide (21) of case (20), the inside of slide (21) is provided with heating plate (22), the lower surface middle part fixed mounting of slide (21) has condenser (23).
2. The apparatus of claim 1, wherein:
feed hoppers are fixedly arranged on two sides of the upper surface of the isolation barrel (6);
the motor (7) is fixedly connected with the middle part of the upper surface of the isolation barrel (6) through a fixed seat.
3. The apparatus of claim 1, wherein:
a backing plate (24) is arranged at the bottom of the inner cavity of the collector (2);
and the middle part of the silicone tube (13) is fixedly provided with a material suction pump (25).
4. The apparatus of claim 1, wherein:
a valve (26) is fixedly arranged in the middle of the feed delivery pipe (19);
a first drainage plate (27) is fixedly arranged in the middle of the other side in the extraction box (20);
and a second drainage plate (28) is fixedly arranged at the bottom of the inner cavity of the extraction box (20).
5. The apparatus of claim 1, wherein:
the middle part of the rotary drum (8) is movably connected with the motor (7) through a rotary shaft;
a plurality of filtering holes (9) are arranged, and the filtering holes (9) are distributed in a rectangular array;
the inside one side of keeping apart bucket (6) is seted up flutedly, the one end of filter (10) is inserted the recess and with recess looks adaptation, the filter (10) other end runs through the one side of keeping apart bucket (6) and is located the surface of keeping apart bucket (6).
6. The apparatus of claim 1, wherein:
the bottom of the support frame (3) is fixedly connected with the upper surface of the base (1);
the other end of the stirring paddle (17) penetrates through the upper surface of the stirring barrel (14) and is fixedly connected with the driving motor (16).
7. The apparatus of claim 1, wherein:
a material taking port is fixedly arranged at the lower end of one side of the extraction box (20);
the equal fixed mounting in lower surface both sides of drawing case (20) has the pillar, the bottom of pillar and the upper surface fixed connection of base (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921367261.1U CN210964033U (en) | 2019-08-22 | 2019-08-22 | Fullerene separation and purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921367261.1U CN210964033U (en) | 2019-08-22 | 2019-08-22 | Fullerene separation and purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210964033U true CN210964033U (en) | 2020-07-10 |
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ID=71460626
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201921367261.1U Active CN210964033U (en) | 2019-08-22 | 2019-08-22 | Fullerene separation and purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210964033U (en) |
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2019
- 2019-08-22 CN CN201921367261.1U patent/CN210964033U/en active Active
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