CN209451815U - A kind of reaction of drug precipitation and separator - Google Patents
A kind of reaction of drug precipitation and separator Download PDFInfo
- Publication number
- CN209451815U CN209451815U CN201822147350.7U CN201822147350U CN209451815U CN 209451815 U CN209451815 U CN 209451815U CN 201822147350 U CN201822147350 U CN 201822147350U CN 209451815 U CN209451815 U CN 209451815U
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- CN
- China
- Prior art keywords
- end outer
- condenser
- cabinet
- motor
- ultrasonic wave
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model discloses a kind of reaction of drug precipitation and separators, including reaction kettle cabinet, the upper end outer surface of the reaction kettle cabinet is fixedly installed with motor, the side of the motor is provided with feeding-in solid body mouth, the other side of the motor is provided with liquid inlet opening, the lower end outer surface of the motor is provided with stirring rod, the lower end outer surface of the stirring rod is provided with blade, one side external surface of the reaction kettle cabinet is provided with linker and condenser, the linker is located at the top of condenser, the condenser is internally provided with heated mechanism, condenser pipe and cooling mechanism.A kind of drug precipitation reaction described in the utility model and separator, equipped with ultrasonic wave cabinet, condenser, heater and sand core bottom, it can carry out ultrasound precipitation reaction and the lock out operation under room temperature and heating condition, it can be very good sufficiently to dissolve internal impurity, convenient for the use of people, better prospect of the application is brought.
Description
Technical field
The utility model relates to medical separation engineering device technique field, in particular to a kind of drug precipitation reaction and separation dress
It sets.
Background technique
Drug precipitation reaction and separator are a kind of precipitation reaction generated suitable for pharmaceutical synthesis, i.e., reaction product is not
Be dissolved in solvent, existing drug precipitation reaction and separator can not carry out under normal temperature conditions the precipitating of drug with separate,
It is secondary, internal impurity sufficiently can not be dissolved well, for this purpose, it is proposed that a kind of reaction of drug precipitation and separation dress
It sets.
Utility model content
The main purpose of the utility model is to provide a kind of reaction of drug precipitation and separators, can effectively solve to carry on the back
The problems in scape technology.
To achieve the above object, the technical solution that the utility model is taken are as follows:
A kind of reaction of drug precipitation and separator, including reaction kettle cabinet, the upper end outer surface of the reaction kettle cabinet
It is fixedly installed with motor, the side of the motor is provided with feeding-in solid body mouth, and the other side of the motor is provided with liquid feedstock
Mouthful, the lower end outer surface of the motor is provided with stirring rod, and the lower end outer surface of the stirring rod is provided with blade, the reaction
One side external surface of stilling box body is provided with linker and condenser, and the linker is located at the top of condenser, the condenser
Be internally provided with heated mechanism, condenser pipe and cooling mechanism, the heated mechanism is located at the side of condenser pipe, the heat dissipation machine
Structure is located at the other side of condenser pipe, and having heaters is fixedly mounted in the lower end outer surface of the reaction kettle cabinet, the heater
Side is provided with liquid material outlet, and the top of the liquid material outlet is provided with sand core bottom, and the inside of the heater is set
It is equipped with heated quarty tube, another side external surface of the reaction kettle cabinet is provided with ultrasonic wave cabinet and solid matter outlet, institute
The top that ultrasonic tank body is located at solid matter outlet is stated, the inside of the ultrasonic wave cabinet is fixedly installed with ultrasonic wave and machine occurs
Structure and central control machine structure, the side of the centrally located control mechanism of ultrasonic wave generating mechanism.
The material of its device linker is glass.
Preferably, one end outer surface of the heated mechanism connects by the way that one end outer surface of condenser pipe and cooling mechanism is fixed
Connect, a side external surface of the heated mechanism is fixedly connected with a side external surface of reaction kettle cabinet, the cooling mechanism it is interior
Portion is provided with heat dissipation leaf.
Preferably, what the liquid material exported is internally provided with rotary valve, the central control machine structure and rotary valve electricity
Property connection, be provided with temperature sensor between the motor and liquid inlet opening.
Preferably, the inside of the ultrasonic wave generating mechanism is fixedly installed with supersonic generator, the central control machine
The inside of structure is fixedly installed with central die, and the ultrasonic wave generating mechanism and central control machine structure are electrically connected.
Preferably, the lower end outer surface of the motor is fixedly connected by stirring rod with one end outer surface of blade, described
The quantity of blade is several groups.
Preferably, the back end outer surface of the reaction kettle cabinet is provided with power supply line, a side external surface of the motor with
One end of power supply line is fixedly connected, and the back end outer surface of the ultrasonic wave generating mechanism is fixedly connected with one end of power supply line, institute
The back end outer surface for stating heater is fixedly connected with one end of power supply line, and the one of the back end outer surface of the condenser and power supply line
End is fixedly connected.
Compared with prior art, the utility model has the following beneficial effects: a kind of drug precipitation reaction and separation dress
It sets, by the ultrasonic wave cabinet of setting, condenser, heater and sand core bottom, the ultrasound under room temperature and heating condition can be carried out
Precipitation reaction and lock out operation, reaction product precipitating can deposit on sand core, open liquid addition port and washing solution is added, start
Motor stirring can sufficiently dissolve the impurity in product, and entirely a kind of drug precipitation reaction and separator are simple, easy to operate,
The effect used is more preferable relative to traditional approach.
Detailed description of the invention
Fig. 1 is the overall structure figure of a kind of drug precipitation reaction of the utility model and separator.
Fig. 2 is the schematic diagram of internal structure of a kind of drug precipitation reaction of the utility model and separator condenser 5.
Fig. 3 is the schematic diagram of internal structure of a kind of drug precipitation reaction of the utility model and separator heater 6.
Fig. 4 is the schematic diagram of internal structure of a kind of drug precipitation reaction of the utility model and separator ultrasonic wave cabinet 9.
In figure: 1, feeding-in solid body mouth；2, reaction kettle cabinet；3, linker；4, stirring rod；5, condenser；6, heater；7,
Motor；8, liquid inlet opening；9, ultrasonic wave cabinet；10, solid matter outlet；11, blade；12, sand core bottom；13, liquid material
Outlet；14, condenser pipe；15, heated mechanism；16, cooling mechanism；17, heated quarty tube；18, ultrasonic wave generating mechanism；19, in
Entreat control mechanism.
Specific embodiment
To be easy to understand the technical means, creative features, achievement of purpose, and effectiveness of the utility model, below
In conjunction with specific embodiment, the utility model is further described.
As shown in Figs 1-4, a kind of drug precipitation reaction and separator, including reaction kettle cabinet 2, reaction kettle cabinet 2
Upper end outer surface is fixedly installed with motor 7, and the side of motor 7 is provided with feeding-in solid body mouth 1, and the other side of motor 7 is provided with liquid
Body feed inlet 8, the lower end outer surface of motor 7 are provided with stirring rod 4, and the lower end outer surface of stirring rod 4 is provided with blade 11, reaction
One side external surface of stilling box body 2 is provided with linker 3 and condenser 5, and linker 3 is located at the top of condenser 5, condenser 5
It is internally provided with heated mechanism 15, condenser pipe 14 and cooling mechanism 16, heated mechanism 15 is located at the side of condenser pipe 14, and radiate machine
Structure 16 is located at the other side of condenser pipe 14, and the lower end outer surface of reaction kettle cabinet 2 is fixedly mounted having heaters 6, and the one of heater 6
Side is provided with liquid material outlet 13, and the top of liquid material outlet 13 is provided with sand core bottom 12, and heater 6 is internally provided with
Heated quarty tube 17, another side external surface of reaction kettle cabinet 2 are provided with ultrasonic wave cabinet 9 and solid matter outlet 10, ultrasound
Wave cabinet 9 is located at the top of solid matter outlet 10, the inside of ultrasonic wave cabinet 9 be fixedly installed with ultrasonic wave generating mechanism 18 with
Central control machine structure 19, the side of the centrally located control mechanism 19 of ultrasonic wave generating mechanism 18.
One end outer surface of heated mechanism 15 is fixedly connected by condenser pipe 14 with one end outer surface of cooling mechanism 16, by
One side external surface of heat engine structure 15 is fixedly connected with a side external surface of reaction kettle cabinet 2, and cooling mechanism 16 is internally provided with
Radiate leaf, is conducive to condenser 5 and plays heat spreading function；Liquid material outlet 13 is internally provided with rotary valve, central control machine structure
19 are electrically connected with rotary valve, temperature sensor are provided between motor 7 and liquid inlet opening 8, convenient for the operation of single unit system；
The inside of ultrasonic wave generating mechanism 18 is fixedly installed with supersonic generator, during the inside of central control machine structure 19 is fixedly installed with
Chip is entreated, ultrasonic wave generating mechanism 18 and central control machine structure 19 are electrically connected, run convenient for ultrasonic wave cabinet 9；Under motor 7
End outer surface is fixedly connected by stirring rod 4 with one end outer surface of blade 11, and the quantity of blade 11 is several groups, convenient for completing
This whipping process；The back end outer surface of reaction kettle cabinet 2 is provided with power supply line, a side external surface of motor 7 and power supply line
One end is fixedly connected, and the back end outer surface of ultrasonic wave generating mechanism 18 is fixedly connected with one end of power supply line, the rear end of heater 6
Outer surface is fixedly connected with one end of power supply line, and the back end outer surface of condenser 5 is fixedly connected with one end of power supply line, is entire
Device provides electric energy.
It should be noted that the utility model reacts for a kind of drug precipitation and separator, when in use, when in use
Rotation threshold switch, solid matter outlet 10 and feeding-in solid body mouth 1, liquid inlet opening 8, fit on temperature sensor is first closed to beat
It opens liquid inlet opening 8 and liquid solvent is added, be then turned off liquid inlet opening 8 and open feeding-in solid body mouth 1, various solid reactions are added
Object starts the stirring of motor 7 to being completely dissolved, obtains homogeneous reaction system, reflux condenser band is matched on feeding-in solid body mouth 1
Suck-back device, control to certain reaction condition for example heat or open ultrasonic wave, and precipitating completely, will after complete reaction
Reflux condenser is removed, and electric stirring is closed, and liquid material outlet 13 is connected with the liquid holding device with decompression, opens rotation
Threshold switch simultaneously opens relief cock in liquid holding device, since the reaction solution in pressure official post reaction kettle enters by the filtering of sand core bottom 12
Until not having liquid solvent outflow to close rotation threshold switch in liquid holding device, reaction product precipitating can be deposited on sand core bottom 12, be beaten
It opens liquid inlet opening 8 and washing solution is added, start the stirring of motor 7 until the impurity in product after completely dissolution, is closed motor 7
Stirring opens rotation threshold switch and opens relief cock in liquid holding device, filters out cleaning solution again until liquid outlet no liquid stream
After out, product can be taken out by opening solid matter outlet 10, more practical.
The basic principles and main features of the present invention and the advantages of the present invention have been shown and described above.Current row
The technical staff of industry is described in above embodiments and description it should be appreciated that the present utility model is not limited to the above embodiments
Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also
It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.The utility model
Claimed range is defined by the appending claims and its equivalent thereof.
Claims (6)
1. a kind of drug precipitation reaction and separator, including reaction kettle cabinet (2), it is characterised in that: the reaction kettle cabinet
(2) upper end outer surface is fixedly installed with motor (7), and the side of the motor (7) is provided with feeding-in solid body mouth (1), the electricity
The other side of machine (7) is provided with liquid inlet opening (8), and the lower end outer surface of the motor (7) is provided with stirring rod (4), described
The lower end outer surface of stirring rod (4) is provided with blade (11), and a side external surface of the reaction kettle cabinet (2) is provided with linker
(3) and condenser (5), the linker (3) are located at the top of condenser (5), and being internally provided with for the condenser (5) is heated
Mechanism (15), condenser pipe (14) and cooling mechanism (16), the heated mechanism (15) is located at the side of condenser pipe (14), described scattered
Heat engine structure (16) is located at the other side of condenser pipe (14), and the lower end outer surface of the reaction kettle cabinet (2) is fixedly installed with heating
Device (6), the side of the heater (6) are provided with liquid material outlet (13), set above the liquid material outlet (13)
Be equipped with sand core bottom (12), the heater (6) is internally provided with heated quarty tube (17), the reaction kettle cabinet (2) it is another
One side external surface is provided with ultrasonic wave cabinet (9) and solid matter outlet (10), and the ultrasonic wave cabinet (9) is located at solid material
The top of (10) is exported, the inside of the ultrasonic wave cabinet (9) is fixedly installed with ultrasonic wave generating mechanism (18) and center controls
Mechanism (19), the side of the centrally located control mechanism of the ultrasonic wave generating mechanism (18) (19).
2. a kind of drug precipitation reaction according to claim 1 and separator, it is characterised in that: the heated mechanism
(15) one end outer surface is fixedly connected by condenser pipe (14) with one end outer surface of cooling mechanism (16), the heated mechanism
(15) a side external surface is fixedly connected with a side external surface of reaction kettle cabinet (2), and the inside of the cooling mechanism (16) is set
It is equipped with heat dissipation leaf.
3. a kind of drug precipitation reaction according to claim 1 and separator, it is characterised in that: the liquid material goes out
Mouth (13) is internally provided with rotary valve, and the central control machine structure (19) and rotary valve are electrically connected, the motor (7) and liquid
Body feed inlet is provided with temperature sensor between (8).
4. a kind of drug precipitation reaction according to claim 1 and separator, it is characterised in that: the ultrasonic wave occurs
The inside of mechanism (18) is fixedly installed with supersonic generator, and the inside of the central control machine structure (19) is fixedly installed with center
Chip, the ultrasonic wave generating mechanism (18) and central control machine structure (19) are electrically connected.
5. a kind of drug precipitation reaction according to claim 1 and separator, it is characterised in that: the motor (7)
Lower end outer surface is fixedly connected by stirring rod (4) with one end outer surface of blade (11), the blade (11) if quantity be
Dry group.
6. a kind of drug precipitation reaction according to claim 1 and separator, it is characterised in that: the reaction kettle cabinet
(2) back end outer surface is provided with power supply line, and a side external surface of the motor (7) is fixedly connected with one end of power supply line, institute
The back end outer surface for stating ultrasonic wave generating mechanism (18) is fixedly connected with one end of power supply line, outside the rear end of the heater (6)
Surface is fixedly connected with one end of power supply line, and the back end outer surface of the condenser (5) is fixedly connected with one end of power supply line.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822147350.7U CN209451815U (en) | 2018-12-20 | 2018-12-20 | A kind of reaction of drug precipitation and separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822147350.7U CN209451815U (en) | 2018-12-20 | 2018-12-20 | A kind of reaction of drug precipitation and separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209451815U true CN209451815U (en) | 2019-10-01 |
Family
ID=68041540
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822147350.7U Expired - Fee Related CN209451815U (en) | 2018-12-20 | 2018-12-20 | A kind of reaction of drug precipitation and separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209451815U (en) |
-
2018
- 2018-12-20 CN CN201822147350.7U patent/CN209451815U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191001 Termination date: 20201220 |