CN210108963U - Wet process chemical parameter on-line detecting instrument - Google Patents
Wet process chemical parameter on-line detecting instrument Download PDFInfo
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- CN210108963U CN210108963U CN201920567545.9U CN201920567545U CN210108963U CN 210108963 U CN210108963 U CN 210108963U CN 201920567545 U CN201920567545 U CN 201920567545U CN 210108963 U CN210108963 U CN 210108963U
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Abstract
The utility model discloses a wet processing procedure chemical parameter on-line measuring instrument, the intelligent cabinet temperature adjusting device comprises a cabinet body, be equipped with sampling unit, titration unit, reaction cup, visual sensor, data acquisition processing unit and operation display unit in the cabinet body, sampling unit extraction appearance liquid is to the reaction cup, titration unit extraction titration liquid is titrated in the reaction cup, the RGB value of liquid in the reaction cup is measured to the visual sensor and is compared with the setting value, data acquisition processing unit carries out the data processing back and shows the calculated result at operation display unit. The utility model is suitable for all color change reactions, and has wide application range; the vision sensor does not need any adjustment, the operation is simple, the result is automatically calculated and displayed, the requirement on an operator is reduced, and the labor intensity is reduced; the visual sensor does not need to be in direct contact with the solution, the service life is long, and the use and maintenance cost is reduced.
Description
Technical Field
The utility model relates to a detecting instrument especially relates to a wet processing procedure chemical parameter on-line measuring instrument.
Background
The colorimetric method is a method for measuring the concentration of a colored substance contained in a solution by comparing the shade of the color of the solution with visible light as a light source. Two types of colorimetric methods are commonly used: visual colorimetry and photoelectric colorimetry. The common visual colorimetry is a standard series method, that is, different amounts of standard solutions of an object to be measured are put into a group of identical colorimetric tubes, and color development is carried out according to the analysis steps to prepare a standard color gradation with gradually changing color. The sample solution is developed under the same condition, and compared with the standard color gradation, the standard with the most similar color is visually found out, and the content of the component to be measured in the sample is calculated and determined according to the amount of the standard solution contained in the standard solution. The photoelectric colorimetry measures the absorbance of a series of standard solutions on a photoelectric colorimeter or a similar structure, plots the absorbance to the concentration, draws a working curve, and then finds the concentration or the content of the solution of the component to be measured on the working curve according to the absorbance of the solution of the component to be measured. Compared with a visual colorimetry, the photoelectric colorimetry eliminates subjective errors, improves the measurement accuracy, and can eliminate interference by selecting an optical filter, so that the selectivity is improved.
At present, the on-line detection of the concentration of a colored substance generally adopts the working principle of photoelectric colorimetry, and is carried out by adopting the colorimetry principle of traditional monochromatic light, different light sources are required to be selected for reagents with different colors, the work of replacing the light sources is complicated and professional, and different optical filters are required to be selected to eliminate interference; the electrodes are directly contacted with the reagent solution, so that the electrodes are passivated, the maintenance of the electrodes is complicated and professional, the electrodes are required to be replaced for 1 time about 1 year in order to ensure the precision of the detection instrument, and the price of the electrodes is high and the maintenance cost is high.
Therefore, it is very meaningful to design an automatic online detection instrument for titrimetric analysis detection.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the technical problem that a wet processing procedure chemical parameter on-line measuring instrument is provided, solve traditional photoelectricity colorimetric method complex operation, problem that the maintenance cost is high.
The utility model discloses a solve above-mentioned technical problem and the technical scheme who adopts provides a wet processing procedure chemical parameter on-line measuring instrument, the intelligent cabinet temperature adjusting device comprises a cabinet body, be equipped with sampling unit, titration unit, reaction cup, visual sensor, data acquisition processing unit and operation display unit in the cabinet body, sampling unit extraction appearance liquid is to the reaction cup, titration unit extraction titration liquid titrates in to the reaction cup, the RGB value of liquid in the visual sensor measurement reaction cup and with the setting value comparison, confirm the titration end point to send the titration result to data acquisition processing unit, data acquisition processing unit carries out and shows the calculated result at operation display unit after data processing.
Furthermore, the sampling unit includes sampling pump and water pump, the titration unit includes chromogenic pump and titration pump, be equipped with the agitator in the reaction cup, data acquisition handles and is accomplished by the control panel, the operation display unit includes the touch-sensitive screen, still include the power module that supplies power in the cabinet body.
Further, the cabinet body is equipped with cabinet body door, be equipped with the analysis window on the cabinet body door, the touch-sensitive screen sets up on cabinet body door, the touch-sensitive screen rear is equipped with the touch-sensitive screen housing, the touch-sensitive screen is connected with the control panel electricity.
Furthermore, set up the volume that the sample pump extracted the appearance liquid, the volume that the color development pump extracted the color development agent, the volume and the target RGB value of water pump extraction pure water on the touch-sensitive screen.
Further, the bottom of the cabinet body is provided with a reagent cabinet, the reagent cabinet is internally provided with a reagent bottle, a pure water barrel and a waste liquid barrel, the reagent bottle is connected to the color developing pump, the pure water barrel is connected to the water pump, and the waste liquid barrel is connected with a waste discharge valve.
Furthermore, a power switch, a USB interface, a 4-20mA interface and an RS485 communication interface are arranged on the side face of the cabinet body.
Furthermore, the control panel comprises a main controller, and the main controller is connected with a power supply conversion circuit, a pump set control circuit, an electromagnetic valve circuit, a stirrer control circuit, an RS485 communication circuit, a 4-20mA output circuit, a switching value output circuit and a switching value input circuit.
Further, the power conversion circuit converts the 24V power provided by the power module into the required 5V and 3.3V power.
Further, the main controller controls the pump set to work by controlling the 12V pulse frequency through the pump set control circuit, controls the electromagnetic valve to work by controlling the on-off of the 24V circuit through the electromagnetic valve circuit through the photoelectric isolation, and controls the stirrer to work through the stirrer control circuit.
The utility model discloses contrast prior art has following beneficial effect: the wet process chemical parameter online detection instrument provided by the utility model is suitable for all color change reactions, including various conditions such as color mutation and gradual change, and has wide application range; the vision sensor for testing various reactions does not need any adjustment, is simple to operate, automatically calculates and displays results, reduces the requirements on operators and reduces the labor intensity; the visual sensor does not need to be in direct contact with the solution, the service life is long, and the use and maintenance cost is reduced.
Drawings
FIG. 1 is a schematic diagram of an apparatus for online measurement of chemical parameters in wet process according to an embodiment of the present invention;
FIG. 2 is an exploded view of an apparatus for online measurement of chemical parameters in wet process according to an embodiment of the present invention;
FIG. 3 is a control block diagram of the wet process chemical parameter on-line measuring instrument according to the embodiment of the present invention.
In the figure:
1 cabinet body door 4 touch screen 13 touch screen housing
22 sampling pump, 23 water pump and 24 color developing pump
26 titration pump 29 waste valve 30 reagent bottle
31 waste liquid barrel 32 pure water barrel 33 vision sensor
35 stirrer 36 reaction cup 38 control plate
39 45 USB interface 464-20 mA interface of power supply module
47 RS485 communication interface 49 cabinet body 50 reagent cabinet
Detailed Description
The invention is further described with reference to the following figures and examples.
FIG. 1 is a schematic structural view of an apparatus for on-line measurement of chemical parameters in wet process according to an embodiment of the present invention.
Please refer to fig. 1, the utility model discloses wet process chemical parameter on-line measuring instrument, the intelligent cabinet temperature adjusting device comprises a cabinet body, be equipped with sampling unit, titration unit, reaction cup 36, vision sensor 33, data acquisition processing unit and operation display unit in the cabinet body, sampling unit extraction sample liquid is to reaction cup 36 in, titration unit extraction titration liquid titrates to reaction cup 36 in, vision sensor 33 measures the RGB value of liquid in reaction cup 36 and compares with the setting value, confirms the titration end point to send the titration result to data acquisition processing unit, data acquisition processing unit carries out data processing after with the calculation result show at operation display unit.
Please refer to fig. 2 simultaneously, the embodiment of the present invention provides an online wet process chemical parameter measuring instrument, the sampling unit includes sampling pump 22 and water pump 23, the titration unit includes chromogenic pump 24 and titration pump 26, be equipped with agitator 35 in the reaction cup 36, data acquisition handles and is accomplished by control panel 38, the operation display unit includes touch-sensitive screen 4, still include the power module 39 who supplies power in the cabinet body. The cabinet body 49 is provided with a cabinet body door 1, the cabinet body door 1 is provided with an analysis window 5, the touch screen 4 is arranged on the cabinet body door 1, the touch screen housing 13 is arranged at the rear of the touch screen 4, and the touch screen 4 is electrically connected with the control panel 38.
Specifically, the utility model discloses wet processing procedure chemical parameter on-line measuring instrument sets up the volume that the developer was drawn to sample pump, chromogenic pump on the touch-sensitive screen 4 and extracts volume, the water pump of developer and the target RGB value.
Referring to fig. 2, in the wet process chemical parameter on-line measuring instrument of the embodiment of the present invention, a reagent cabinet 50 is disposed at the bottom of a cabinet 49, a reagent bottle 30, a pure water bucket 32 and a waste liquid bucket 31 are disposed in the reagent cabinet 50, the reagent bottle 30 is connected to the color developing pump 24, the pure water bucket 32 is connected to the water pump 23, and the waste liquid bucket 31 is connected to the waste discharge valve 29. The side of the cabinet body 49 is provided with a power switch 48, a USB interface 45, a 4-20mA interface 46 and an RS485 communication interface 47.
Referring to fig. 3, in the wet process chemical parameter on-line detecting apparatus of the embodiment of the present invention, the control panel 38 includes a main controller, and the main controller is connected to a power conversion circuit, a pump set control circuit, a solenoid valve circuit, a stirrer control circuit, an RS485 communication circuit, a 4-20mA output circuit, a switching value output circuit, and a switching value input circuit.
Specifically, the utility model discloses wet processing procedure chemical parameter on-line measuring instrument, power conversion circuit convert the 24V power that the power module provided into required 5V and 3.3V power. The main controller controls the 12V pulse frequency through the pump set control circuit to control the pump set to work, controls the electromagnetic valve to work through the electromagnetic valve circuit through the on-off of the photoelectric isolation control 24V circuit, and controls the stirrer to work through the stirrer control circuit.
To sum up, the wet process chemical parameter online detection instrument provided by the utility model is suitable for all color change reactions, including various conditions such as color mutation and gradual change, and has a wide application range; the vision sensor for testing various reactions does not need any adjustment, is simple to operate, automatically calculates and displays results, reduces the requirements on operators and reduces the labor intensity; the visual sensor does not need to be in direct contact with the solution, the service life is long, and the use and maintenance cost is reduced.
Although the present invention has been described with reference to the preferred embodiments, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (9)
1. The utility model provides a wet processing procedure chemical parameter on-line measuring instrument, its characterized in that, includes the cabinet body, be equipped with sampling unit, titration unit, reaction cup (36), vision sensor (33), data acquisition processing unit and operation display element in the cabinet body, sampling unit extracts during sample liquid arrives reaction cup (36), titration unit extraction titration liquid titrates in reaction cup (36), vision sensor (33) measure in reaction cup (36) the RGB value of liquid and compare with the setting value, confirm the titration end point to send the titration result to data acquisition processing unit, data acquisition processing unit carries out to show the calculated result at operation display element after the data processing.
2. The wet process chemical parameter on-line measuring instrument according to claim 1, wherein the sampling unit comprises a sampling pump (22) and a water pump (23), the titration unit comprises a chromogenic pump (24) and a titration pump (26), a stirrer (35) is arranged in the reaction cup (36), the data acquisition and processing are completed by a control board (38), the operation display unit comprises a touch screen (4), and the cabinet body further comprises a power supply module (39) for supplying power.
3. The wet process chemical parameter online detection instrument according to claim 2, wherein the cabinet body (49) is provided with a cabinet body door (1), the cabinet body door (1) is provided with an analysis window (5), the touch screen (4) is arranged on the cabinet body door (1), a touch screen cover (13) is arranged behind the touch screen (4), and the touch screen (4) is electrically connected with the control board (38).
4. The wet process chemical parameter on-line measuring instrument as claimed in claim 2, wherein the touch screen (4) is provided with a sample liquid amount pumped by a sampling pump, a color developing agent amount pumped by a color developing pump, a pure water amount pumped by a water pump, and target RGB values.
5. The wet process chemical parameter on-line measuring instrument as claimed in claim 2, wherein a reagent cabinet (50) is provided at the bottom of the cabinet body (49), a reagent bottle (30), a pure water tank (32) and a waste liquid tank (31) are provided in the reagent cabinet (50), the reagent bottle (30) is connected to the color developing pump (24), the pure water tank (32) is connected to the water pump (23), and the waste liquid tank (31) is connected to the waste discharge valve (29).
6. The wet process chemical parameter on-line measuring instrument as claimed in claim 2, wherein a power switch (48), a USB interface (45), a 4-20mA interface (46) and an RS485 communication interface (47) are provided on the side of the cabinet body (49).
7. The apparatus of claim 2, wherein the control board (38) comprises a main controller, and the main controller is connected to a power conversion circuit, a pump set control circuit, a solenoid valve circuit, a stirrer control circuit, an RS485 communication circuit, a 4-20mA output circuit, a switching value output circuit, and a switching value input circuit.
8. The apparatus of claim 7, wherein the power conversion circuit converts the 24V power provided by the power module into the required 5V and 3.3V power.
9. The apparatus of claim 7, wherein the main controller controls the pump set to operate by controlling a pulse frequency of 12V through the pump set control circuit, controls the solenoid valve to operate by controlling the solenoid valve circuit to switch on and off the 24V circuit through the optoelectronic isolation, and controls the stirrer to operate through the stirrer control circuit.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111141868A (en) * | 2020-03-27 | 2020-05-12 | 帝业分析仪器(上海)有限公司 | Reaction device for double-electrode detection and detection method |
CN113026021A (en) * | 2021-02-02 | 2021-06-25 | 宁波职业技术学院 | PID-based etching solution regeneration device control system and method |
-
2019
- 2019-04-24 CN CN201920567545.9U patent/CN210108963U/en active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111141868A (en) * | 2020-03-27 | 2020-05-12 | 帝业分析仪器(上海)有限公司 | Reaction device for double-electrode detection and detection method |
CN113026021A (en) * | 2021-02-02 | 2021-06-25 | 宁波职业技术学院 | PID-based etching solution regeneration device control system and method |
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Effective date of registration: 20210519 Address after: 231401 building B1, phase I Incubation Park, economic development zone, Anqing City, Anhui Province Patentee after: Anhui DIYe Analytical Instrument Co., Ltd Address before: 201805 room 402, 4th floor, 51 Lane 156, Changji Road, Anting Town, Jiading District, Shanghai Patentee before: Imperial analytical instruments (Shanghai) Co.,Ltd. |
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