CN210700035U - Three-dimensional continuous flow micro-reaction channel, reaction substrate, micro-reactor and system - Google Patents

Three-dimensional continuous flow micro-reaction channel, reaction substrate, micro-reactor and system Download PDF

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CN210700035U
CN210700035U CN201921185279.XU CN201921185279U CN210700035U CN 210700035 U CN210700035 U CN 210700035U CN 201921185279 U CN201921185279 U CN 201921185279U CN 210700035 U CN210700035 U CN 210700035U
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reaction
channel
micro
substrate
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官星辰
王清龙
孟凡国
黄振
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Himile Mechanical Manufacturing Co Ltd
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Himile Mechanical Manufacturing Co Ltd
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Abstract

The utility model provides a three-dimensional continuous flow micro-reaction channel, a reaction substrate, a micro-reactor and a system, which comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting the mixed media; the reaction section comprises a plurality of reaction units, each reaction unit comprises a first part for mixing the fluid and a second part for dividing the fluid into at least two paths, and the first part and the second part are connected and positioned in the same plane; the reaction units are connected in sequence, and the adjacent reaction units are positioned in different planes; the present disclosure can extend channel space variation to three-dimensional spaces, can greatly improve fluid mixing effects and alleviate pressure drop.

Description

Three-dimensional continuous flow micro-reaction channel, reaction substrate, micro-reactor and system
Technical Field
The disclosure belongs to the field of micro-reaction, and particularly relates to a three-dimensional continuous flow micro-reaction channel, a reaction substrate, a micro-reactor and a system.
Background
The statements in this section merely provide background information related to the present disclosure and may not necessarily constitute prior art.
The micro chemical technology is widely applied to the fields of chemistry, chemical engineering, energy, environment and the like due to the super-strong heat and mass transfer capacity, and the micro reactor is used as a representative of the micro chemical technology, has good application prospect, is often used in physical or chemical reactions, and generally needs to mix media/materials to be reacted in the reaction processes. Separation and recombination are a typical mixing design concept, and are widely applied to design of a microreactor by breaking a laminar boundary through fluid separation and performing fluid collision through recombination.
According to the inventor's understanding, in the design of the current microreactor, a secondary flow with a direction different from the main flow direction is generally caused by various changes of the channel structure, so that a series of changes such as stretching, folding, splitting and the like occur on a fluid unit, the contact area between fluids is improved, and the mass transfer efficiency is further improved.
SUMMERY OF THE UTILITY MODEL
The present disclosure provides a three-dimensional continuous flow micro-reaction channel, a reaction substrate, a micro-reactor and a system, which can change the channel structure spatially without limiting the channel structure to a two-dimensional planar structure, so that the extension path of the channel structure is extended into a three-dimensional space, thereby greatly improving the fluid mixing effect and alleviating the pressure drop.
According to some embodiments, the following technical scheme is adopted in the disclosure:
the first purpose of the present disclosure is to provide a three-dimensional continuous flow micro-reaction channel, which no longer limits the channel structure in a two-dimensional plane, expands the extension path of the channel structure into a three-dimensional space, and no longer just simply stretches the plane, but stretches the three-dimensional level, and can effectively destroy the flow interface in the third direction, thereby ensuring that a large amount of secondary flows are generated in the flow process, and promoting the mixing.
In some embodiments, a three-dimensional continuous flow micro-reaction channel comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting mixed media;
the reaction section comprises a plurality of reaction units, each reaction unit comprises a first part for mixing fluid and a second part for dividing the fluid into at least two paths, and the first part and the second part are connected and positioned in the same plane;
the reaction units are connected in sequence, and the adjacent reaction units are positioned in different planes.
Above-mentioned design, reaction unit are located different planes, ingenious structure three-dimensional continuous flow environment, with traditional plane tensile conversion three-dimensional level tensile, can effectual destruction flow interface in the third direction, can guarantee that the reaction medium/material that the entry got into constantly merges, separates, superposes through reaction unit, and the circulation is many times, realizes the unlimited layering of reaction medium/material, finally reaches the mixed effect of high efficiency.
As a possible embodiment, the edges of the reaction unit are curved or rounded transitions. The design can effectively reduce dead zones and adapt to corresponding working conditions.
As a possible embodiment, the adjacent reaction units have a certain included angle.
Preferably, the adjacent reaction units intersect with each other.
Through the setting that has certain contained angle, can reduce reaction channel's total length, construct sufficient reaction space in limited space, guarantee the reaction effect.
As a possible embodiment, the inlet section is connected to a first component of one reaction unit and the outlet section is connected to a second component of another reaction unit.
As a possible embodiment, the edge of the first part is flush with the corresponding edge of the second part of the adjacent reaction unit.
In some embodiments, a three-dimensional continuous flow micro-reaction channel comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting mixed media;
the reaction section comprises a plurality of reaction units and transition sections, each reaction unit comprises a first part for mixing fluid and a second part for dividing the fluid into at least two paths, the first part and the second part are connected and positioned in the same plane, and the transition sections are flow channels for guiding media;
the reaction unit and the transition section are sequentially connected at intervals, and the reaction unit and the transition section are located in different planes.
As a possible embodiment, the connected reaction units and the transition section have an angle therebetween.
Preferably, the included angle is 90 °.
As a possible embodiment, the first part is a first flow channel and the second part comprises at least two branch flow channels, which branch flow channels communicate with the first flow channel.
As a possible embodiment, the branched runners are arranged in parallel.
As a possible embodiment, the first flow channel and the branch flow channel are smoothly transitioned between. The resistance action to the medium/material can be reduced as much as possible, and the dead zone is reduced.
As possible examples, the reaction channel may be extended in one direction, or may be bent, such as zigzag, s-shaped distribution, to make the most of the reaction space.
It is a second object of the present disclosure to provide a three-dimensional microreactor comprising the above-described microreactor channels, which ensures generation of a large amount of secondary flow during flow, promoting mixing.
In some embodiments, a three-dimensional micro-reaction substrate is provided, which includes a substrate body on which a plurality of reaction units in the same plane and an input section or/and an output section are disposed, the reaction units each including a first member for mixing a fluid, a second member for dividing the fluid into at least two paths, and the first member and the second member being connected to each other and located in the same plane.
Of course, there is also a three-dimensional micro-reaction substrate comprising a substrate body on which a plurality of the above-mentioned transition sections, as well as input sections or/and output sections, are arranged.
In some embodiments, a three-dimensional microreactor is provided, which comprises a first reaction substrate and a second reaction substrate, wherein a plurality of reaction units in the same plane and an input section or/and an output section are arranged on the opposite surfaces of the first reaction substrate and the second reaction substrate, the reaction units each comprise a first part for mixing fluids and a second part for dividing the fluids into at least two paths, the first part is connected with the second part and is positioned in the same plane, and the first reaction substrate and the second reaction substrate are arranged oppositely to form a three-dimensional continuous flow micro-reaction channel.
As a possible embodiment, a first end plate and a second end plate are further included, and the first end plate and the second end plate are respectively disposed at the outer sides of the first reaction substrate and the second reaction substrate.
As a possible embodiment, the first reaction substrate and the second reaction substrate are detachably connected;
the first end plate and the second end plate are detachably connected with the first reaction substrate and the second reaction substrate.
As a possible embodiment, a sealing structure is disposed between the first reaction substrate and the second reaction substrate, between the first end plate and the first reaction substrate, and between the second reaction substrate and the second end plate.
A third object of the present disclosure is to provide a three-dimensional micro-reaction system comprising a plurality of the above-mentioned microreactors, which can be adapted to long-time or large-flux requirements or other industrial requirements.
A three-dimensional micro-reaction system comprises a plurality of micro-reactors connected in series, wherein the output section of any micro-reactor is connected with the input section of the micro-reactor adjacent to the output section.
A three-dimensional micro-reaction system comprises a plurality of micro-reactors connected in parallel, wherein the input sections of any micro-reactor are connected through a multi-branch flow dividing passage, and the output sections are connected through a multi-branch flow converging passage.
Compared with the prior art, the beneficial effect of this disclosure is:
the extension state of the channel structure is expanded into a three-dimensional space, the channel structure is not simply stretched in a plane, but is stretched in three dimensions with different levels in a three-dimensional mode, a flowing interface can be effectively damaged in the third direction, a large amount of secondary flows are generated in the flowing process, and mixing is promoted.
According to the mass transfer device, through an ingenious space structure, when the flow field is broken by continuous separation and combination, convection structures such as wall collision, fluid collision and turbulence bodies are assisted, and finally high-efficiency mass transfer is realized.
The reaction system provided by the disclosure can increase reaction time or flux through the series-parallel micro-reactors, and meets the requirement of industrial production.
The method is suitable for reaction of two materials and reaction of multiple materials, can premix two materials and then feed a third material, and can expand the number of branch runners, so that the method has flexibility and expandability.
The method can flexibly change the base plates or the reactors with different reaction unit quantities according to different reaction materials/media and different reaction conditions and working conditions, and has the advantages of higher practicability and application prospect, simple preparation process and lower input cost.
This openly can carry out slick and sly processing to each reaction unit, reduces the blind spot, has guaranteed the smoothness nature and the efficiency of reaction, is fit for various operating modes.
Drawings
The accompanying drawings, which are included to provide a further understanding of the disclosure, illustrate embodiments of the disclosure and together with the description serve to explain the disclosure and are not to limit the disclosure.
FIG. 1 is a schematic structural view of an embodiment of a reaction channel according to the present disclosure;
FIG. 2 is a schematic diagram of a process for mixing reaction channel fluids according to the present disclosure;
FIG. 3 is a schematic structural view of a second embodiment of a reaction channel according to the present disclosure;
FIG. 4 is a schematic diagram of a third embodiment of a process channel according to the present disclosure;
FIG. 5 is a schematic diagram of a reactor configuration of the present disclosure;
FIGS. 6(a) and 6(b) are schematic structural views of two reaction substrates according to the present disclosure;
FIG. 7 is a schematic external view of a reactor of the present disclosure;
FIG. 8 is a schematic diagram of a series reaction system configuration of the present disclosure;
FIG. 9 is a schematic diagram of a fourth embodiment of a process channel according to the present disclosure;
fig. 10(a) (b) is a comparison graph of a fluid simulation of a prior art cardioid channel and a channel of the present disclosure.
Wherein, 1, end plate, 2, reaction plate A, 3, reaction plate B, 4, end plate;
2-1, 2-2, 3-1, 3-2 and 3-2 of an inlet and a sealing groove;
I. materials A and II and material B.
The specific implementation mode is as follows:
the present disclosure is further described with reference to the following drawings and examples.
It should be noted that the following detailed description is exemplary and is intended to provide further explanation of the disclosure. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this disclosure belongs.
It is noted that the terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of example embodiments according to the present disclosure. As used herein, the singular forms "a", "an" and "the" are intended to include the plural forms as well, and it should be understood that when the terms "comprises" and/or "comprising" are used in this specification, they specify the presence of stated features, steps, operations, devices, components, and/or combinations thereof, unless the context clearly indicates otherwise.
In the present disclosure, terms such as "upper", "lower", "left", "right", "front", "rear", "vertical", "horizontal", "side", "bottom", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only relational terms determined for convenience in describing structural relationships of the parts or elements of the present disclosure, and do not refer to any parts or elements of the present disclosure, and are not to be construed as limiting the present disclosure.
In the present disclosure, terms such as "fixedly connected", "connected", and the like are to be understood in a broad sense, and mean either a fixed connection or an integrally connected or detachable connection; may be directly connected or indirectly connected through an intermediate. The specific meanings of the above terms in the present disclosure can be determined on a case-by-case basis by persons skilled in the relevant art or technicians, and are not to be construed as limitations of the present disclosure.
The microreactor is a microreactor which is manufactured at least partially by using a micro-reaction technology or an ultra-precision machining technology, and the characteristic dimension of an internal structure (such as a flow channel) of the microreactor is generally between submicron and millimeter.
The micro-reactor in the broad sense is a micro-reaction system which takes the main purpose of reflection, mainly comprises one or more micro-reactors, and also can comprise auxiliary devices such as micro-mixing, heat exchange, separation, extraction and the like, and key components such as micro-sensors, micro-actuators and the like.
The microreactors of the present disclosure may be any of the above.
In addition, the materials, media, etc. referred to in this disclosure are all materials that participate in the mixing/reaction and may be fluids.
The reaction medium/material of the microreactors provided by the present disclosure may be gaseous, liquid or dispersed for physical or chemical reaction of reactants within the channel.
As described in the background art, the current mainstream microchannel structure mainly uses a planar two-dimensional structure, and is simply stretched in a planar manner in a third direction, so that a flow interface is difficult to be damaged in the third direction, and the effect of convection is relied on, and a pressure drop caused by strong convection also causes a burden to the operation of equipment.
The first embodiment is as follows: as shown in fig. 1, firstly, a three-dimensional micro-channel structure is provided, an extension path of the channel structure is expanded into a three-dimensional space, and is not only simply stretched in a plane, but also stretched in a three-dimensional layer, so that a flow interface can be effectively damaged in a third direction, a large amount of secondary flows can be generated in a flow process, mixing is promoted, and a good mass and heat transfer effect is realized while pressure drop is effectively reduced.
A three-dimensional continuous flow micro-reaction channel comprises an input section (in the embodiment, A in FIG. 1), a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting mixed media;
the reaction section comprises a plurality of reaction units, each reaction unit comprises a first part (in the embodiment, B, D, F shown in FIG. 1) for mixing the fluid, a second part (in the embodiment, C, E shown in FIG. 1) for dividing the fluid into at least two paths, and the first part and the second part are connected and positioned in the same plane;
the reaction units are connected in sequence, and the adjacent reaction units are positioned in different planes.
As shown in fig. 2, the flow regions and mixing mechanisms of the three-dimensional channels are ideally the following main flow modes:
the materials enter from two inlets of the area A respectively, form upper and lower layers in the area B, are separated in the area C through a bifurcation structure, and form a double-channel upper and lower layered state. And C, superposing the double-channel fluid up and down in the D area to form a four-layer fluid layering state. And (3) continuing to form branches at the position E, merging at the position F, and repeating in such a way, so that infinite layering of the fluid can be realized theoretically, and finally, a strong mixing effect is achieved.
In practical cases, due to the presence of interfacial tension, although it is difficult to completely achieve the described ideal layered state, a large amount of secondary flow can be generated in the flow due to the distortion of the spatial structure, thereby promoting mixing.
In the first embodiment, the fluid region shown in fig. 1 is only a single row of channels, and in practical applications, the channels may be densely distributed on the channel plate in a continuous series manner or in a grouped parallel manner.
That is, in other embodiments, the general extending direction of the reaction channel may not be a straight line, but a curve, such as S-shape, zigzag, etc., or a spiral in space, which is not described herein again. Such modifications will readily suggest themselves to those skilled in the art based upon this disclosure and are intended to be included within the scope of the present disclosure.
In this embodiment, adjacent reaction units intersect with each other.
In some other embodiments, the size of the included angle between adjacent reaction units can be adjusted according to specific situations. May be the same or different.
Through the setting that has certain contained angle, can reduce reaction channel's total length, construct sufficient reaction space in limited space, guarantee the reaction effect.
In this embodiment, the edge of the first part is flush with the corresponding edge of the second part of the adjacent reaction unit. The stable flowing and no leakage of the medium/material are ensured.
Because the 'n' -shaped unit module (referring to every three connected reaction units in fig. 1) of the structure has simple figure, the space on the reaction plate can be better utilized, and higher flux can be realized.
Of course, in other embodiments, it is not necessary to have an "n" shaped cell module, such as an "R" shape, an "h" shape, a "Y" shape, and so forth.
Of course, the structures of the individual shape elements may or may not be uniform.
For example, in the fourth embodiment, as shown in FIG. 9, a reaction channel is provided that is generally "R" shaped, with at least one leg in the second portion being S-shaped, having a more serpentine channel than n-shaped, to facilitate mixing. On the other hand, the pressure drop is properly reduced, the channel mainly adopts plug flow, the back mixing condition can be greatly reduced, and meanwhile, the reaction with strict dead zone requirements is also very suitable, and the relative processing process is more complex.
In addition, depending on the specific application environment or conditions, and the process conditions, in other embodiments, the specific form or length of the modules may be adjusted, for example, when the mixing requirement is general, the number of "n" modules may be reduced appropriately, and a simple channel connection may be adopted to further alleviate the pressure drop, so as to construct the embodiment as embodied in the second embodiment shown in fig. 3.
Example two: as shown in fig. 3, part of the reaction units in the "n" shaped unit module are simplified into different flow channels or transmission channels, thereby reducing the processing cost and improving the throughput.
Namely, a three-dimensional continuous flow micro-reaction channel is provided, which comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting the mixed media;
the reaction section comprises a plurality of reaction units and transition sections, each reaction unit comprises a first part for mixing fluid and a second part for dividing the fluid into at least two paths, the first part and the second part are connected and positioned in the same plane, and the transition sections are flow channels for guiding media;
the reaction unit and the transition section are sequentially connected at intervals, and the reaction unit and the transition section are positioned in different planes.
In some embodiments, the reaction units and the transition section are connected with an included angle therebetween. And the included angle between each reaction unit and the transition section can be different or the same.
In common, the first member in the above embodiments is a first flow passage, and the second member includes at least two branch flow passages, each of which communicates with the first flow passage.
In some embodiments, the branch flow channels are arranged in parallel.
Certainly, in some embodiments, the branch flow channels may also be arranged in other manners, such as being arranged in a Y shape with the first flow channel, and the first flow channel is not necessarily rectangular, and may be in other shapes, such as a trapezoid, which are all simple deformations, and are not described herein again.
In some embodiments, the structures, dimensions, etc. of the respective reaction units are the same.
However, in some embodiments, the structures and sizes of the reaction units may be different.
All the reaction units are connected end to end in sequence, but the adjacent reaction units are not in the same plane, so that a spatial three-dimensional structure is formed.
The first flow channel may be a uniform cross-sectional channel and its cross-sectional shape includes, but is not limited to, rectangular, circular, square, triangular, etc.
The branch flow channel may be a uniform cross-section channel, and the cross-sectional shape thereof includes, but is not limited to, a rectangle, a circle, a square, an ellipse, or the like.
Of course, in other embodiments, the first flow channel or the branch flow channel may be a flow channel with different cross-sections.
In some embodiments, the sum of the cross-sectional areas of the branch runners is equal to or greater than the cross-sectional area of the first runner.
In some embodiments, the first flow passage and the branch flow passage smoothly transition therebetween. The resistance effect on the medium/material can be reduced as much as possible, and the dead zone is reduced, that is, as shown in fig. 4, in the third embodiment, in some preparation process requirements, the requirement for avoiding the dead zone of the channel is severe, so that the channel form can be subjected to smooth processing, and the dead zone is reduced, so as to adapt to the corresponding working condition.
The embodiment is used for reaction of various materials, two materials can be premixed, then the third material is introduced, and the number of branch runners can be expanded, so that the flexibility and the expandability are realized.
The premixing mode can adopt a traditional stirring and mixing device besides the mixing mode by the structure provided in the above embodiment, and the details are not repeated.
The micro-reaction channels may be metal stainless steels such as 304 stainless steel, 316L stainless steel, duplex steel, super austenitic stainless steel, super duplex stainless steel, etc., nickel based alloys: hastelloy, monel, inconel, etc., special non-ferrous metals: titanium, tantalum, niobium, zirconium, and the like, or a non-metallic material such as SiC, acrylic, quartz, and the like, in combination with one or more of these.
Different passageway materials can be changed according to the reaction requirement of difference to adapt to different reaction conditions, more high pressure resistant like the metal material, the SiC material is more resistant to acid and alkali corrosion. The replacement can be performed at different chemical or physical reactions.
Simulation tests are carried out, simulation comparison is carried out on the provided three-dimensional space structure channel and a two-dimensional structure, namely the channel shown in fig. 10(a) and 10(b), and data show that the pressure drop is reduced by about 77% per unit volume under the condition that the mixing effect is not influenced or even improved (388.04 is increased by 454.43). Has good effect.
Figure BDA0002143479820000131
For a plate reactor, the present disclosure also provides a three-dimensional micro-reaction substrate, including a reaction plate body, as shown in fig. 6(a) and 6(b), a plurality of reaction units and an input section or an output section are disposed on the substrate body in the same plane, each reaction unit includes a first component for mixing fluids, a second component for dividing the fluids into at least two paths, and the first component is connected with the second component and located in the same plane.
In some embodiments, the reaction plate a (2) and the reaction plate B (3) are connected to form a three-dimensional micro-reactor, and a plurality of reaction units in the same plane and an input section or/and an output section are disposed on the facing surfaces of the reaction plate a (2) and the reaction plate B (3), the reaction units each include a first member for mixing fluids, a second member for dividing the fluids into at least two paths, the first member is connected to the second member and located in the same plane, the reaction plate a (2) and the reaction plate B (3) are arranged opposite to each other, and the reaction units, the input section and the output section form the three-dimensional continuous flow micro-reaction channel provided in the above embodiments.
Of course, in some embodiments, for the channel structure of the second embodiment shown in fig. 3, only a plurality of the above-mentioned transition sections, as well as the input section and/or the output section, may be disposed on one of the reaction plates.
In addition, the two plates are provided with an input section and an output section, which can realize the construction of a three-dimensional space reaction channel, and can be simultaneously arranged on one reaction plate or respectively arranged on different reaction plates, which can be determined by the skilled person according to common knowledge and are not described herein again.
As a possible embodiment, as shown in fig. 5, the microreactor further comprises two end plates disposed outside the reaction plate a (2) and the reaction plate B (3), respectively. And the two end plates, the reaction plate A (2) and the reaction plate B (3) are detachably connected.
In the embodiment shown in fig. 5, the four plates are provided with positioning holes (or screw holes), and are connected by bolts to form a closed whole, and the plates are sealed by mirror surfaces or sealing rings, and the specific assembly method is the same as the conventional assembly method, which is not described herein again.
The end plate and the reaction plate may be made of a material satisfying the processing conditions, such as metal or silicon carbide.
The two end plates have the same structure, are sealing covers at two ends of the equipment and simultaneously seal heat exchange channels at the back sides of the reaction plate A (2) and the reaction plate B (3).
The inner side of the reaction plate A (2) is provided with a reaction channel, and two material inlets (2-1) and (2-2) are provided, the structure is shown in figure 6(a), and the material inlets enter the channel through the side perforation of the plate. In addition, the back side is a heat exchange channel, and the heat exchange channel can be selected from the existing structure and is not described in detail here.
The inner side of the reaction plate B (3) is provided with a channel which is combined with the reaction plate A (2) in a sealing way to form a three-dimensional space channel with a material outlet (3-1), as shown in figure 6(B), the outlet enters the channel through the side perforation of the plate, the back side is a heat exchange channel, the existing structure can be selected, and is not shown here.
As possible examples, sealing O-rings are provided between the reaction plate A (2) and the reaction plate B (3), between the end plate and the reaction plate A (2), and between the reaction plate B (3) and the end plate.
After assembly, the above examples provide a plurality of reactors, with residence time increased by series connection. And meanwhile, the flux can be increased by mutually connecting in parallel. Depending on the process requirements.
In series, as shown in FIG. 8, the output section of any one microreactor is connected to the input section of an adjacent microreactor.
When in parallel connection, the input sections of any micro-reactor are connected through a multi-branch flow dividing passage, and the output sections of all micro-reactors are connected through a multi-branch flow converging passage. Namely, the input section of each micro-reactor shares one drainage port, and the output section shares one mixing output port through a branch structure.
Of course, free series-parallel combination can be realized according to the process requirements to form an array.
To sum up, no matter be little reaction channel, reactor or reaction system, can all be under the condition that processing conditions satisfied, extend to three-dimensional space with the change of channel space, can improve the fluid greatly and mix the effect and alleviate the pressure drop, when the continuous separation combination of flow field is broken, the supplementary structure of strengthening the convection current with the wall collision, the fluid collision, the vortex body etc. finally realizes high-efficient mass transfer, simultaneously, because the strong wall collision of big bent angle and the greatly reduced of reducing the reducing structure, the pressure drop has also been improved, do benefit to the industrialization and enlarge.
The above description is only a preferred embodiment of the present disclosure and is not intended to limit the present disclosure, and various modifications and changes may be made to the present disclosure by those skilled in the art. Any modification, equivalent replacement, improvement and the like made within the spirit and principle of the present disclosure should be included in the protection scope of the present disclosure.
Although the present disclosure has been described with reference to specific embodiments, it should be understood that the scope of the present disclosure is not limited thereto, and those skilled in the art will appreciate that various modifications and changes can be made without departing from the spirit and scope of the present disclosure.

Claims (20)

1. A three-dimensional continuous flow micro-reaction channel is characterized in that: the device comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting the mixed media;
the reaction section comprises a plurality of reaction units, each reaction unit comprises a first part for mixing fluid and a second part for dividing the fluid into at least two paths, and the first part and the second part are connected and positioned in the same plane;
the reaction units are connected in sequence, and the adjacent reaction units are positioned in different planes.
2. The three-dimensional continuous flow micro-reaction channel of claim 1, wherein: and a certain included angle is formed between the adjacent reaction units.
3. The three-dimensional continuous flow micro-reaction channel of claim 2, wherein: the adjacent reaction units are intersected.
4. The three-dimensional continuous flow micro-reaction channel of claim 1 or 2, wherein: the input section is connected with a first part of one reaction unit, and the output section is connected with a second part of another reaction unit.
5. The three-dimensional continuous flow micro-reaction channel of claim 1 or 2, wherein: the edges of the first part are flush with the corresponding edges of the second part of an adjacent reaction unit.
6. A three-dimensional continuous flow micro-reaction channel is characterized in that: the device comprises an input section, a reaction section and an output section which are connected in sequence, wherein the input section comprises at least two inlets for inputting reaction media and corresponding transmission channels, and the output section comprises at least one transmission channel for mixing and an outlet for outputting the mixed media;
the reaction section comprises a plurality of reaction units and transition sections, each reaction unit comprises a first part for mixing fluid and a second part for dividing the fluid into at least two paths, the first part and the second part are connected and positioned in the same plane, and the transition sections are flow channels for guiding media;
the reaction unit and the transition section are sequentially connected at intervals, and the reaction unit and the transition section are located in different planes.
7. The three-dimensional continuous flow micro-reaction channel of claim 6, wherein: and a certain included angle is formed between the connected reaction units and the transition section.
8. The three-dimensional continuous flow micro-reaction channel of claim 7, wherein: the included angle is 90 degrees.
9. The three-dimensional continuous flow micro-reaction channel of any of claims 1-3, 6-8, wherein: the first component is a first flow passage, the second component comprises at least two branch flow passages, and the branch flow passages are communicated with the first flow passage.
10. The three-dimensional continuous flow micro-reaction channel of claim 9, wherein: the branch flow channels are arranged in parallel.
11. The three-dimensional continuous flow micro-reaction channel of claim 9, wherein: the first flow passage and the branch flow passage are in smooth transition.
12. The three-dimensional continuous flow micro-reaction channel of any of claims 1-3, 6-8, wherein: the edge of the reaction unit is an arc-shaped or smooth transition section.
13. A reaction substrate, characterized in that: the reaction unit comprises a substrate body, wherein a plurality of reaction units and input sections or/and output sections which are arranged in the same plane are arranged on the substrate body, the reaction units respectively comprise first parts for mixing fluid and second parts for dividing the fluid into at least two paths, and the first parts are connected with the second parts and are positioned in the same plane.
14. A micro-reactor is characterized in that: the device comprises a first reaction substrate and a second reaction substrate, wherein a plurality of reaction units in the same plane and an input section or/and an output section are arranged on the opposite surfaces of the first reaction substrate and the second reaction substrate, the reaction units respectively comprise a first component for mixing fluid and a second component for dividing the fluid into at least two paths, the first component is connected with the second component and is positioned in the same plane, and the first reaction substrate and the second reaction substrate are oppositely arranged to form a three-dimensional continuous flow micro-reaction channel.
15. A microreactor according to claim 14, wherein: the reactor also comprises a first end plate and a second end plate, wherein the first end plate and the second end plate are respectively arranged at the outer sides of the first reaction substrate and the second reaction substrate.
16. A microreactor according to claim 14, wherein: the first reaction substrate and the second reaction substrate are detachably connected.
17. A microreactor according to claim 14, wherein: the first end plate and the second end plate are detachably connected with the first reaction substrate and the second reaction substrate.
18. A microreactor according to claim 14, wherein: and a sealing structure is arranged between the first reaction substrate and the second reaction substrate, between the first end plate and the first reaction substrate, and between the second reaction substrate and the second end plate.
19. A system, characterized by: comprising a plurality of microreactors as claimed in any of claims 14 to 18 connected in series, the output section of any one microreactor being connected to the input section of an adjacent microreactor.
20. A system, characterized by: comprising a plurality of microreactors as claimed in any of claims 14 to 18 connected in parallel, the input sections of any microreactor being connected by a multi-branch split flow path and the output sections being connected by a multi-branch confluent flow path.
CN201921185279.XU 2019-07-25 2019-07-25 Three-dimensional continuous flow micro-reaction channel, reaction substrate, micro-reactor and system Active CN210700035U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114505026A (en) * 2022-02-16 2022-05-17 微流科技(湖州)有限公司 Multi-level micro-channel reaction structure

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114505026A (en) * 2022-02-16 2022-05-17 微流科技(湖州)有限公司 Multi-level micro-channel reaction structure
CN114505026B (en) * 2022-02-16 2023-09-26 微流科技(湖州)有限公司 Multi-level micro-channel reaction structure

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