CN209612377U - A kind of de- ammonium salt device of tri-phenyl-ethyl phosphonium bromide hypergravity - Google Patents

Abstract

The utility model discloses a kind of tri-phenyl-ethyl phosphonium bromide hypergravities to take off ammonium salt device, including processing case, fitting case is provided with above the processing case, the two sides of the processing case are provided with lifting device, the fitting case is internally provided with centrifugal device, and the inner wall of the processing case is welded with partition, and the partition and the top for processing case offer through slot, it is provided with heating device below the partition, is provided with water plug on the right side of the processing case.The setting that the utility model passes through processing case, fitting case, lifting device, centrifugal device, partition, heating device, water plug and drying unit, de- ammonium salt device is set to significantly increase three phenyl-bromide Phosphonium purity of second base, ammonium salt can be generated during preparation by solving current three phenyl-bromide Phosphonium of second base simultaneously, the ratio increase of ammonium salt will affect the purity of three phenyl-bromide Phosphonium of second base, thus the problem of influencing its using effect.

Description

A kind of de- ammonium salt device of tri-phenyl-ethyl phosphonium bromide hypergravity

Technical field

The utility model relates to chemical equipment technical field, specially a kind of tri-phenyl-ethyl phosphonium bromide hypergravity takes off ammonium salt Device.

Background technique

Three phenyl-bromide Phosphonium of second base is also known as Ethyltriphenylphosphonium brimide, and molecular formula is C20H20BrP, and molecular weight is 371.2506, it is very promising quaternary phosphonium salt class product, is mainly used for as catalyst, and can be used for organic synthesis, it is new Purposes is constantly opened up, and demand increases year by year, and three phenyl-bromide Phosphonium of second base can generate ammonium salt, ammonium salt during preparation at present Ratio increase will affect the purity of three phenyl-bromide Phosphonium of second base, so that its using effect is influenced, because of a kind of ethyl three of the invention It is very necessary that phenyl phosphonium bromide hypergravity, which takes off ammonium salt device,.

Utility model content

The purpose of this utility model is to provide a kind of tri-phenyl-ethyl phosphonium bromide hypergravities to take off ammonium salt device, has greatly Three phenyl-bromide Phosphonium purity of increase second base the advantages of, solving current three phenyl-bromide Phosphonium of second base can produce during preparation Raw ammonium salt, the ratio increase of ammonium salt will affect the purity of three phenyl-bromide Phosphonium of second base, thus the problem of influencing its using effect.

To achieve the above object, the utility model provides the following technical solutions: a kind of tri-phenyl-ethyl phosphonium bromide hypergravity De- ammonium salt device, including case is processed, fitting case is provided with above the processing case, the two sides of the processing case are provided with liter Falling unit, the fitting case are internally provided with centrifugal device, and the inner wall of the processing case is welded with partition, the partition with plus The top of work case offers through slot, and heating device is provided with below the partition, is provided with pumping on the right side of the processing case Water installations are provided with drying unit on the left of the processing case.

Preferably, the lifting device includes bottom plate, and the quantity of the bottom plate is two and the surface with processing case is welded Connect, electric telescopic rod be welded at the top of the bottom plate, be welded with top plate at the top of the electric telescopic rod, the top plate it is interior Side and the surface of fitting case are welded.

Preferably, the centrifugal device includes servo motor, the bottom of the servo motor and the bottom of accessory box cavity It is fixedly connected, the output shaft of the servo motor is welded with driving wheel, and charging leakage is communicated at the center at the top of the fitting case Bucket, the bottom through flow fitting case of the loading hopper and inner cavity for extending to fitting case is connected with tube by bearing, institute The surface for stating tube is welded with driven wheel, the driving wheel and driven wheel by belt transmission connection, the bottom of the tube according to Secondary through flow fitting case and processing case and the inner cavity for extending to processing case is welded with fixed plate, the bottom of the fixed plate be welded with from The bottom of heart bucket, the tube runs through fixed plate and extends to the inner cavity of centrifugal barrel.

Preferably, the heating device includes heater, and the bottom of the heater and the bottom of processing box cavity are fixed It connects, is fixedly connected with mixing tank at the top of the heater, is communicated with drain pipe, and drain on the left of the mixing tank bottom The surface of pipe is communicated with solenoid valve, and the bottom of drain pipe runs through processing case and extends to the outside of processing case.

Preferably, the water plug includes water pump, is fixedly connected on the right side of the left side of the water pump and processing case, described The bottom of water pump is communicated with water inlet pipe, and outlet pipe is communicated at the top of the water pump, and the outlet pipe is passed through far from one end of water pump It wears processing case and the inner cavity for extending to processing case is connected to the right side of mixing tank.

Preferably, the drying unit includes air-heater, is fixedly connected on the left of the right side of the air-heater and processing case, Air-exhausting duct is communicated at the top of the air-heater, the one end of the air-exhausting duct far from air-heater is through processing case and extends to processing The inner cavity of case is communicated with jet thrust.

Preferably, the front of the processing case offers observation window, and the inner wall of the observation window is fixedly connected with glass, institute It states the front of processing case and is located at below observation window and be fixedly connected with control panel.

Compared with prior art, the beneficial effects of the utility model are as follows:

1, by processing, case, fitting case, lifting device, centrifugal device, partition, heating device, draw water the utility model dress The setting with drying unit is set, so that de- ammonium salt device is significantly increased three phenyl-bromide Phosphonium purity of second base, while solving mesh Preceding three phenyl-bromide Phosphonium of second base can generate ammonium salt during preparation, and the ratio increase of ammonium salt will affect ethyltriphenyl phosphonium bromide The purity of Phosphonium, thus the problem of influencing its using effect.

2, the utility model is able to drive centrifugal device and carries out upper and lower movement, make to be centrifuged by the setting of lifting device After device completes centrifugal process, can be moved to above partition and be dried, by the setting of centrifugal device, can by from The mixed liquor of ammonium salt and water is purged by heart mode, so that the ammonium salt inside three phenyl-bromide Phosphonium of second base is purged, is increased The purity for adding three phenyl-bromide Phosphonium of second base, by the setting of heating device, can accelerate ammonium salt and water merges speed, to increase Clear water can be pumped into inside mixing tank by the working efficiency for adding whole device by the setting of water plug, then by ethyl three Ammonium salt inside phenyl phosphonium bromide is merged with clear water, can be by the ethyl triphen after purification by the setting of drying unit Base phosphonium bromide carries out rapid draing, is conveniently collected, and by the setting of observation window, worker can be facilitated to observe inside device Working condition can facilitate worker to operate whole device by the setting of control panel.

Detailed description of the invention

FIG. 1 is a schematic structural view of the utility model；

Fig. 2 is the utility model structure front view；

Fig. 3 is the top view of the utility model loading hopper；

Fig. 4 is the top view of the utility model centrifugal barrel.

In figure: 1 processing case, 2 fitting cases, 3 lifting devices, 31 bottom plates, 32 electric telescopic rods, 33 top plates, 4 centrifugal devices, 41 servo motors, 42 driving wheels, 43 loading hoppers, 44 tubes, 45 driven wheels, 46 fixed plates, 47 centrifugal barrels, 5 partitions, 6 heating Device, 61 heaters, 62 mixing tanks, 63 solenoid valves, 7 water plugs, 71 water pumps, 72 outlet pipes, 8 drying units, 81 air-heaters, 82 air-exhausting ducts, 83 jet thrusts, 9 observation windows, 10 control panels.

Specific embodiment

The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.

Fig. 1-4, a kind of de- ammonium salt device of tri-phenyl-ethyl phosphonium bromide hypergravity, including processing case 1 are please referred to, case 1 is processed Top be provided with fitting case 2, the two sides of processing case 1 are provided with lifting device 3, and fitting case 2 is internally provided with centrifugation dress 4 are set, the inner wall of processing case 1 is welded with partition 5, and partition 5 and the top for processing case 1 offer through slot, the lower section setting of partition 5 There is heating device 6, the right side of processing case 1 is provided with water plug 7, and the left side of processing case 1 is provided with drying unit 8, lifting dress Setting 3 includes bottom plate 31, and the quantity of bottom plate 31 is two and the surface with processing case 1 is welded, and the top of bottom plate 31 is welded with electricity Dynamic telescopic rod 32, the top of electric telescopic rod 32 are welded with top plate 33, and the inside of top plate 33 and the surface of fitting case 2 are welded, led to The setting for crossing lifting device 3 is able to drive centrifugal device 4 and carries out upper and lower movement, after so that centrifugal device 4 is completed centrifugal process, The top that partition 5 can be moved to is dried, and centrifugal device 4 includes servo motor 41, the bottom of servo motor 41 and accessory The bottom of 2 inner cavity of case is fixedly connected, and the output shaft of servo motor 41 is welded with driving wheel 42, is connected at the center at 2 top of fitting case It is connected with loading hopper 43, the bottom through flow fitting case 2 of the loading hopper 43 and inner cavity for extending to fitting case 2 is connected by bearing activity It is connected to tube 44, the surface of tube 44 is welded with driven wheel 45, driving wheel 42 and driven wheel 45 and is sequentially connected by belt, tube 44 bottom sequentially pass through fitting case 2 and process case 1 and extend to processing case 1 inner cavity be welded with fixed plate 46, fixed plate 46 Bottom be welded with centrifugal barrel 47, the bottom of tube 44 is through fixed plate 46 and extends to the inner cavity of centrifugal barrel 47, passes through centrifugation The mixed liquor of ammonium salt and water can be purged by the setting of device 4 by centrifugation, thus by three phenyl-bromide Phosphonium of second base Internal ammonium salt is purged, and increases the purity of three phenyl-bromide Phosphonium of second base, and heating device 6 includes heater 61, heater 61 Bottom with processing 1 inner cavity of case bottom be fixedly connected, the top of heater 61 is fixedly connected with mixing tank 62,62 bottom of mixing tank Drain pipe is communicated on the left of portion, and the surface of drain pipe is communicated with solenoid valve 63, the bottom of drain pipe through processing case 1 and is prolonged The outside for extending to processing case 1, by the setting of heating device 6, can accelerate ammonium salt and water merges speed, to increase entire The working efficiency of device, water plug 7 include water pump 71, and the left side of water pump 71 is fixedly connected with the right side of processing case 1, water pump 71 Bottom be communicated with water inlet pipe, the top of water pump 71 is communicated with outlet pipe 72, the one end of outlet pipe 72 far from water pump 71 through plus Work case 1 and extend to processing case 1 inner cavity be connected to the right side of mixing tank 62, can be by clear water by the setting of water plug 7 It is pumped into inside mixing tank 62, then merges the ammonium salt inside three phenyl-bromide Phosphonium of second base with clear water, drying unit 8 includes The right side of air-heater 81, air-heater 81 is fixedly connected with the left side of processing case 1, and the top of air-heater 81 is communicated with air-exhausting duct 82, Air-exhausting duct 82 far from air-heater 81 one end through processing case 1 and extend to processing case 1 inner cavity be communicated with jet thrust 83, pass through Three phenyl-bromide Phosphonium of second base after purification can be carried out rapid draing, conveniently be collected, process by the setting of drying unit 8 The front of case 1 offers observation window 9, and the inner wall of observation window 9 is fixedly connected with glass, processes the front of case 1 and is located at observation window 9 Lower section be fixedly connected with control panel 10, by the setting of observation window 9, worker can be facilitated to observe the work feelings inside device Condition can facilitate worker to operate whole device by the setting of control panel 10, by processing case 1, fitting case 2, rise The setting of falling unit 3, centrifugal device 4, partition 5, heating device 6, water plug 7 and drying unit 8 keeps de- ammonium salt device very big Increase three phenyl-bromide Phosphonium purity of second base, while solving current three phenyl-bromide Phosphonium of second base and can be produced during preparation Raw ammonium salt, the ratio increase of ammonium salt will affect the purity of three phenyl-bromide Phosphonium of second base, thus the problem of influencing its using effect.

In use, being powered by external power supply for whole device, and by control panel 10 come to whole device Operation control is carried out, which carries out de- ammonium salt work using ammonium salt characteristic soluble easily in water, and worker passes through charging Funnel 43 adds materials, and material is flowed into inside centrifugal barrel 47 by tube 44, and electric telescopic rod 32 drives top plate 33 downward at this time Mobile, top plate 33 drives fitting case 2 to move down, and fitting case 2 drives tube 44 to move down, and tube 44 drives 46 He of fixed plate Centrifugal barrel 47 moves down, and until centrifugal barrel 47 is located at the inside of mixing tank 62, water pump 71 will by outlet pipe 72 at this time Clear water is infused into inside mixing tank 62, and heater 61 is begun to warm up, and at the same time, the output shaft of servo motor 41 drives actively The slowly rotation of wheel 42, driving wheel 42 drive driven wheel 45 slowly to rotate by belt, and driven wheel 45 drives tube 44 slowly to rotate, Tube 44 drives centrifugal barrel 47 slowly to rotate by fixed plate 46, so that the ammonium salt inside three phenyl-bromide Phosphonium of second base is sufficient It being dissolved in water, solenoid valve 63 is opened at this time, mixed solution outflow, and the output shaft of servo motor 41 quickly rotates at this time, And it drives centrifugal barrel 47 quickly to rotate, carries out centrifugal movement, the moisture inside three phenyl-bromide Phosphonium of second base is thrown away, has been dehydrated Cheng Hou, electric telescopic rod 32 drive centrifugal barrel 47 to move up, and are moved to 5 top of partition, air-heater 81 passes through air-exhausting duct at this time 82 and jet thrust 83 three phenyl-bromide Phosphonium of second base is dried, it is dry after electric telescopic rod 32 drive centrifugal barrel 47 be moved to plus The top of work case 1, so that worker be facilitated to collect, therefore to significantly increase three phenyl-bromide Phosphonium of second base pure for the de- ammonium salt device Degree.

In summary: the tri-phenyl-ethyl phosphonium bromide hypergravity takes off ammonium salt device, passes through processing case 1, fitting case 2, lifting The cooperation of device 3, centrifugal device 4, partition 5, heating device 6, water plug 7 and drying unit 8 solves current ethyl triphen Base phosphonium bromide can generate ammonium salt during preparation, and the ratio increase of ammonium salt will affect the purity of three phenyl-bromide Phosphonium of second base, The problem of to influence its using effect.

While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (7)

1. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity takes off ammonium salt device, including processing case (1), it is characterised in that: the processing It is provided with above case (1) fitting case (2), the two sides of processing case (1) are provided with lifting device (3), the fitting case (2) inner wall of be internally provided with centrifugal device (4), processing case (1) is welded with partition (5), the partition (5) and processing The top of case (1) offers through slot, is provided with heating device (6) below the partition (5), the right side of processing case (1) Side is provided with water plug (7), is provided with drying unit (8) on the left of the processing case (1).

2. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described Lifting device (3) includes bottom plate (31), and the quantity of the bottom plate (31) is two and welds with the surface of processing case (1), institute It states and is welded at the top of bottom plate (31) electric telescopic rod (32), be welded with top plate (33) at the top of the electric telescopic rod (32), The inside of the top plate (33) and the surface of fitting case (2) are welded.

3. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described Centrifugal device (4) includes servo motor (41), the fixed company in the bottom of the servo motor (41) and the bottom of fitting case (2) inner cavity Connect, the output shaft of the servo motor (41) is welded with driving wheel (42), be communicated at the center at the top of the fitting case (2) into Funnel (43), the bottom through flow fitting case (2) of the loading hopper (43) and the inner cavity for extending to fitting case (2) pass through bearing It is connected with tube (44), the surface of the tube (44) is welded with driven wheel (45), the driving wheel (42) and driven wheel (45) it is sequentially connected by belt, the bottom of the tube (44), which sequentially passes through fitting case (2) and processing case (1) and extends to, to be added The inner cavity of work case (1) is welded with fixed plate (46), and the bottom of the fixed plate (46) is welded with centrifugal barrel (47), the tube (44) bottom runs through fixed plate (46) and extends to the inner cavity of centrifugal barrel (47).

4. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described Heating device (6) includes heater (61), and the bottom of the heater (61) is fixedly connected with the bottom of processing case (1) inner cavity, It is fixedly connected with mixing tank (62) at the top of the heater (61), is communicated with drain on the left of mixing tank (62) bottom Pipe, and the surface of drain pipe is communicated with solenoid valve (63), the bottom of drain pipe through processing case (1) and extends to processing case (1) Outside.

5. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described Water plug (7) includes water pump (71), is fixedly connected on the right side of the left side of the water pump (71) and processing case (1), the water pump (71) bottom is communicated with water inlet pipe, is communicated with outlet pipe (72) at the top of the water pump (71), and the outlet pipe (72) is separate One end of water pump (71) through processing case (1) and extend to processing case (1) inner cavity be connected to the right side of mixing tank (62).

6. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described Drying unit (8) includes air-heater (81), is fixedly connected on the left of the right side of the air-heater (81) and processing case (1), described It is communicated at the top of air-heater (81) air-exhausting duct (82), the one end of the air-exhausting duct (82) far from air-heater (81) is through processing case (1) and extend to processing case (1) inner cavity be communicated with jet thrust (83).

7. a kind of tri-phenyl-ethyl phosphonium bromide hypergravity according to claim 1 takes off ammonium salt device, it is characterised in that: described The front of processing case (1) offers observation window (9), and the inner wall of the observation window (9) is fixedly connected with glass, the processing case (1) front and it is located at below observation window (9) and is fixedly connected with control panel (10).