CN208512543U - A kind of reaction kettle with cleaning function - Google Patents
A kind of reaction kettle with cleaning function Download PDFInfo
- Publication number
- CN208512543U CN208512543U CN201820818907.2U CN201820818907U CN208512543U CN 208512543 U CN208512543 U CN 208512543U CN 201820818907 U CN201820818907 U CN 201820818907U CN 208512543 U CN208512543 U CN 208512543U
- Authority
- CN
- China
- Prior art keywords
- tank body
- reaction kettle
- cleaning
- cleaning function
- agitating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of reaction kettles with cleaning function, it includes tank body, the cover for being set to the top of the tank, the material outlet and agitating device for being set to the tank base, feeding device is provided on the cover and/or tank body, the agitating device includes being arranged in the intracorporal agitating paddle of tank, agitating shaft and driving mechanism, the agitating shaft passes through the cover or tank body, and one end of the agitating shaft is connected with the agitating paddle, the other end is connected with the driving mechanism；It is characterized by: being additionally provided with cleaning discharge port on the tank body, filter element is provided in the cleaning discharge port.The continuous operation of subtle powder preparation, cleaning may be implemented in the utility model, reduces operating cost, has saved occupied area and equipment investment cost；And it ensures that fine particle is not reunited in preparation and cleaning process, while can effectively wash the stabilizer and impurity for being adsorbed on particle surface, obtain satisfactory product.
Description
Technical field
The utility model relates to chemical fields, and in particular to a kind of reaction kettle with cleaning function, can be used for micron and
The reaction of nano particle prepares and cleaning.
Background technique
Particle such as copper, silver, copper oxide, aluminium oxide, silica etc. is prepared using chemical method, is usually completed in a solvent
Preparation is reunited since the fine particles such as micron, nanometer are easy, and preparing can be by introducing ultrasonic device, being added surely in reaction process
The modes such as agent, control reaction temperature are determined to prevent from reuniting between particle.In the fine particle usually prepared can containing a large amount of stabilizers,
Reducing agent and other impurities need to clean the powder of preparation in order to not influence the subsequent use of these fine particles.
Traditional fine particle production technology needs take out the powder granule of preparation from reaction kettle to be cleaned, and
It needs sufficiently to clean reaction kettle just and can be carried out production preparation next time, fine particle cleaning process is quite cumbersome, can not carry out
Continuous operation, it is time-consuming, laborious, production efficiency is low, and invest it is big, take up space greatly.
Utility model content
The product in reaction kettle clean in kettle in order to realize, reaches continuous production, shortens the production cycle, improves life
The purpose of efficiency is produced, the utility model provides a kind of reaction kettle with cleaning function, and specific technical solution is as follows.
A kind of reaction kettle with cleaning function comprising tank body, is set to institute at the cover for being set to the top of the tank
Material outlet, the agitating device of tank base are stated, feeding device, the agitating device are provided on the cover and/or tank body
Including setting in the intracorporal agitating paddle of tank, agitating shaft and driving mechanism, the agitating shaft passes through the cover or tank body, and described
One end of agitating shaft is connected with the agitating paddle, and the other end is connected with the driving mechanism；It is characterized by: on the tank body also
It is provided with cleaning discharge port, the cleaning discharge outlet is provided with filter element.
Optionally, the filter element plays the function that will be separated by the fine particle for cleaning discharge port with liquid,
The filter element can be located in discharge port, can also be located on reaction kettle body inner wall locating for discharge port.
Further, the temperature control chamber for controlling temperature is formed in the side wall of the tank body, on the side wall of the tank body
It is provided with the fluid inlet and fluid outlet being connected to the temperature control chamber.
Further, spiral is provided with fluid conduit systems in the side wall of the tank body, be provided on the side wall of the tank body with
The fluid inlet and fluid outlet of the fluid conduit systems connection.
Further, the reaction kettle further includes having ultrasonic device, and ultrasonic device (9) ultrasonic probe is arranged described
In tank body (1), the setting of control power supply the tank body (1) outside.
Further, the reaction kettle further includes having air compressor, and the air compressor passes through pipeline and the tank
The inner cavity of body is connected to.
Further, the filter element is one of filter membrane, stainless steel filtering net or a variety of.
Further, side wall and/or the bottom of the tank body is arranged in the cleaning discharge port.
Further, the cleaning discharge port is also connected with devil liquor recovery tank.
The continuous operation of subtle powder preparation, cleaning may be implemented in the utility model, reduces operating cost, saves
Occupied area and equipment investment cost；And ensure that fine particle is not reunited in preparation and cleaning process, while energy
The stabilizer and impurity for being adsorbed on particle surface effectively are washed, obtains satisfactory product.
Detailed description of the invention
Fig. 1 is a kind of schematic diagram of the reaction kettle with cleaning function of the utility model.
In figure: tank body 1, cover 2, material outlet 3, agitating paddle 4, agitating shaft 5, driving mechanism 6, cleaning discharge port 7, fluid
Conduit 8, ultrasonic device 9, air compressor 10, devil liquor recovery tank 11, filter element 12, feeding device 13, bracket 14.
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawing.
A kind of reaction kettle with cleaning function comprising tank body 1, the cover 2 for being set to 1 top of tank body, setting
Material outlet 3 and agitating device in 1 bottom of tank body, cover 2 and tank body 1 form the closed receiving that is used for and react
Bracket 14 is arranged in the inner cavity of material, 1 bottom of tank body, and feeding device 13 is provided on the cover 2, and the agitating device includes setting
Agitating paddle 4, agitating shaft 5 and driving mechanism 6 in tank body 1 are set, the agitating shaft 5 passes through the cover 2, and the agitating shaft
5 one end is connected with the agitating paddle 4, and the other end is connected with the driving mechanism 6, and driving mechanism 6 is motor etc.；The tank body
Cleaning discharge port 7 is additionally provided on 1, side wall and/or the bottom of the tank body 1, the cleaning is arranged in the cleaning discharge port 7
Filter element 12 is provided in discharge port 7, the discharge port 7 is also connected with devil liquor recovery tank 11.
Wherein, feeding device 13 can be set on tank body 1 or be arranged on cover 2 and/or tank body 1 simultaneously, feeding device
13 quantity can according to need to be arranged, and the valve of control material disengaging, opening when needing to feed are provided on feeding device
Valve does not need the airtightness closed in valve holding tank body 1 when charging；Material outlet 3 and cleaning discharge port 7 are provided with control
Make the valve of opening and closing；The filter element 12 is preferably filter membrane, and the filtering gap of filter membrane is less than the big of the powder for needing to recycle
It is small.Agitating shaft 5 is illustrated in Fig. 1 across the cover 2, but agitating shaft 5 can also pass through the cover 2 and protrude into tank body 1
It is interior.
Optionally, it for the ease of controlling the temperature in reaction kettle, can be formed in the side wall of the tank body 1 for controlling temperature
The temperature control chamber of degree is provided with the fluid inlet and fluid outlet being connected to the temperature control chamber on the side wall of the tank body 1.Cooling water
Or hot water enters that temperature control is intracavitary from fluid inlet, and the heat in tank body 1 is taken away or transferred heat in tank body 1, it is cooling
Water or hot water are flowed out from fluid outlet again.
Optionally, for the ease of controlling the temperature in reaction kettle, spiral is provided with fluid conduit systems in the side wall of the tank body 1
8, the fluid inlet 81 and fluid outlet 82 being connected to the fluid conduit systems 8 are provided on the side wall of the tank body 1.Cooling water or
Hot water enters in fluid conduit systems 8 from fluid inlet 81, and the heat in tank body 1 is taken away or transferred heat in tank body 1, cold
But water or hot water are flowed out from fluid outlet 82 again.
Powder reunites during the reaction and convenient for cleaning to powder in order to prevent, and the reaction kettle further includes having
Ultrasonic device 9, the ultrasonic device 9 are arranged in the tank body 1.Ultrasonic device 9 may be provided at the interior table of tank body 1 or cover 2
Face, the ultrasonic wave that such ultrasonic device 9 issues directly act on the fluid of tank body 1, improve the effect for preventing reuniting and powder
Cleaning effect.
In order to control the pressure in reaction kettle and improve cleaning efficiency, the reaction kettle further includes having air compressor
10, the air compressor is connected to by pipeline with the inner cavity of the tank body 1.10 one side of air compressor can be reaction kettle
The pressure that reaction needs is provided, on the other hand after completing to powder cleaning process, air compressor 10 increases in reaction kettle
Pressure can accelerate the rate of filtration of waste liquid and impurity, save the working time of cleaning.
When preparing subtle powder, the raw material (material) for reacting required is added in tank body 1 from feeding device 13, is entered by fluid
Cooling water or hot water are added in mouth 81 to be discharged to control the interior temperature of tank body 1, cooling water or hot water from fluid outlet 82, adjusts
Finely dispersed fine particle is prepared in the stirring rate of agitating paddle 4 and the power of ultrasonic device 9, through air after fully reacting
Compressor 10 adjusts the pressure in tank body 1, opens the valve of cleaning discharge port 7, and waste liquid and impurity passed through under high pressure effect
Filter component 12 flows in devil liquor recovery tank 11, and powder stays in reaction kettle, and cleaning solution is then added from feeding device 13, utilizes
The cleaning to powder is realized in the ultrasonic cleaning effect of ultrasonic device 9 and the turning effort of agitating paddle 4, and waste liquid flows into waste liquid after cleaning
In recycling can 11, powder can be carried out step is cleaned multiple times according to specific needs, after the completion of cleaning, open material outlet 3
Valve, satisfactory subtle product particle are recycled from material outlet 3.
The embodiments of the present invention are described above in conjunction with attached drawing, in the absence of conflict, this is practical new
The feature in embodiment and embodiment in type can be combined with each other.The utility model is not limited to above-mentioned specific embodiment party
Formula, the above mentioned embodiment is only schematical, rather than limitation, those skilled in the art are in this reality
With under novel enlightenment, when not departing from the utility model aims and scope of the claimed protection, can also make very
Multi-form, these are belonged within the protection scope of the utility model.
Claims (8)
1. a kind of reaction kettle with cleaning function comprising tank body (1), the cover (2) being set at the top of the tank body (1),
It is set to the material outlet (3), agitating device of the tank body (1) bottom, is provided with and adds on the cover (2) and/or tank body (1)
To expect device (13), the agitating device includes agitating paddle (4), agitating shaft (5) and the driving mechanism (6) being arranged in tank body (1),
The agitating shaft (5) passes through the cover (2) or tank body (1), and one end of the agitating shaft (5) and the agitating paddle (4) phase
Even, the other end is connected with the driving mechanism (6)；It is characterized by: cleaning discharge port (7) is additionally provided on the tank body (1),
Filter element (12) are provided at the cleaning discharge port (7).
2. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the side of the tank body (1)
It is formed with the temperature control chamber for controlling temperature in wall, is provided with the stream being connected to the temperature control chamber on the side wall of the tank body (1)
Body entrance and fluid outlet.
3. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the side of the tank body (1)
Spiral is provided with fluid conduit systems (8) in wall, is provided with the stream being connected to the fluid conduit systems (8) on the side wall of the tank body (1)
Body entrance (81) and fluid outlet (82).
4. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the reaction kettle further includes
Have ultrasonic device (9), in the tank body (1), control power supply is arranged in the tank for ultrasonic device (9) the ultrasonic probe setting
Body (1) is outside.
5. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the reaction kettle further includes
Have air compressor (10), the air compressor is connected to by pipeline with the inner cavity of the tank body (1).
6. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the filter element (12)
For one or both of filter membrane, stainless steel filtering net.
7. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the cleaning discharge port
(7) side wall and/or the bottom in the tank body (1) are set.
8. a kind of reaction kettle with cleaning function according to claim 1, which is characterized in that the cleaning discharge port
(7) devil liquor recovery tank (11) are also connected with.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820818907.2U CN208512543U (en) | 2018-05-30 | 2018-05-30 | A kind of reaction kettle with cleaning function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820818907.2U CN208512543U (en) | 2018-05-30 | 2018-05-30 | A kind of reaction kettle with cleaning function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208512543U true CN208512543U (en) | 2019-02-19 |
Family
ID=65340638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820818907.2U Active CN208512543U (en) | 2018-05-30 | 2018-05-30 | A kind of reaction kettle with cleaning function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208512543U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110935688A (en) * | 2019-12-11 | 2020-03-31 | 上海玺唐半导体科技有限公司 | Cleaning method |
| CN111112224A (en) * | 2020-01-16 | 2020-05-08 | 连云港秉文科技有限公司 | Ultrasonic micro powder cleaning disperser and dispersing method |
-
2018
- 2018-05-30 CN CN201820818907.2U patent/CN208512543U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110935688A (en) * | 2019-12-11 | 2020-03-31 | 上海玺唐半导体科技有限公司 | Cleaning method |
| CN111112224A (en) * | 2020-01-16 | 2020-05-08 | 连云港秉文科技有限公司 | Ultrasonic micro powder cleaning disperser and dispersing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206404763U (en) | A kind of reactor dehydration device with sampled functions | |
| CN208943563U (en) | A kind of Multifunction filtering machine | |
| CN208512543U (en) | A kind of reaction kettle with cleaning function | |
| CN212090976U (en) | A filter equipment for piperic acid crystallization | |
| CN107866192A (en) | The retracting device of solid matter | |
| CN109261100A (en) | A kind of reaction system being used to prepare carbon material | |
| CN212288393U (en) | Novel polyurethane high-pressure foaming machine | |
| CN113786787A (en) | Ultrahigh-temperature continuous carbon nanotube purifying equipment | |
| CN211099033U (en) | Dicyandiamide recovery plant in glycocyamine production process | |
| CN209287257U (en) | A kind of warehouse separated type reacting furnace suitable for salting out method | |
| CN208758199U (en) | Ion exchange resin sieves purification device | |
| CN208995151U (en) | A kind of reacting furnace | |
| CN109499504A (en) | A kind of horizontal degassing reaction kettle | |
| CN209113492U (en) | It is a kind of to be rotated into rewinding carbon nanotube equipment for purifying automatically | |
| CN210393741U (en) | Boron carbide purification device | |
| CN209438579U (en) | A kind of horizontal degassing reaction kettle | |
| CN213811341U (en) | Gas-solid fluidized bed dryer suitable for low glass transition temperature solid acrylic resin | |
| CN205269657U (en) | Reaction kettle | |
| CN109264759B (en) | Reaction furnace | |
| CN107552808A (en) | The scale continuous preparation device and method of a kind of nano-nickel powder | |
| CN207221443U (en) | A kind of coating agitation and filtration device | |
| CN209696887U (en) | A kind of plastic additive synthesis reaction vessel | |
| CN206777924U (en) | Heparin sodium adsorption resin elutes recovery device | |
| CN207845782U (en) | A kind of powder electroless closing device | |
| CN208770937U (en) | A kind of Water filtration device for filtering |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 7th Floor, Building B8, Lugu Enterprise Plaza, Yuelu District, Changsha City, Hunan Province, 410000 Patentee after: Aerospace Science and Industry (Changsha) New Materials Research Institute Co.,Ltd. Address before: 410205 7th floor, building B8, Lugu Enterprise Square, Yuelu District, Changsha City, Hunan Province Patentee before: CHANGSHA ADVANCED MATERIALS INDUSTRIAL RESEARCH INSTITUTE Co.,Ltd. |