CN209348633U - A kind of ionic liquid preparation biodiesel reactor - Google Patents

A kind of ionic liquid preparation biodiesel reactor Download PDF

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Publication number
CN209348633U
CN209348633U CN201822123472.2U CN201822123472U CN209348633U CN 209348633 U CN209348633 U CN 209348633U CN 201822123472 U CN201822123472 U CN 201822123472U CN 209348633 U CN209348633 U CN 209348633U
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China
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ionic liquid
disk
inner cylinder
outer cylinder
biodiesel
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CN201822123472.2U
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Chinese (zh)
Inventor
王昌梅
赵振兴
张无敌
尹芳
刘士清
赵兴玲
吴凯
柳静
杨红
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Yunnan University YNU
Yunnan Normal University
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Yunnan Normal University
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Abstract

A kind of ionic liquid preparation biodiesel reactor, it is related to biodiesel production facility technical field;Outer cylinder is set in the outside of inner cylinder, and magnetic stirring apparatus is equipped on inner cylinder, and stirring motor and magnetic stirring apparatus are drivingly connected;The side wall of the inner cylinder is equipped with steam pipe coil and cooling water coil;The bottom of the inner cylinder is provided with discharge port, discharge port is located in outer cylinder, and the disk of several layers of cone cell is fixed in outer cylinder, is provided with demarcation plate above several layers of disk, tap hole is provided on every layer of disk, the bottom of every layer of disk is respectively arranged with ionic liquid outlet;The top of the demarcation plate is ionic liquid collecting chamber, and biodiesel collecting chamber is communicated with several layers of disk;It separates motor and outer cylinder is drivingly connected.A kind of ionic liquid described in the utility model prepares biodiesel reactor, and using static seal, good airproof performance No leakage can carry out the reclaimer operation of ionic liquid immediately out after liquid, reclaimer operation is easy.

Description

A kind of ionic liquid preparation biodiesel reactor
Technical field
The utility model relates to biodiesel production facility technical fields, and in particular to a kind of biological bavin of ionic liquid preparation Oil reactor.
Background technique
Biodiesel is also known as biomass fuel, and main component is fatty acid methyl ester or fatty-acid ethyl ester.It is to use animal and plant The waste greases such as object grease, microalgae grease and gutter oil have ring by one kind that esterification or ester exchange reaction prepare It protects, the biomass fuel of regenerative nature.This bio-fuel can be used as diesel oil.
Biodiesel has that excellent environmental protection characteristic, low-temperature startup performance, the greasy property of biodiesel be better than diesel oil, tool There is good security performance, the excellent performance of biodiesel makes not only full using the engine exhaust emission index of biodiesel The current European II standard of foot, or even meeting will be in the discharge standard of stringenter Europe III of Europe issuing and implementation.And And when as biodiesel burning the carbon dioxide that discharges far below carbon dioxide absorbed in the growing process, thus Improve due to carbon dioxide discharge caused by global warming this be harmful to the great environmental problem of the mankind.Thus biological bavin Oil is a kind of real green diesel.
The biodiesel preparation of this patent introduction uses ionic liquid as catalyst, using autoclave certain Reaction, vacuum distillation obtain biodiesel oil product under the conditions of temperature and time, and ionic liquid can continue to serve as being esterified after the drying Reaction or transesterification catalyst, catalyst is recycled, existing autoclave be easy leakage, need in addition into The reclaimer operation of row ionic liquid is not easy to the separation and recovery of ionic liquid.
Utility model content
The purpose of this utility model is that in view of the drawbacks of the prior art and insufficient, provide that a kind of structure is simple, design is closed Reason, ionic liquid easy to use prepare biodiesel reactor.
In order to achieve the above purposes, the technical solution adopted by the utility model is: it include outer cylinder, inner cylinder, magnetic stirring apparatus, Stirring motor, steam pipe coil, cooling water coil, discharge port, disk, tap hole, demarcation plate, ionic liquid outlet, ionic liquid Collecting chamber, biodiesel collecting chamber, separation motor;The outer cylinder is set in the outside of inner cylinder, is equipped with magnetic force on inner cylinder and stirs Device is mixed, stirring motor and magnetic stirring apparatus are drivingly connected;The side wall of the inner cylinder is equipped with steam pipe coil and cooling water coil; The bottom of the inner cylinder is provided with discharge port, and discharge port is located in outer cylinder, is fixed with the disk of several layers of cone cell in outer cylinder, and several layers It is provided with demarcation plate above disk, tap hole is provided on every layer of disk, the bottom of every layer of disk is respectively arranged with ion Liquid outlet;The top of the demarcation plate is ionic liquid collecting chamber, and biodiesel collecting chamber is communicated with several layers of disk;It is described Separation motor and outer cylinder be drivingly connected.
Preferably, being equipped with stirrer paddle on the agitating shaft of the magnetic stirring apparatus.
Preferably, the upper end of the inner cylinder is provided with feed inlet.
Preferably, the outer cylinder is connect by idler wheel and slideway with bracket slideway.
Preferably, the upper end of the inner cylinder is additionally provided with manhole.
Preferably, the steam pipe coil is located at the outside of cooling water coil.
The working principle of the utility model are as follows: the inner cylinder of sealing forms static seal chamber, is completely in reaction medium quiet close In envelope state, no any leakage, pollution and Personal Risk, stirring motor drive magnetic stirring apparatus, carry out high temperature by strong magnetic force High-pressure stirring reaction disconnects the steam pipework, cooling water pipeline and power supply of inner cylinder after reaction, opens discharge port, ion Liquid and the mixed liquor of biodiesel enter outer cylinder, connect separation motor, and separation motor drives outer cylinder revolution at a high speed, mixture Liquid is flowed upwards out through the tap hole on disk, and under effect of centrifugal force, heavier ionic liquid is exported by ionic liquid and is discharged One end through demarcation plate enters the collection of ionic liquid collecting chamber, and lighter biodiesel is expelled to biology along the disk of cone cell upwards Diesel oil collecting chamber, to have the function that separating ionic liquid.
After adopting the above structure, the utility model is the beneficial effects are as follows: a kind of ionic liquid described in the utility model Body prepares biodiesel reactor, and using static seal, good airproof performance No leakage can carry out the recycling of ionic liquid immediately out after liquid Operation, reclaimer operation is easy, and the utility model has many advantages, such as that structure is simple, setting is reasonable, low manufacture cost.
Detailed description of the invention
Fig. 1 is the structure chart of the utility model;
Fig. 2 is the scheme of installation of the utility model disk;
Fig. 3 is the top view of Fig. 2.
Description of symbols:
Outer cylinder 1, inner cylinder 2, magnetic stirring apparatus 3, stirring motor 4, steam pipe coil 5, cooling water coil 6, discharge port 7, disk 8, tap hole 9, demarcation plate 10, ionic liquid outlet 11, ionic liquid collecting chamber 12, biodiesel collecting chamber 13, separation motor 14, stirrer paddle 15, feed inlet 16, bracket 17, idler wheel 18, manhole 19.
Specific embodiment
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property It puts, is also possible to obtain other drawings based on these drawings.
Referring to such as Fig. 1 --- shown in Fig. 3, present embodiment adopts the following technical scheme that it includes outer cylinder 1, inner cylinder 2, magnetic stirring apparatus 3, stirring motor 4, steam pipe coil 5, cooling water coil 6, discharge port 7, disk 8, tap hole 9, demarcation plate 10, Ionic liquid outlet 11, ionic liquid collecting chamber 12, biodiesel collecting chamber 13, separation motor 14;The outer cylinder 1 is set in The outside of inner cylinder 2, the upper end of inner cylinder 2 are provided with feed inlet 16, and magnetic stirring apparatus 3, stirring motor 4 and magnetic are equipped on inner cylinder 2 Power blender 3 is drivingly connected;Stirrer paddle 15, the formation of inner cylinder 2 of sealing are installed on the agitating shaft of the magnetic stirring apparatus 3 Static seal chamber is completely in reaction medium in static seal state, no any leakage, pollution and Personal Risk, 4 band of stirring motor Dynamic magnetic stirring apparatus 3 drives stirrer paddle 15 to carry out high temperature and pressure and is stirred to react by strong magnetic force.
The side wall of the inner cylinder 2 is equipped with the cooling water coil 6 and steam pipe coil 5 being arranged inside and outside, and is passed through steam or cold But water is heated or is cooled down to the stoste of reaction;The bottom of the inner cylinder 2 is provided with discharge port 7, and discharge port 7 is located at outer cylinder In 1, it is fixed with the disk 8 of several layers of cone cell in outer cylinder 1, the top of several layers of disk 8 is provided with demarcation plate 10, on every layer of disk 8 It is provided with tap hole 9, the bottom of every layer of disk 8 is respectively arranged with ionic liquid outlet 11;The top of the demarcation plate 10 is Ionic liquid collecting chamber 12, biodiesel collecting chamber 13 are communicated with several layers of disk 8;The separation motor 14 and outer cylinder 1 drives Connection, after reaction, disconnects the steam pipework, cooling water pipeline and power supply of inner cylinder, to avoid pipeline and circuit to outer cylinder The mixed liquor of the influence of rotation, opening discharge port 7, ionic liquid and biodiesel enters outer cylinder 1, connects separation motor 14, It separates motor 14 and drives 1 revolution at a high speed of outer cylinder, mixed liquor is flowed upwards out through the tap hole on disk 8, in effect of centrifugal force Under, heavier ionic liquid enters ionic liquid collecting chamber 12 by 11 one end of discharge through demarcation plate 10 of ionic liquid outlet and receives Collection, lighter biodiesel is expelled to biodiesel collecting chamber 13 along the disk 8 of cone cell upwards, to reach separating ionic liquid Effect.
The outer cylinder 1 is connect by idler wheel 18 and slideway with 17 slideway of bracket, the stabilization highly rotated in favor of outer cylinder 1 Property.
The upper end of the inner cylinder 2 is additionally provided with manhole 19, easy access.
After adopting the above structure, present embodiment is the beneficial effects are as follows: one described in present embodiment Kind ionic liquid prepares biodiesel reactor, and using static seal, good airproof performance No leakage can carry out ionic liquid immediately out after liquid The reclaimer operation of body, reclaimer operation are easy, present embodiment have structure is simple, setting rationally, cost of manufacture it is low etc. excellent Point.
The advantages of basic principles and main features and the utility model of the utility model have been shown and described above.This The technical staff of industry is retouched in above embodiments and description it should be appreciated that the present utility model is not limited to the above embodiments That states only illustrates the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model It will also have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.This is practical new Type is claimed range and is defined by the appending claims and its equivalent thereof.

Claims (6)

1. a kind of ionic liquid prepares biodiesel reactor, it is characterised in that: it includes outer cylinder, inner cylinder, magnetic stirring apparatus, stirs Mix motor, steam pipe coil, cooling water coil, discharge port, disk, tap hole, demarcation plate, ionic liquid outlet, ionic liquid receipts Collect room, biodiesel collecting chamber, separation motor;The outer cylinder is set in the outside of inner cylinder, is equipped with magnetic agitation on inner cylinder Device, stirring motor and magnetic stirring apparatus are drivingly connected;The side wall of the inner cylinder is equipped with steam pipe coil and cooling water coil;Institute The bottom for the inner cylinder stated is provided with discharge port, and discharge port is located in outer cylinder, and the disk of several layers of cone cell, several layers of dish are fixed in outer cylinder It is provided with demarcation plate above piece, tap hole is provided on every layer of disk, the bottom of every layer of disk is respectively arranged with ionic liquid Body outlet;The top of the demarcation plate is ionic liquid collecting chamber, and biodiesel collecting chamber is communicated with several layers of disk;Described It separates motor and outer cylinder is drivingly connected.
2. a kind of ionic liquid according to claim 1 prepares biodiesel reactor, it is characterised in that: the magnetic force Stirrer paddle is installed on the agitating shaft of blender.
3. a kind of ionic liquid according to claim 1 prepares biodiesel reactor, it is characterised in that: the inner cylinder Upper end be provided with feed inlet.
4. a kind of ionic liquid according to claim 1 prepares biodiesel reactor, it is characterised in that: the outer cylinder It is connect by idler wheel and slideway with bracket slideway.
5. a kind of ionic liquid according to claim 1 prepares biodiesel reactor, it is characterised in that: the inner cylinder Upper end be additionally provided with manhole.
6. a kind of ionic liquid according to claim 1 prepares biodiesel reactor, it is characterised in that: the steam Coil pipe is located at the outside of cooling water coil.
CN201822123472.2U 2018-12-18 2018-12-18 A kind of ionic liquid preparation biodiesel reactor Active CN209348633U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822123472.2U CN209348633U (en) 2018-12-18 2018-12-18 A kind of ionic liquid preparation biodiesel reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201822123472.2U CN209348633U (en) 2018-12-18 2018-12-18 A kind of ionic liquid preparation biodiesel reactor

Publications (1)

Publication Number Publication Date
CN209348633U true CN209348633U (en) 2019-09-06

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201822123472.2U Active CN209348633U (en) 2018-12-18 2018-12-18 A kind of ionic liquid preparation biodiesel reactor

Country Status (1)

Country Link
CN (1) CN209348633U (en)

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