CN209596875U - A kind of hydrogen chloride and methane chloride separator - Google Patents

A kind of hydrogen chloride and methane chloride separator Download PDF

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Publication number
CN209596875U
CN209596875U CN201920107405.3U CN201920107405U CN209596875U CN 209596875 U CN209596875 U CN 209596875U CN 201920107405 U CN201920107405 U CN 201920107405U CN 209596875 U CN209596875 U CN 209596875U
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CN
China
Prior art keywords
adsorption tower
methane
tower
hydrogen chloride
chloride
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Expired - Fee Related
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CN201920107405.3U
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Chinese (zh)
Inventor
陈开华
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Chongqing Haoran Energy Conservation And Environmental Protection Technology Consulting Service Co Ltd
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Chongqing Haoran Energy Conservation And Environmental Protection Technology Consulting Service Co Ltd
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Priority to CN201920107405.3U priority Critical patent/CN209596875U/en
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Publication of CN209596875U publication Critical patent/CN209596875U/en
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Abstract

The utility model discloses a kind of hydrogen chloride and methane chloride separator, including adsorption tower, the bottom end of the adsorption tower is equipped with solvent outlet, the adsorption tower in the horizontal direction on side be equipped with methane chloride entrance and hydrogen chloride and export, and methane chloride entrance is close to the bottom end of adsorption tower, the adsorption tower is welded with two fixing seats far from the side of methane chloride entrance, the bottom of one fixing seat is fixedly installed with driving motor, the driving end of the driving motor is fixedly connected with screw rod through one end of fixing seat, the outer surface of the screw rod is arranged with pedestal.A kind of hydrogen chloride described in the utility model and methane chloride separator, improve the attachment site of spray liquid, spray liquid and the methane chloride of Ta Nei and containing hydrogen chloride are come into full contact with, improve the fused to improve its separation rate of methane chloride and spray liquid, furthermore facilitate the folding of top cover and then simplify the process of uncapping and facilitate cleaning operation in progress tower, bring better prospect of the application.

Description

A kind of hydrogen chloride and methane chloride separator
Technical field
The utility model relates to methane chloride separating-purifying device field, in particular to a kind of hydrogen chloride and methane chlorination Object separator.
Background technique
Methane chloride includes monochloro methane, methylene chloride, chloroform and tetrachloromethane, with the development of industrialization, Methane chloride has become important industrial chemicals and organic solvent, in the production process of chloromethanes and its methane chloride not It is evitable to generate a large amount of byproduct hydrogen chloride, thus the byproduct hydrogen chloride for needing to generate in the actual production process and Methane chloride is separated, and is improved the obtained rate of methane chloride and is reduced the loss of raw material.
Existing hydrogen chloride is separated with methane chloride using spraying specific shower spray of solvent at the top of adsorption tower, under adsorption tower End is passed through the methane chloride of containing hydrogen chloride, after the methane chloride and spray liquid of containing hydrogen chloride come into full contact in tower, due to Hydrogen chloride is immiscible with shower spray of solvent, so that hydrogen chloride gas is discharged from adsorption tower upper end, methane chloride and spray The mixture of liquid is discharged from tower bottom, while the separation of hydrogen chloride and methane chloride, this mistake are completed by processes such as recycling, purifications The methane chloride of containing hydrogen chloride there is a problem of contacting being not enough with spray liquid in journey causes separation rate poor, is located at simultaneously The spray flow container of tower top is not easy to carry out processing of uncapping because position is higher, causes to operate less during for clearing up in tower Easily, therefore during use, certain influence is brought, for this purpose, it is proposed that a kind of hydrogen chloride and methane chloride point From device.
Utility model content
Purpose of the utility model is to solve disadvantage existing in the prior art, and a kind of hydrogen chloride and first proposed Alkane chloride separator.
To achieve the above object, the technical solution that the utility model is taken are as follows:
A kind of hydrogen chloride and methane chloride separator, including adsorption tower, the bottom end of the adsorption tower go out equipped with solvent Mouthful, the adsorption tower in the horizontal direction on side be equipped with methane chloride entrance and hydrogen chloride and export, and methane chloride enters Mouth is welded with two fixing seats, an institute far from the side of methane chloride entrance close to the bottom end of adsorption tower, the adsorption tower The bottom for stating fixing seat is fixedly installed with driving motor, and the driving end of the driving motor is fixedly connected through one end of fixing seat There is screw rod, the outer surface of the screw rod is arranged with pedestal, and the top of the adsorption tower, which is fitted into, top cover, outside the top of the top cover Surface is equipped with spray flow container, and the internal vertical of the adsorption tower is equipped with newel, and the outer surface parallel sleeve of the newel is equipped with The top of multiple combination tower trays, the top cover is equipped with cap-opening mechanism close to the side of spray flow container.
It is as above-mentioned technical proposal to further describe:
The cap-opening mechanism includes hydraulic cylinder, hydraulic stem, attachment base, curved bar, L shape bar, spring stack and stand, the liquid Cylinder pressure is set to the outer surface of cupular part of pedestal, and hydraulic stem, the top of the hydraulic stem are fixedly connected at the top of the hydraulic cylinder Outer surface is rotatably connected to attachment base, and the outer surface of the attachment base is welded with curved bar, and the side sidewall weld of the top cover has L Shape bar, the outer surface of cupular part bolt of the L shape bar are fixed with spring stack, and the outer surface of cupular part of the top cover is welded with stand.
It is as above-mentioned technical proposal to further describe:
The combination tower tray includes lantern ring, taper tower tray and side plate, and the lantern ring is set in the outer surface of newel, institute The lateral wall for stating lantern ring is welded with taper tower tray, and the inner sidewall of the adsorption tower is fitted with side plate.
It is as above-mentioned technical proposal to further describe:
The L shape bar vertically on right-angle side be fixedly connected by pin shaft with curved bar, and L shape bar passes through spring stack It is fixedly connected with curved bar, the curved bar is fixedly connected by pin shaft with stand close to one end of stand.
It is as above-mentioned technical proposal to further describe:
The screw rod is vertically installed between two fixing seats, and the pedestal is connected by screw rod and driving motor transmission It connects.
It is as above-mentioned technical proposal to further describe:
Side side wall of the top cover inside adsorption tower is provided with multiple spray heads, Duo Gesuo about newel annular State spray head through top cover one end pass through separating tube with spray flow container be fixedly connected.
It is as above-mentioned technical proposal to further describe:
The lateral wall of the lantern ring is symmetrically arranged with four taper tower trays about newel, four taper tower trays Outer surface is hollow out setting, and the inner sidewall distribution of the adsorption tower is fitted with side plate corresponding with four taper tower trays, And taper tower tray is equipped with corresponding convex architecture with the lateral wall of side plate.
In the utility model: 1. hydrogen chloride and methane chloride separator pass through the combination tower tray of setting, combined column Disk is made of lantern ring, taper tower tray and side plate, and four taper tower trays are socketed by lantern ring and newel, while four conical towers Disk is corresponded with four side plates and taper tower tray and the lateral wall of side plate are equipped with corresponding convex architecture, improves spray liquid Attachment site, the methane chloride of spray liquid and Ta Nei and containing hydrogen chloride sprayed from tower top spray flow container is filled Tap touching, raising methane chloride and spray liquid fuse, and then improve its separation rate;
2. the hydrogen chloride and methane chloride separator, curved bar be fixedly connected by pin shaft with stand L shape bar simultaneously and The pin shaft of curved bar connects, while passing through Driven by Hydraulic Cylinder hydraulic stem, hydraulic stem up-and-down movement, so that top cover is able to carry out Under operation of uncapping, since attachment base and hydraulic stem are rotatably assorted, while by the effect of driving motor and screw rod so that passing through It is mobile that the cap-opening mechanism of pedestal connection can carry out the position in vertical direction, and then facilitates the folding of top cover, meanwhile, simplification is opened Lid process, which facilitates, carries out cleaning operation in tower, more preferable relative to traditional approach.
Detailed description of the invention
Fig. 1 be the utility model proposes a kind of hydrogen chloride and methane chloride separator overall structure diagram;
Fig. 2 is schematic enlarged-scale view at A in Fig. 1;
Fig. 3 be the utility model proposes a kind of hydrogen chloride and methane chloride separator combination tower tray vertical view Figure;
In figure: 1, adsorption tower;2, solvent outlet;3, methane chloride entrance;4, hydrogen chloride exports;5, fixing seat;6, it drives Dynamic motor;7, screw rod;8, pedestal;9, top cover;10, flow container is sprayed;11, newel;12, tower tray is combined;13, cap-opening mechanism;14, Hydraulic cylinder;15, hydraulic stem;16, attachment base;17, curved bar;18, L shape bar;19, spring stack;20, stand;21, lantern ring;22, taper Tower tray;23, side plate.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
It is in the description of the present invention, it should be noted that term " center ", "upper", "lower", "left", "right", " perpendicular Directly ", the orientation or positional relationship of the instructions such as "horizontal", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, and is only For ease of description the utility model and simplify description, rather than the device or element of indication or suggestion meaning must have it is specific Orientation, be constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention;Term " first ", " the Two ", " third " is used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance;In addition, unless otherwise specific Regulation and restriction, term " installation ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, be also possible to It is detachably connected, or is integrally connected;It can be mechanical connection, be also possible to be electrically connected;It can be directly connected, can also lead to It crosses intermediary to be indirectly connected, can be the connection inside two elements.It for the ordinary skill in the art, can be with Concrete condition understands the concrete meaning of above-mentioned term in the present invention.
Referring to Fig.1-3, a kind of hydrogen chloride and methane chloride separator, including adsorption tower 1, the bottom end of adsorption tower 1 are set Have solvent outlet 2, for being discharged methane chloride and spray liquid, adsorption tower 1 in the horizontal direction on side be equipped with methane chlorination Object entrance 3 and hydrogen chloride outlet 4, and methane chloride entrance 3, close to the bottom end of adsorption tower 1, adsorption tower 1 is far from methane chloride The side of entrance 3 is welded with two fixing seats 5, standing screw 7, and the bottom of a fixing seat 5 is fixedly installed with driving motor 6, The driving end of driving motor 6 is fixedly connected with screw rod 7 through one end of fixing seat 5, and the outer surface of screw rod 7 is arranged with pedestal 8, holds Cap-opening mechanism 13 is carried, the top of adsorption tower 1 is chimeric top cover 9, and the outer surface of cupular part of top cover 9 is equipped with spray flow container 10, adsorption tower 1 Internal vertical be equipped with newel 11, fixed Combination tower tray 12, the outer surface parallel sleeve of newel 11 is equipped with multiple combination tower trays 12, the top of top cover 9 is equipped with cap-opening mechanism 13 close to the side of spray flow container 10.
Cap-opening mechanism 13 include hydraulic cylinder 14, hydraulic stem 15, attachment base 16, curved bar 17, L shape bar 18, spring stack 19 and Stand 20, hydraulic cylinder 14 are set to the outer surface of cupular part of pedestal 8, and the top of hydraulic cylinder 14 is fixedly connected with hydraulic stem 15, hydraulic The outer surface of cupular part of bar 15 is rotatably connected to attachment base 16, facilitates curved bar 17 and hydraulic stem 15 that can carry out certain angle rotation, The outer surface of attachment base 16 is welded with curved bar 17, and the side sidewall weld of top cover 9 has L shape bar 18, the outer surface of cupular part of L shape bar 18 Bolt is fixed with spring stack 19, guarantees that the stable connection of curved bar 17 and L shape bar 18, the outer surface of cupular part of top cover 9 are welded with stand 20。
Combining tower tray 12 includes lantern ring 21, taper tower tray 22 and side plate 23, and lantern ring 21 is set in the appearance of newel 11 Face connects four taper tower trays 22, and the lateral wall of lantern ring 21 is welded with taper tower tray 22, and the inner sidewall of adsorption tower 1 is fitted with side Plate 23.
L shape bar 18 vertically on right-angle side be fixedly connected with curved bar 17 by pin shaft, and L shape bar 18 passes through spring Column 19 is fixedly connected with curved bar 17, guarantees that the stable connection of curved bar 17 and L shape bar 18, curved bar 17 pass through close to one end of stand 20 Pin shaft is fixedly connected with stand 20, and curved bar 17 and stand 20 can be rotated.
Screw rod 7 is vertically installed between two fixing seats 5, and pedestal 8 is sequentially connected by screw rod 7 and driving motor 6, is passed through The driving of driving motor 6 is so that the cap-opening mechanism 13 that pedestal 8 carries is able to carry out vertical displacement movement.
Side side wall of the top cover 9 inside adsorption tower 1 is provided with multiple spray heads, multiple sprays about 11 annular of newel Leaching head passes through separating tube through one end of top cover 9 and is fixedly connected with spray flow container 10, convenient for uniformly sprinkling spray liquid.
The lateral wall of lantern ring 21 is symmetrically arranged with four taper tower trays 22, the appearance of four taper tower trays 22 about newel 11 Face is hollow out setting, and the inner sidewall distribution of adsorption tower 1 is fitted with side plate 23 corresponding with four taper tower trays 22, and conical tower Disk 22 is equipped with corresponding convex architecture with the lateral wall of side plate 23, increases the attachment site of spray liquid, and then improve gas With the contact area of spray liquid.
Working principle: the utility model is hydrogen chloride and methane chloride separator, the methane chloride of containing hydrogen chloride Enter in tower from the methane chloride entrance 3 of 1 lower end of adsorption tower, rises in tower, the spray flow container 10 on top cover 9 is set There are multiple spray heads and then in can uniformly spray spray liquid in tower, right multiple be parallel to each other is arranged by newel 11 in tower Combine tower tray 12, the lateral wall of lantern ring 21 is symmetrically arranged with four taper tower trays 22 about newel 11, four taper tower trays 22 Outer surface is hollow out setting, and the inner sidewall distribution of adsorption tower 1 is fitted with side plate 23 corresponding with four taper tower trays 22, and bores Shape tower tray 22 is equipped with corresponding convex architecture with the lateral wall of side plate 23, increases the attachment site of spray liquid, and then improve The contact area of gas and spray liquid improves separation rate, and the gas after lock out operation is discharged from hydrogen chloride outlet 4, methane chlorine The mixture of compound and spray liquid is discharged from 1 bottom solvent outlet 2 of adsorption tower, in addition, being connected at top cover 9 by 20 pin shaft of stand Curved bar 17 be rotatably assorted with L shape bar 18 by pin shaft, 17 other end of curved bar passes through attachment base 16 and is fixedly connected with hydraulic stem 15, Attachment base 16 is rotatably assorted with hydraulic stem 15, is made convenient for top cover 9 and 15 angle change of hydraulic stem by the driving of hydraulic cylinder 14 It obtains top cover 9 to be able to carry out upper and lower operation of uncapping, while 1 side of adsorption tower passes through the driving of driving motor 6 so that screw rod 7 connects The cap-opening mechanism 13 that carries of pedestal 8 be able to carry out vertical displacement movement, and then facilitate the folding of top cover 9, simplify process of uncapping Facilitate and carries out cleaning operation in tower, it is more practical.
Finally, it should be noted that the above descriptions are merely preferred embodiments of the present invention, it is not limited to this Utility model, although the utility model is described in detail with reference to the foregoing embodiments, for those skilled in the art For, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic Be equivalently replaced, any modification, equivalent replacement, improvement and so on, should be included in the protection scope of the utility model it It is interior.

Claims (7)

1. a kind of hydrogen chloride and methane chloride separator, including adsorption tower (1), it is characterised in that: the adsorption tower (1) Bottom end be equipped with solvent outlet (2), the adsorption tower (1) in the horizontal direction on side be equipped with methane chloride entrance (3) and chlorine Change hydrogen outlet (4), and methane chloride entrance (3), close to the bottom end of adsorption tower (1), the adsorption tower (1) is far from methane chlorination The side of object entrance (3) is welded with two fixing seats (5), and the bottom of a fixing seat (5) is fixedly installed with driving motor (6), the driving end of the driving motor (6) is fixedly connected with screw rod (7) through the one end of fixing seat (5), the screw rod (7) Outer surface is arranged with pedestal (8), and the top of the adsorption tower (1) is chimeric to be had top cover (9), the outer surface of cupular part of the top cover (9) Equipped with spray flow container (10), the internal vertical of the adsorption tower (1) is equipped with newel (11), the outer surface of the newel (11) Parallel sleeve is equipped with multiple combination tower trays (12), and the top of the top cover (9) is equipped with machine of uncapping close to the side of spray flow container (10) Structure (13).
2. a kind of hydrogen chloride according to claim 1 and methane chloride separator, it is characterised in that: the machine of uncapping Structure (13) include hydraulic cylinder (14), hydraulic stem (15), attachment base (16), curved bar (17), L shape bar (18), spring stack (19) and Stand (20), the hydraulic cylinder (14) are set to the outer surface of cupular part of pedestal (8), are fixedly connected at the top of the hydraulic cylinder (14) Have hydraulic stem (15), the outer surface of cupular part of the hydraulic stem (15) is rotatably connected to attachment base (16), the attachment base (16) Outer surface is welded with curved bar (17), and the side sidewall weld of the top cover (9) has L shape bar (18), the top of the L shape bar (18) Outer surface bolt is fixed with spring stack (19), and the outer surface of cupular part of the top cover (9) is welded with stand (20).
3. a kind of hydrogen chloride according to claim 1 and methane chloride separator, it is characterised in that: the combined column Disk (12) includes lantern ring (21), taper tower tray (22) and side plate (23), and the lantern ring (21) is set in the outer of newel (11) The lateral wall on surface, the lantern ring (21) is welded with taper tower tray (22), and the inner sidewall of the adsorption tower (1) is fitted with side plate (23)。
4. a kind of hydrogen chloride according to claim 2 and methane chloride separator, it is characterised in that: the L shape bar (18) vertically on right-angle side be fixedly connected with curved bar (17) by pin shaft, and L shape bar (18) passes through spring stack (19) It is fixedly connected with curved bar (17), the curved bar (17) is fixedly connected by pin shaft with stand (20) close to the one end of stand (20).
5. a kind of hydrogen chloride according to claim 1 and methane chloride separator, it is characterised in that: the screw rod (7) it is vertically installed between two fixing seats (5), the pedestal (8) is connected by screw rod (7) and driving motor (6) transmission It connects.
6. a kind of hydrogen chloride according to claim 1 and methane chloride separator, it is characterised in that: the top cover (9) close to adsorption tower (1), internal side side wall is provided with multiple spray heads, multiple sprays about newel (11) annular Head passes through separating tube through the one end of top cover (9) and is fixedly connected with spray flow container (10).
7. a kind of hydrogen chloride according to claim 3 and methane chloride separator, it is characterised in that: the lantern ring (21) lateral wall is symmetrically arranged with four taper tower trays (22) about newel (11), four taper tower trays (22) Outer surface is hollow out setting, and the inner sidewall distribution of the adsorption tower (1) is fitted with corresponding with four taper tower tray (22) Side plate (23), and taper tower tray (22) is equipped with corresponding convex architecture with the lateral wall of side plate (23).
CN201920107405.3U 2019-01-23 2019-01-23 A kind of hydrogen chloride and methane chloride separator Expired - Fee Related CN209596875U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920107405.3U CN209596875U (en) 2019-01-23 2019-01-23 A kind of hydrogen chloride and methane chloride separator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920107405.3U CN209596875U (en) 2019-01-23 2019-01-23 A kind of hydrogen chloride and methane chloride separator

Publications (1)

Publication Number Publication Date
CN209596875U true CN209596875U (en) 2019-11-08

Family

ID=68401643

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201920107405.3U Expired - Fee Related CN209596875U (en) 2019-01-23 2019-01-23 A kind of hydrogen chloride and methane chloride separator

Country Status (1)

Country Link
CN (1) CN209596875U (en)

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Granted publication date: 20191108