CN209392761U - A kind of uniform DMSO distillation still of charging - Google Patents
A kind of uniform DMSO distillation still of charging Download PDFInfo
- Publication number
- CN209392761U CN209392761U CN201920033580.2U CN201920033580U CN209392761U CN 209392761 U CN209392761 U CN 209392761U CN 201920033580 U CN201920033580 U CN 201920033580U CN 209392761 U CN209392761 U CN 209392761U
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- China
- Prior art keywords
- fixedly connected
- distillation still
- main body
- uniform
- dmso
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000004821 distillation Methods 0.000 title claims abstract description 90
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 title claims abstract description 87
- 238000003756 stirring Methods 0.000 claims abstract description 29
- 238000005485 electric heating Methods 0.000 claims abstract description 12
- 238000001704 evaporation Methods 0.000 claims description 3
- 238000010025 steaming Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 10
- 238000010438 heat treatment Methods 0.000 abstract description 8
- 239000000126 substance Substances 0.000 description 8
- 238000007789 sealing Methods 0.000 description 5
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Abstract
The utility model discloses a kind of uniform DMSO distillation stills of charging, it is related to distillation still technical field, specially a kind of uniform DMSO distillation still of charging, including distillation still main body and support plate, fixed cylinder is fixedly connected at the top of the distillation still main body, the inner wall of the fixed cylinder is fixedly connected with first bearing, and the side of the fixed cylinder is fixedly connected with fixing axle, is fixedly connected with motor at the top of the fixing axle.The uniform DMSO distillation still of the charging, by starting motor, motor is set to drive rotating bar, so that motor drives stirring horizontal axis, stirring cambered axle and screw rod rotation, and screw rod is made to drive flight rotation, while charging, or, while heating distillation, the uniform DMSO distillation still of the charging is made to play the role of stirring evenly, achievees the effect that distillation is abundant, pass through the setting of electric heating cover, by starting electric heating cover, make being internally heated for distillation still main body, so that the uniform DMSO distillation still effect easy to use of the charging.
Description
Technical field
The utility model relates to distillation still technical field, specially a kind of uniform DMSO distillation still of charging.
Background technique
The relationship of the mankind and chemical industry is very close, spreads to the every aspect of life.In the modern life, almost at any time with
Ground all be unable to do without chemical products, from material lifes such as clothing, food, shelter and rows to the cultural lives such as culture and arts, amusement, requiring
Chemical product services for it.Some chemical products play epoch-making important function in human development history.Their production and
Using, or even certain historical stage of human civilization is represent, and high temperature distillation is frequently necessary in Chemical Manufacture to extract
The substance needed, existing chemical industry pass through electric heater with high temperature distillation kettle mostly and directly carry out heating distillation to industrial chemicals,
Make distillation efficiency lower in this way, for this purpose, it is proposed that a kind of chemical industry high temperature distillation kettle.Currently, a kind of existing charging is equal
That there are uneven heatings is even for even DMSO distillation still, while charging, alternatively, stirring is uneven while heating distillation, it is difficult
To achieve the purpose that distillation is abundant.
Utility model content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the utility model provides a kind of uniform DMSO distillation still of charging, solves
State the problem of proposing in background technique.
(2) technical solution
In order to achieve the above object, the utility model is achieved by the following technical programs: a kind of uniform DMSO of charging
Distillation still, including distillation still main body and support plate are fixedly connected with fixed cylinder, the fixed cylinder at the top of the distillation still main body
Inner wall be fixedly connected with first bearing, the side of the fixed cylinder is fixedly connected with fixing axle, and the top of the fixing axle is solid
Surely it is connected with motor, the output end of the motor is fixedly connected with rotating bar, and the outer surface of the rotating bar is from top to bottom successively
It is fixedly connected with stirring horizontal axis, stirring cambered axle and screw rod, the outer surface of the screw rod and is fixedly connected with flight, the steaming
The inner bottom wall for evaporating kettle main body is fixedly connected with support frame, and second bearing, the distillation are fixedly connected at the top of support frame as described above
The inner wall of kettle main body is fixedly connected with electric heating cover, and the bottom of the distillation still main body is fixedly connected with discharge port, the discharging
The side of mouth is provided with valve, and the side of the distillation still body top is fixedly connected with feeding inlet, the top of the feeding inlet
It is threaded with sealing cover, the other side of the distillation still body top is provided with air gauge.
Optionally, the escape pipe being fixedly connected at the top of the distillation still body side, the distillation still main body are another
Condensation tracheae is fixedly connected at the top of side.
Optionally, the upper surface of the support plate is overlapped with supporting block, and the side of the supporting block is fixedly connected on distillation
The side of kettle main body.
Optionally, the upper surface of the support plate is fixedly connected with controllable exhaust fan close to the side of supporting block.
Optionally, the four corners of the support plate lower surface are fixedly connected to support column, and the quantity of the support column is
Four, four support columns are fixedly connected on the lower surface of support plate in the form of rectangular array.
Optionally, the quantity of the supporting block is four, and four supporting blocks are fixedly connected in the form of annular array
In the side of distillation still main body.
(3) beneficial effect
The utility model provides a kind of uniform DMSO distillation still of charging, has following the utility model has the advantages that the charging is uniform
DMSO distillation still, by motor, rotating bar, stirring horizontal axis, stir cambered axle and screw rod setting, by start motor, make
Motor drives rotating bar, so that motor drives stirring horizontal axis, stirring cambered axle and screw rod rotation, and screw rod is made to drive spiral
Piece rotation, while charging, alternatively, making the uniform DMSO distillation still of the charging play stirring equal while heating distillation
Even effect achievees the effect that distillation is abundant, makes distillation still main body by starting electric heating cover by the setting of electric heating cover
Be internally heated so that the uniform DMSO distillation still effect easy to use of the charging.
Detailed description of the invention
Fig. 1 is the utility model schematic cross-sectional view;
Fig. 2 is the utility model positive structure diagram.
In figure: 1- distillation still main body, 2- fixed cylinder, 3- first bearing, 4- fixing axle, 5- motor, 6- rotating bar, 7- support
Plate, 8- stirring horizontal axis, 9- stir cambered axle, 10- screw rod, 11- flight, 12- support frame, 13- second bearing, 14- electric heating
Set, 15- discharge port, 16- valve, 17- feeding inlet, 18- sealing cover, 19- air gauge, 20- escape pipe, 21- condense tracheae, 22-
The controllable exhaust fan of supporting block, 23-, 24- support column.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.
Fig. 1 to Fig. 2 is please referred to, the utility model provides a kind of technical solution: a kind of uniform DMSO distillation still of charging, packet
Distillation still main body 1 and support plate 7 are included, the top of distillation still main body 1 is fixedly connected with fixed cylinder 2, and the inner wall of fixed cylinder 2 is fixed to be connected
It is connected to first bearing 3, by the setting of first bearing 3, plays the role of fixed rotating bar 6, the side of fixed cylinder 2 is fixedly connected
There is fixing axle 4, the top of fixing axle 4 is fixedly connected with motor 5, and the output end of motor 5 is fixedly connected with rotating bar 6, rotating bar 6
Outer surface be fixedly connected sequentially have stirring horizontal axis 8, stirring cambered axle 9 and screw rod 10, the outer surface of screw rod 10 from top to bottom
It is fixedly connected with flight 11, by motor 5, rotating bar 6, stirring horizontal axis 8, the setting for stirring cambered axle 9 and screw rod 10, is passed through
Start motor 5, motor 5 is made to drive rotating bar 6, so that motor 5 drives stirring horizontal axis 8, stirring cambered axle 9 and screw rod 10 to rotate,
And make screw rod 10 that flight 11 be driven to rotate, while charging, alternatively, keeping the charging equal while heating distillation
Even DMSO distillation still plays the role of stirring evenly, and achievees the effect that distillation is abundant, and the inner bottom wall of distillation still main body 1 is fixed to be connected
It is connected to support frame 12, by the setting of support frame 12, plays the role of fixed second bearing 13, the top of support frame 12 is fixed to be connected
It is connected to second bearing 13, by the setting of second bearing 13, plays the role of fixed rotating bar 6, the inner wall of distillation still main body 1 is solid
Surely it is connected with electric heating cover 14, the inside of distillation still main body is made by starting electric heating cover 14 by the setting of electric heating cover 14
It is heated, so that the uniform DMSO distillation still effect easy to use of the charging, the bottom of distillation still main body 1 is fixed to be connected
It is connected to discharge port 15, the side of discharge port 15 is provided with valve 16, by the setting of valve 16, when valve 16 is opened, so that
Material inside distillation still main body 1 flows out, so that the charging is uniform under gravity from the inside of distillation still main body 1
DMSO distillation still reaches effect easy to use, and the side at 1 top of distillation still main body is fixedly connected with feeding inlet 17, feeding inlet 17
Top be threaded with sealing cover 18, by the setting of sealing cover 18, sealing cover 18 is carried out feeding inlet 17 close
Envelope, and then the uniform DMSO distillation still working efficiency of the charging is improved, the other side at 1 top of distillation still main body is provided with air pressure
Table 19, due to while heating, making the inside of distillation still main body 1 generate heat, at this moment, is steamed by the setting of air gauge 19
Evaporating the pressure inside kettle main body 1 will will increase, can be according to the numerical values recited of air gauge 19, and then to judge distillation still main body 1
Internal air pressure change, the escape pipe 20 being fixedly connected at the top of 1 side of distillation still main body, by the setting of escape pipe 20,
When air pressure inside distillation still main body 1 is excessive, the gas inside distillation still main body 1 can be extracted out by controllable exhaust fan,
Safety accident is avoided, condensation tracheae 21 is fixedly connected at the top of 1 other side of distillation still main body, passes through condensation tracheae 21
Setting so that condensation tracheae 21 is connected with condensing plant, and carries out distillation processing, and the upper surface of support plate 7 is overlapped with supporting block
22, by the setting of supporting block 22, play the role of supporting distillation still main body 1, the quantity of supporting block 22 is four, four supports
Block 22 is fixedly connected on the side of distillation still main body 1 in the form of annular array, and the side of supporting block 22 is fixedly connected on distillation
The upper surface of the side of kettle main body 1, support plate 7 is fixedly connected with controllable exhaust fan 23, support plate 7 close to the side of supporting block 22
The four corners of lower surface are fixedly connected to support column 24, and the quantity of support column 24 is four, and four support columns 24 are with rectangle battle array
The form of column is fixedly connected on the lower surface of support plate 7, main controller and 220V of the electric elements occurred in this article with the external world
Alternating current electrical connection, and main controller can play the conventionally known equipment of control for computer etc..
A kind of optimal technical scheme as the utility model: the quantity of stirring cambered axle 9 is three, three stirring cambered axles 9
The side of rotating bar 6 is fixedly connected in the form of annular array.
In conclusion the uniform DMSO distillation still of the charging, in use, by motor 5, rotating bar 6, stirring horizontal axis 8, stirring
The setting for mixing cambered axle 9 and screw rod 10 makes motor 5 drive rotating bar 6, so that motor 5 drives stirring horizontal by starting motor 5
Axis 8, stirring cambered axle 9 and screw rod 10 rotate, and make screw rod 10 that flight 11 be driven to rotate, while charging, alternatively,
While heating distillation, the uniform DMSO distillation still of the charging is made to play the role of stirring evenly, reaches and distill abundant effect
Fruit makes being internally heated for distillation still main body, to make by starting electric heating cover 14 by the setting of electric heating cover 14
Obtain the uniform DMSO distillation still effect easy to use of the charging.
The preferable specific embodiment of the above, only the utility model, but the protection scope of the utility model is not
It is confined to this, anyone skilled in the art is within the technical scope disclosed by the utility model, practical according to this
Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model
Within enclosing.
Claims (6)
1. a kind of uniform DMSO distillation still of charging, including distillation still main body (1) and support plate (7), it is characterised in that: the steaming
It evaporates and is fixedly connected at the top of kettle main body (1) fixed cylinder (2), the inner wall of the fixed cylinder (2) is fixedly connected with first bearing
(3), the side of the fixed cylinder (2) is fixedly connected with fixing axle (4), is fixedly connected with motor at the top of the fixing axle (4)
(5), the output end of the motor (5) is fixedly connected with rotating bar (6), and the outer surface of the rotating bar (6) is from top to bottom successively
Stirring horizontal axis (8), stirring cambered axle (9) and screw rod (10), the outer surface of the screw rod (10) is fixedly connected with to be fixedly connected
Have flight (11), the inner bottom wall of the distillation still main body (1) is fixedly connected with support frame (12), the top of support frame as described above (12)
Portion is fixedly connected with second bearing (13), and the inner wall of the distillation still main body (1) is fixedly connected with electric heating cover (14), the steaming
The bottom for evaporating kettle main body (1) is fixedly connected with discharge port (15), and the side of the discharge port (15) is provided with valve (16), described
Side at the top of distillation still main body (1) is fixedly connected with feeding inlet (17), is threaded with above the feeding inlet (17) close
It covers (18), the other side at the top of the distillation still main body (1) is provided with air gauge (19).
2. a kind of uniform DMSO distillation still of charging according to claim 1, it is characterised in that: the distillation still main body
(1) escape pipe (20) being fixedly connected at the top of side is fixedly connected at the top of distillation still main body (1) other side cold
Solidifying tracheae (21).
3. a kind of uniform DMSO distillation still of charging according to claim 1, it is characterised in that: the support plate (7)
Upper surface is overlapped with supporting block (22), and the side of the supporting block (22) is fixedly connected on the side of distillation still main body (1).
4. a kind of uniform DMSO distillation still of charging according to claim 3, it is characterised in that: the support plate (7)
Upper surface is fixedly connected with controllable exhaust fan (23) close to the side of supporting block (22).
5. a kind of uniform DMSO distillation still of charging according to claim 1, it is characterised in that: under the support plate (7)
The four corners on surface are fixedly connected to support column (24), and the quantity of the support column (24) is four, four support columns
(24) lower surface of support plate (7) is fixedly connected in the form of rectangular array.
6. a kind of uniform DMSO distillation still of charging according to claim 3, it is characterised in that: the supporting block (22)
Quantity is four, and four supporting blocks (22) are fixedly connected on the side of distillation still main body (1) in the form of annular array.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201920033580.2U CN209392761U (en) | 2019-01-09 | 2019-01-09 | A kind of uniform DMSO distillation still of charging |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201920033580.2U CN209392761U (en) | 2019-01-09 | 2019-01-09 | A kind of uniform DMSO distillation still of charging |
Publications (1)
Publication Number | Publication Date |
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CN209392761U true CN209392761U (en) | 2019-09-17 |
Family
ID=67897987
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Application Number | Title | Priority Date | Filing Date |
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CN201920033580.2U Expired - Fee Related CN209392761U (en) | 2019-01-09 | 2019-01-09 | A kind of uniform DMSO distillation still of charging |
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CN (1) | CN209392761U (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115581934A (en) * | 2022-10-08 | 2023-01-10 | 山东信谊制药有限公司 | Separation and purification device for drug synthesis |
-
2019
- 2019-01-09 CN CN201920033580.2U patent/CN209392761U/en not_active Expired - Fee Related
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115581934A (en) * | 2022-10-08 | 2023-01-10 | 山东信谊制药有限公司 | Separation and purification device for drug synthesis |
CN115581934B (en) * | 2022-10-08 | 2023-06-16 | 山东信谊制药有限公司 | Separation and purification device for drug synthesis |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190917 |