CN209985404U - Metal organic chemistry light reaction unit - Google Patents
Metal organic chemistry light reaction unit Download PDFInfo
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- CN209985404U CN209985404U CN201920327188.9U CN201920327188U CN209985404U CN 209985404 U CN209985404 U CN 209985404U CN 201920327188 U CN201920327188 U CN 201920327188U CN 209985404 U CN209985404 U CN 209985404U
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- light reaction
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Abstract
The utility model discloses a metal organic chemistry light reaction unit, including base, reactor and ultraviolet lamp, the reactor includes reaction zone and parcel at the outside cooling cycle district of reaction zone, the ultraviolet lamp is inserted in the reaction zone by the reactor top, be equipped with temperature probe in the cooling cycle district. This metal organic chemistry light reaction unit can cool off fast when the photoreaction to the cooling is even, and stable in structure relies on clamping device enough for the reactor provides fixed effect in the reaction moreover, guarantees going on that the reaction can be stable.
Description
Technical Field
The utility model relates to a light response equipment technical field, concretely relates to metal organic chemistry light reaction unit.
Background
The photochemical reaction refers to a chemical reaction which can be carried out only under the irradiation of a certain light source, a specific photochemical reaction needs to be carried out in a photoreaction device, a large amount of heat is generated during the reaction, the temperature needs to be reduced through continuous cooling, the existing photochemical reaction device has the phenomena of low cooling speed and uneven cooling during the reaction, the carrying out of the photochemical reaction is influenced, a part of the photochemical reaction device adopts vibration stirring to achieve the uniform cooling, but the vibration drives the whole photochemical reaction device to vibrate at the same time, and the carrying out of the photochemical reaction is greatly influenced due to unstable fixation.
SUMMERY OF THE UTILITY MODEL
In order to solve the problem, the utility model provides a metal organic chemistry light reaction unit.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the utility model provides a metal organic chemistry light reaction unit, includes base, reactor and ultraviolet lamp, the reactor includes reaction zone and the outside cooling circulation district of parcel in reaction zone, the ultraviolet lamp is inserted in the reaction zone by the reactor top, be equipped with temperature probe in the cooling circulation district, be equipped with magnetic stirrers in the base, magnetic stirrers includes rotating magnet cover and magnetic stirrers, the reactor sets up in rotating magnet cover top, magnetic stirrers sets up inside cooling circulation district, cooling circulation district right side top is equipped with the inlet tube, inlet tube one end connection condenser, cooling circulation district left side top is equipped with the outlet pipe, be equipped with the stop valve on the outlet pipe.
Preferably, the base is provided with at least three fixing rods, the fixing rods are provided with supporting plates, and the supporting plates are provided with clamping devices for fixing the reactor.
Preferably, the clamping device is respectively arranged at four symmetrical positions of the reactor, namely the front, the back, the left and the right, and comprises an air cylinder, a push rod is arranged on the air cylinder, and a clamping piece is arranged at one end of the push rod.
Preferably, one side of the clamping piece is provided with an anti-slip pad.
Preferably, the clip has a curvature on the inside.
The utility model discloses following beneficial effect has:
this metal organic chemistry light reaction unit can cool off fast when the photoreaction to the cooling is even, and stable in structure relies on clamping device enough for the reactor provides fixed effect in the reaction moreover, guarantees going on that the reaction can be stable.
Drawings
Fig. 1 is a schematic structural diagram of a metal organic chemical light reaction device according to the present invention.
Fig. 2 is a schematic structural diagram of a clamping device of a metal organic chemical light reaction device according to the present invention.
In the figure: 1. the device comprises a base, 2, a fixing rod, 3, a temperature probe, 4, a water outlet pipe, 5, a stop valve, 6, a clamping device, 7, a supporting plate, 8, an ultraviolet lamp, 9, a reaction zone, 10, a cooling circulation zone, 11, a water inlet pipe, 12, a condenser, 13, a magnetic stirrer, 14, a magnetic stirrer, 15, a rotary magnet cover, 16, a clamping piece, 17, a push rod, 18, an air cylinder, 19, an anti-skid pad, 20 and a reactor.
Detailed Description
In order to make the objects and advantages of the present invention more apparent, the present invention will be described in further detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
As shown in fig. 1, the embodiment of the present invention provides a metal organic chemical light reaction apparatus, which comprises a base 1, a reactor 20 and an ultraviolet lamp 8, wherein the reactor 20 comprises a reaction zone 9 and a cooling circulation zone 10 wrapped outside the reaction zone, the ultraviolet lamp 8 is inserted into the reaction zone 9 from above the reactor 20, a mounting frame 21 for mounting the ultraviolet lamp 8 is arranged above the reactor 20, the ultraviolet lamp passes through a mounting ring at the center of the mounting frame 21, the upper end of the ultraviolet lamp is fixedly connected to the mounting ring through a bolt, a temperature probe 3 is arranged in the cooling circulation zone 10, a magnetic stirrer 13 is arranged in the base 1, the magnetic stirrer 13 comprises a rotary magnet cover 15 and a magnetic stirrer 14, the reactor 20 is arranged above the rotary magnet cover 15, the magnetic stirrer 14 is arranged inside the cooling circulation zone 10, a water inlet pipe 11 is arranged above the right side of the cooling circulation zone 10, one end of the water inlet pipe 11 is connected to a condenser 12, a water outlet pipe 4 is arranged above the left side of the cooling circulation area 10, and a stop valve 5 is arranged on the water outlet pipe 4.
According to above-mentioned structure, ultraviolet lamp 8 is used for improving the illumination, when reacting, condenser 12 provides cooling water, get into cooling circulation district 10 through inlet tube 11, because cooling circulation district 10 wraps up the cooling that can be comprehensive quick outside the reaction zone completely, temperature probe 3 is used for measuring the temperature of cooling circulation district 10, the circulating temperature in cooling circulation district 10 can be stabilized to the leaving water temperature through controlling condenser 12, thereby be favorable to the internal reaction of reaction zone 9, the continuous stirring of 14 of magnetic stirrers 13 control magnetic stirrers in the cooling process, be favorable to even cooling, can adjust stirring rate according to actual conditions.
As shown in fig. 1, at least three fixing rods 2 are arranged on the base 1, a supporting plate 7 is arranged on each fixing rod 2, a clamping device 6 for fixing the reactor 20 is arranged on each supporting plate 7, and under the stirring action of the magnetic stirrer 13, the clamping device 6 can provide a fixing effect for the reactor 20, so that the reaction can be stably carried out.
As shown in fig. 2, the clamping devices 6 are respectively arranged at four symmetrical positions of the reactor 20, the clamping devices 6 comprise air cylinders 18, the air cylinders 18 are provided with push rods 17, one ends of the push rods 17 are provided with clamping pieces 16, the clamping devices 6 are arranged at four symmetrical positions of the reactor 20, the clamping and fixing effects are further enhanced, the push rods 17 are pushed through the air cylinders 18, the clamping pieces 16 at one ends of the push rods 17 are used for clamping the reactor 20, and the clamping force can be adjusted according to actual conditions.
Further, during the reaction, water vapor may exist between the clip 16 and the reactor 20 to cause wet slip of the contact surface, and the slip-proof pad 19 is provided on one side of the clip 16 to effectively prevent slip.
Further, the reactor 20 is a circular reaction beaker, and the inner side of the clamping piece 16 has a certain radian, so that the clamping piece and the reactor 20 can have mutually matched radians, thereby further facilitating the fixation and clamping.
To sum up, the utility model discloses the device can cool off fast when the photoreaction to the cooling is even, and stable in structure relies on clamping device 6 enough for reactor 20 provides fixed effect at the reaction time moreover, guarantees going on that the reaction can be stable.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, a plurality of modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (5)
1. A metal organic chemistry light reaction unit which characterized in that: including base, reactor and ultraviolet lamp, the reactor includes reaction zone and the outside cooling circulation district of parcel in the reaction zone, the ultraviolet lamp is inserted in the reaction zone by the reactor top, be equipped with temperature probe in the cooling circulation district, be equipped with magnetic stirrers in the base, magnetic stirrers includes rotating magnet cover and magnetic stirrers, the reactor sets up in rotating magnet cover top, magnetic stirrers sets up inside the cooling circulation district, cooling circulation district right side top is equipped with the inlet tube, inlet tube one end connection condenser, cooling circulation district left side top is equipped with the outlet pipe, be equipped with the stop valve on the outlet pipe.
2. The metal organic chemical light reaction device according to claim 1, wherein: the reactor is characterized in that at least three fixed rods are arranged on the base, supporting plates are arranged on the fixed rods, and clamping devices for fixing the reactor are arranged on the supporting plates.
3. The metal organic chemical light reaction device according to claim 2, wherein: the clamping device is respectively arranged at four symmetrical positions of the reactor, namely the front, the back, the left and the right, and comprises an air cylinder, a push rod is arranged on the air cylinder, and clamping pieces are arranged at one end of the push rod.
4. The metal organic chemical light reaction device according to claim 3, wherein: and one side of the clamping piece is provided with an anti-slip pad.
5. The metal-organic chemical photoreaction apparatus according to claim 3 or 4, wherein: the inside of the clamping piece is provided with a radian.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920327188.9U CN209985404U (en) | 2019-03-15 | 2019-03-15 | Metal organic chemistry light reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920327188.9U CN209985404U (en) | 2019-03-15 | 2019-03-15 | Metal organic chemistry light reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209985404U true CN209985404U (en) | 2020-01-24 |
Family
ID=69289654
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920327188.9U Expired - Fee Related CN209985404U (en) | 2019-03-15 | 2019-03-15 | Metal organic chemistry light reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209985404U (en) |
-
2019
- 2019-03-15 CN CN201920327188.9U patent/CN209985404U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200124 Termination date: 20210315 |