CN209985411U - Ammonium glycyrrhetate extraction element - Google Patents
Ammonium glycyrrhetate extraction element Download PDFInfo
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- CN209985411U CN209985411U CN201920353427.8U CN201920353427U CN209985411U CN 209985411 U CN209985411 U CN 209985411U CN 201920353427 U CN201920353427 U CN 201920353427U CN 209985411 U CN209985411 U CN 209985411U
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Abstract
The utility model discloses an ammonium glycyrrhetate extraction element relates to chemistry chemical technology field. The device comprises a primary reaction cylinder, a secondary reaction cylinder and three reaction cylinders, wherein a feeding port I is formed in one side of the top of the primary reaction cylinder, a feeding port is formed in one side of the secondary reaction cylinder, a feeding port II is formed in one side of the top of the three reaction cylinders, opening and closing bottom plates are arranged in the primary reaction cylinder, the secondary reaction cylinder and the three reaction cylinders, and the opening and closing bottom plates enable the primary reaction cylinder, the secondary reaction cylinder and the three reaction cylinders to form a stirring reaction cylinder I, a stirring reaction cylinder II and a stirring reaction cylinder III respectively. Through setting up medicine pump one, when tentatively drawing the operation, be convenient for extract the agent in the first explosive box and extract in stirring reaction section of thick bamboo one, through setting up rabbling mechanism, be convenient for stir when drawing the operation, improve reaction efficiency, when carrying out secondary extraction operation, set up in medicine pump one is convenient for extract the agent in the first explosive box and extract stirring reaction section of thick bamboo two, be convenient for improve secondary and draw reaction efficiency.
Description
Technical Field
The utility model relates to a chemistry and chemical engineering technical field specifically is an ammonium glycyrrhetate extraction element.
Background
Ammonium glycyrrhetate is a chemical substance, and can be used for treating chronic persistent hepatitis, chronic active hepatitis, hepatotoxicity, early-stage liver cirrhosis, monoammonium glycyrrhizinate hydrate, and Qianglining.
However, in the process of preparing and extracting ammonium glycyrrhizinate, the problems of complex structure of a preparation device, unsatisfactory chemical reaction efficiency, complex operation of the reaction process and the like exist, and therefore, the ammonium glycyrrhizinate extraction device is provided to solve the problems.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
Not enough to prior art, the utility model provides an ammonium glycyrrhizate extraction element possesses reaction preparation efficiently, draws advantages such as convenient operation, has solved the device structure complicacy, and chemical reaction efficiency is unsatisfactory to and the loaded down with trivial details problem of reaction process complex operation.
(II) technical scheme
For realizing above-mentioned reaction preparation is efficient, draws convenient operation's purpose, the utility model provides a following technical scheme: an ammonium glycyrrhizinate extraction device comprises a primary reaction cylinder, a secondary reaction cylinder and three reaction cylinders, wherein a feeding port I is formed in one side of the top of the primary reaction cylinder, a feeding port is formed in one side of the secondary reaction cylinder, a feeding port II is formed in one side of the top of each of the three reaction cylinders, opening and closing bottom plates are arranged in the primary reaction cylinder, the secondary reaction cylinder and the three reaction cylinders respectively, the opening and closing bottom plates enable the primary reaction cylinder, the secondary reaction cylinder and the three reaction cylinders to form a stirring reaction cylinder I, a stirring reaction cylinder II and a stirring reaction cylinder III, a discharge port is formed in the bottom of each opening and closing bottom plate, slurry valves are arranged at the bottoms of the discharge ports, stirring mechanisms are arranged in the stirring reaction cylinder I, the stirring reaction cylinder II and the stirring reaction cylinder III, discharge ports are formed in one sides of the primary reaction cylinder, the secondary reaction cylinder and the three reaction cylinders, and filtering inclined plates located right below the discharge ports are arranged in the primary reaction cylinder, the secondary reaction, one side of the primary reaction cylinder is fixedly connected with a guide plate positioned at the bottom of the discharge port, one end of the guide plate, far away from the primary reaction cylinder, is positioned at one side of the feed port, one side of the secondary reaction cylinder is fixedly connected with a first collecting tank positioned at the discharge port, one side of the three reaction cylinders is fixedly connected with a second collecting tank positioned at the discharge port, the bottom of the second collecting tank is movably connected with a spray head through a hook, a first medicine pump and a first medicine storage box are arranged between the primary reaction cylinder and the secondary reaction cylinder, the first medicine pump and the first medicine storage box are connected through a connecting pipe, one end of the first medicine pump, far away from the first medicine storage box, is respectively communicated with a first stirring reaction cylinder and a second stirring reaction cylinder through a connecting pipe, an air pump and an air storage tank are arranged between the secondary reaction cylinder and the three reaction cylinders, the air pump and the air storage tank are, one side of three reaction barrels is equipped with medicine pump two and explosive box two, medicine pump two and explosive box two pass through connecting pipe fixed connection, the one end that explosive box two was kept away from to medicine pump two is passed through connecting pipe and three reaction barrels and shower nozzle intercommunication, the outlet has all been seted up to the bottom of just reaction barrel, time reaction barrel and three reaction barrels, the equal fixedly connected with stabilizer blade in bottom of just reaction barrel, time reaction barrel and three reaction barrels.
Further optimize this technical scheme, the thick liquid valve includes the three-way pipe, one side fixedly connected with screwed pipe of three-way pipe, be equipped with the screw thread axle in the screwed pipe, the one end fixedly connected with of screw thread axle is located the intraductal seal block of three-way.
Further optimize this technical scheme, the one end that the tee bend was kept away from to the screwed pipe is with the barrel inner wall one side fixed connection of primary reaction section of thick bamboo, inferior reaction section of thick bamboo and three reaction sections, the one end fixed connection that the sealed piece was kept away from to the screw axis is located the rotation handle of barrel one side.
This technical scheme is further optimized, rabbling mechanism includes (mixing) shaft, stirring rake and servo motor, servo motor passes through installation piece and barrel fixed connection, servo motor's output shaft passes through connecting piece fixedly connected with (mixing) shaft, equal fixedly connected with is located the stirring rake in stirring reaction section of thick bamboo one, stirring reaction section of thick bamboo two and the stirring reaction section of thick bamboo three on the (mixing) shaft.
Further optimize this technical scheme, the one end of filtering the swash plate and the barrel inner wall one side fixed connection of primary reaction section of thick bamboo, inferior reaction section of thick bamboo and three reaction sections, and be located the bottom of discharge gate.
Further optimize this technical scheme, be equipped with coarse pad on the rotation handle, the shower nozzle is hand-held type spray gun, the shower nozzle passes through coupling hose and the connecting pipe fixed connection of medicine pump two.
Further optimize this technical scheme, one side of pan feeding mouth is equipped with the baffle that is located the secondary reaction section of thick bamboo, and equal fixedly connected with linking bridge on primary reaction section of thick bamboo, secondary reaction section of thick bamboo and the three reaction sections of thick bamboo, and linking bridge and connecting pipe fixed connection.
(III) advantageous effects
Compared with the prior art, the utility model provides an ammonium glycyrrhetate extraction element possesses following beneficial effect:
1. this ammonium glycyrrhizinate extraction element through setting up medicine pump one, when tentatively drawing the operation, is convenient for extract the extracting agent in the first explosive box in stirring reaction section of thick bamboo one, through setting up rabbling mechanism, is convenient for stir when drawing the operation, improves reaction efficiency, when carrying out secondary extraction operation, sets up in medicine pump one is convenient for extract the extracting agent in the first explosive box two stirring reaction section of thick bamboos in, is convenient for improve secondary extraction reaction efficiency.
2. This ammonium glycyrrhizinate extraction element, through setting up the filtration swash plate, after extracting the operation and accomplishing, be convenient for with liquid filtration, improve reaction efficiency, through setting up the deflector, be convenient for shift the material after elementary drawing to inferior reaction cylinder, through setting up the air pump, be convenient for let in three reaction cylinders with the gaseous reactant in the gas holder, be convenient for improve reaction efficiency, through setting up the shower nozzle, be convenient for carry out the recrystallization operation to the reactant in the collecting vat two, simplify the preparation operation.
Drawings
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is the structure schematic diagram of the pulp valve of the present invention.
In the figure: 1. a primary reaction cylinder; 101. a feeding port I; 2. a secondary reaction cylinder; 201. a feeding port; 22. a baffle plate; 3. three reaction cylinders; 31. a feeding port II; 4. opening and closing the bottom plate; 5. stirring the reaction cylinder I; 51. stirring the reaction cylinder II; 52. stirring the reaction cylinder III; 6. a paddle valve; 61. a three-way pipe; 62. a threaded shaft; 63. a sealing block; 64. a threaded pipe; 65. rotating the handle; 7. a stirring mechanism; 71. a stirring shaft; 72. a stirring paddle; 73. a servo motor; 74. mounting blocks; 8. a discharge port; 9. a filtering inclined plate; 10. a guide plate; 11. collecting a first tank; 12. a second collecting tank; 13. a spray head; 14. a first medicine pump; 15. a first medicine storage box; 16. an air pump; 17. a gas storage tank; 18. a second medicine pump; 19. a second medicine storage box; 20. a support leg; 21. and a water outlet.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-2, the utility model discloses an ammonium glycyrrhizinate extraction device, which comprises a primary reaction cylinder 1, a secondary reaction cylinder 2 and three reaction cylinders 3, wherein one side of the top of the primary reaction cylinder 1 is provided with a feeding port 101, one side of the secondary reaction cylinder 2 is provided with a feeding port 201, one side of the top of the three reaction cylinders 3 is provided with a feeding port two 31, the primary reaction cylinder 1, the secondary reaction cylinder 2 and the three reaction cylinders 3 are all internally provided with an opening and closing bottom plate 4, the opening and closing bottom plate 4 enables the primary reaction cylinder 1, the secondary reaction cylinder 2 and the three reaction cylinders 3 to respectively form a stirring reaction cylinder one 5, a stirring reaction cylinder two 51 and a stirring reaction cylinder three 52, the bottom of the opening and closing bottom plate 4 is provided with a discharge port, the bottom of the discharge port is provided with a slurry valve 6, stirring mechanisms 7 are respectively arranged in the stirring reaction cylinder one 5, the stirring reaction cylinder two 51 and the stirring reaction cylinder three reaction cylinders 52, one sides of the primary reaction cylinder 1, the secondary reaction, a filter inclined plate 9 positioned right below the discharge port is arranged in each of the primary reaction cylinder 1, the secondary reaction cylinder 2 and the three reaction cylinders 3, a guide plate 10 positioned at the bottom of the discharge port 8 is fixedly connected to one side of the primary reaction cylinder 1, one end of the guide plate 10 far away from the primary reaction cylinder 1 is positioned at one side of the feed port 201, a first collecting tank 11 positioned at the discharge port 8 is fixedly connected to one side of the secondary reaction cylinder 2, a second collecting tank 12 positioned at the discharge port 8 is fixedly connected to one side of the three reaction cylinders 3, a spray head 13 is movably connected to the bottom of the second collecting tank 12 through a hook, a first medicine pump 14 and a first medicine storage tank 15 are arranged between the primary reaction cylinder 1 and the secondary reaction cylinder 2, the first medicine pump 14 and the first medicine storage tank 15 are connected through connecting pipes, one end of the first medicine pump 14 far away from the first medicine storage tank 15 is respectively communicated with the first stirring reaction cylinder 5 and the second stirring reaction cylinder 51 through, air pump 16 and gas storage tank 17 pass through connecting pipe fixed connection, the one end that gas storage tank 17 was kept away from to air pump 16 passes through connecting pipe and time reaction cylinder 2 intercommunication, one side of three reaction cylinders 3 is equipped with second 18 of medicine pump and second 19 of explosive box, second 18 of medicine pump and second 19 of explosive box pass through connecting pipe fixed connection, the one end that second 18 of medicine pump kept away from second 19 of explosive box passes through connecting pipe and three reaction cylinders 3 and shower nozzle 13 intercommunication, first reaction cylinder 1, outlet 21 has all been seted up to the bottom of time reaction cylinder 2 and three reaction cylinders 3, first reaction cylinder 1, the equal fixedly connected with stabilizer blade 20 in bottom of time reaction cylinder 2 and three reaction cylinders 3, be convenient for improve the stable effect of device.
Specifically, thick liquid valve 6 includes three-way pipe 61, one side fixedly connected with screwed pipe 64 of three-way pipe 61, be equipped with threaded shaft 62 in the screwed pipe 64, the one end fixedly connected with of threaded shaft 62 is located the sealing block 63 of three-way pipe 61, the one end and the first reaction section of thick bamboo 1 of three reaction section of thick bamboo inner wall one side fixed connection of inferior reaction section of thick bamboo 2 and three reaction section of thick bamboo 3 that three-way pipe 61 was kept away from to screwed pipe 64, the one end fixedly connected with that sealed block 63 was kept away from to threaded shaft 62 is located the rotation handle 65 of barrel one side, be convenient for rotate threaded shaft.
Specifically, the stirring mechanism 7 includes a stirring shaft 71, a stirring paddle 72 and a servo motor 73, the type of the servo motor 73 is RJ090-E03520, the servo motor 73 is fixedly connected with the cylinder body through an installation block 74, an output shaft of the servo motor 73 is fixedly connected with the stirring shaft 71 through a connecting piece, the stirring shaft 71 is fixedly connected with the stirring paddles 5 located in the first stirring reaction cylinder 5, the second stirring reaction cylinder 51 and the third stirring reaction cylinder 52, one end of the filtering inclined plate 9 is fixedly connected with the first reaction cylinder 1, one side of the inner wall of the cylinder body of the second reaction cylinder 2 and the third reaction cylinder 3, and is located at the bottom of the discharge port 8, a rough pad is arranged on the rotating handle 65, the spray head 13 is a handheld spray gun, the spray head 13 is fixedly connected with a connecting pipe of the second medicine pump 18 through a connecting hose, and by arranging the spray head 13, recrystallization operation of.
Specifically, one side of pan feeding mouth 201 is equipped with the baffle 22 that is located on time reaction cylinder 2, and equal fixedly connected with linking bridge on first reaction cylinder 1, time reaction cylinder 2 and three reaction cylinders 3, and linking bridge and connecting pipe fixed connection are convenient for keep the stability of connecting pipe.
When in use, the crude glycyrrhizic acid product is put into the primary reaction cylinder 1 from the feeding port I101, the medicine pump I14 is arranged, ethanol acidified by hydrochloric acid in the medicine storage box I15 is led into the stirring reaction cylinder I5 and the stirring reaction cylinder II 51, the stirring mechanism 7 is arranged, the reactant is fully stirred, after complete precipitation, the slurry valve 6 is arranged, the precipitate is discharged, flows into the stirring reaction cylinder II 51 through the guide plate 10 and is stirred, after the reaction is finished, the air pump 16 is arranged, ammonia gas in the air storage box 17 is led into the stirring reaction cylinder II 51 and is fully precipitated, the slurry valve 6 is arranged, the precipitate is discharged to the first reaction tank 11, the medicine pump collecting tank II 18 is arranged, glacial acetic acid in the medicine storage box II 19 is led into the stirring reaction cylinder III 52, the precipitate is dispersed and prepared into paste, the paste is stood, filtered and converted into monoammonium salt, the generated monoammonium salt is discharged to the collecting tank II 12 after being filtered, and arranging a spray head 13 to introduce glacial acetic acid in the second medicine storage box 19 into the second collecting tank 12 for washing, and then carrying out activated carbon decoloration and recrystallization on the materials in the second collecting tank 12 by using ethanol.
In summary, the ammonium glycyrrhizinate extraction device is provided with the first medicine pump 14, so that the extractant in the first medicine storage box 15 can be conveniently pumped into the first stirring reaction cylinder 5 during the primary extraction operation, the stirring mechanism 7 is arranged, so that the stirring is convenient during the extraction operation, the reaction efficiency is improved, when the secondary extraction operation is carried out, the first medicine pump 14 is arranged to facilitate the extraction agent in the first medicine storage box 15 to be pumped into the second stirring reaction cylinder 51 and to facilitate the improvement of the secondary extraction reaction efficiency, and by arranging the filtering inclined plate 9, after the extraction operation is finished, the liquid is convenient to filter, the reaction efficiency is improved, the guide plate 10 is arranged, the material after primary extraction is convenient to transfer to the secondary reaction cylinder 2, the air pump 16 is arranged, so that the gas reactant in the air storage tank 17 can be conveniently introduced into the three reaction cylinders 3, the reaction efficiency can be conveniently improved, and the spray head 13 is arranged, so that the recrystallization operation of the reactants in the second collecting tank 12 is facilitated.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides an ammonium glycyrrhizinate extraction element, includes primary reaction section of thick bamboo (1), inferior reaction section of thick bamboo (2) and three reaction section of thick bamboo (3), its characterized in that: the feeding port I (101) is formed in one side of the top of the primary reaction cylinder (1), the feeding port (201) is formed in one side of the secondary reaction cylinder (2), the feeding port II (31) is formed in one side of the top of the tertiary reaction cylinder (3), the opening and closing bottom plates (4) are arranged in the primary reaction cylinder (1), the secondary reaction cylinder (2) and the tertiary reaction cylinder (3), the opening and closing bottom plates (4) enable the primary reaction cylinder (1), the secondary reaction cylinder (2) and the tertiary reaction cylinder (3) to form the stirring reaction cylinder I (5), the stirring reaction cylinder II (51) and the stirring reaction cylinder III (52) respectively, the discharge port is formed in the bottom of the opening and closing bottom plate (4), the slurry valve (6) is arranged at the bottom of the discharge port, the stirring mechanism (7) is arranged in the stirring reaction cylinder I (5), the stirring reaction cylinder II (51) and the stirring reaction cylinder III (52), and the primary reaction cylinder (1), Discharge gates (8) are respectively formed in one sides of the secondary reaction cylinder (2) and the three reaction cylinders (3), a filter inclined plate (9) positioned under the discharge port is respectively arranged in the primary reaction cylinder (1), the secondary reaction cylinder (2) and the three reaction cylinders (3), a guide plate (10) positioned at the bottom of the discharge port (8) is fixedly connected to one side of the primary reaction cylinder (1), one end, far away from the primary reaction cylinder (1), of the guide plate (10) is positioned at one side of the feed port (201), a first collecting tank (11) positioned at the discharge port (8) is fixedly connected to one side of the secondary reaction cylinder (2), a second collecting tank (12) positioned at the discharge port (8) is fixedly connected to one side of the three reaction cylinders (3), a spray nozzle (13) is movably connected to the bottom of the second collecting tank (12) through a hook, a first medicine pump (14) and a first medicine storage box (15) are arranged between the primary reaction cylinder (1) and the secondary reaction, the device is characterized in that a first medicine pump (14) and a first medicine storage box (15) are connected through a connecting pipe, one end, far away from the first medicine storage box (15), of the first medicine pump (14) is communicated with a first stirring reaction cylinder (5) and a second stirring reaction cylinder (51) through the connecting pipe respectively, an air pump (16) and an air storage box (17) are arranged between a second reaction cylinder (2) and a third reaction cylinder (3), the air pump (16) and the air storage box (17) are fixedly connected through the connecting pipe, one end, far away from the air storage box (17), of the air pump (16) is communicated with the second reaction cylinder (2) through the connecting pipe, a second medicine pump (18) and a second medicine storage box (19) are arranged on one side of the third reaction cylinder (3), the second medicine pump (18) and the second medicine storage box (19) are fixedly connected through the connecting pipe, one end, far away from the second medicine storage box (19) of the second medicine pump (18) is communicated with the third, the bottom of the primary reaction cylinder (1), the bottom of the secondary reaction cylinder (2) and the bottom of the three reaction cylinders (3) are provided with water outlets (21), and the bottom of the primary reaction cylinder (1), the bottom of the secondary reaction cylinder (2) and the bottom of the three reaction cylinders (3) are fixedly connected with support legs (20).
2. The ammonium glycyrrhizinate extraction device according to claim 1, wherein: the slurry valve (6) comprises a three-way pipe (61), a threaded pipe (64) is fixedly connected to one side of the three-way pipe (61), a threaded shaft (62) is arranged in the threaded pipe (64), and one end of the threaded shaft (62) is fixedly connected with a sealing block (63) located in the three-way pipe (61).
3. The ammonium glycyrrhizinate extraction device according to claim 2, wherein: one end of the threaded pipe (64), which is far away from the three-way pipe (61), is fixedly connected with one side of the inner wall of the primary reaction barrel (1), the secondary reaction barrel (2) and the three reaction barrels (3), and one end of the threaded shaft (62), which is far away from the sealing block (63), is fixedly connected with a rotating handle (65) which is positioned on one side of the barrels.
4. The ammonium glycyrrhizinate extraction device according to claim 1, wherein: stirring mechanism (7) include (mixing) shaft (71), stirring rake (72) and servo motor (73), servo motor (73) are through installation piece (74) and barrel fixed connection, the output shaft of servo motor (73) passes through connecting piece fixedly connected with (mixing) shaft (71), equal fixedly connected with is located stirring reaction section of thick bamboo one (5), stirring reaction section of thick bamboo two (51) and stirring reaction section of thick bamboo three (52) stirring rake (72).
5. The ammonium glycyrrhizinate extraction device according to claim 1, wherein: one end of the filtering sloping plate (9) is fixedly connected with one side of the inner wall of the primary reaction cylinder (1), the secondary reaction cylinder (2) and the three reaction cylinders (3), and is positioned at the bottom of the discharge hole (8).
6. The ammonium glycyrrhizinate extraction device according to claim 3, wherein: the rotary handle (65) is provided with a rough pad, the spray head (13) is a handheld spray gun, and the spray head (13) is fixedly connected with a connecting pipe of the second medicine pump (18) through a connecting hose.
7. The ammonium glycyrrhizinate extraction device according to claim 1, wherein: one side of pan feeding mouth (201) is equipped with baffle (22) that are located on time reaction cylinder (2), and equal fixedly connected with linking bridge, and linking bridge and connecting pipe fixed connection are gone up in first reaction cylinder (1), time reaction cylinder (2) and three reaction cylinder (3).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201920353427.8U CN209985411U (en) | 2019-03-20 | 2019-03-20 | Ammonium glycyrrhetate extraction element |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201920353427.8U CN209985411U (en) | 2019-03-20 | 2019-03-20 | Ammonium glycyrrhetate extraction element |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111228848A (en) * | 2020-02-14 | 2020-06-05 | 冯琨 | Cooling crystallization cleaning and purifying device |
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2019
- 2019-03-20 CN CN201920353427.8U patent/CN209985411U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111228848A (en) * | 2020-02-14 | 2020-06-05 | 冯琨 | Cooling crystallization cleaning and purifying device |
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