CN209333755U - A kind of solid-liquid hybrid reactor - Google Patents

A kind of solid-liquid hybrid reactor Download PDF

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Publication number
CN209333755U
CN209333755U CN201822195307.8U CN201822195307U CN209333755U CN 209333755 U CN209333755 U CN 209333755U CN 201822195307 U CN201822195307 U CN 201822195307U CN 209333755 U CN209333755 U CN 209333755U
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China
Prior art keywords
autoclave body
agitating shaft
solid
liquid
wall
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CN201822195307.8U
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Chinese (zh)
Inventor
孙奎峰
陈贵宝
宋新军
邹万利
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WEIHAI CHEMICAL MACHINERY CO Ltd
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WEIHAI CHEMICAL MACHINERY CO Ltd
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Abstract

The utility model provides a kind of solid-liquid hybrid reactor, the technical issues of which solve existing solid-liquid reaction kettle sealing element or agitating shaft excessive wears is equipped with autoclave body, kettle cover is arranged at the top of autoclave body, agitating shaft is arranged in autoclave body and decelerating motor is arranged on the outside of autoclave body;Sealing device is equipped with seal assembly, and seal assembly is equipped with rotating ring, stationary ring;Rotating ring is that cup-shaped structure, agitating shaft are fixedly connected with ring seal;Stationary ring is equipped with cylinder and goblet, and cylinder outer wall, which is connected with, upwardly extends goblet, and cylinder and goblet form cavity, injects liquid in cavity;Agitating shaft passes through cylinder intracoelomic cavity, and is mutually not connected between cylinder inner wall;Rotating ring wall of cup is downwardly into cavity, and rotating ring cup edge is located under liquid levels, is mutually not connected between rotating ring and stationary ring;Backgauge umbrella is equipped with below stirring port, backgauge umbrella covers stirring port, and agitating shaft is sealedly and fixedly connected with backgauge umbrella, can be widely applied to reaction kettle technical field.

Description

A kind of solid-liquid hybrid reactor
Technical field
The utility model relates to reaction kettle technical field, in particular to a kind of solid-liquid hybrid reactor.
Background technique
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, To realize the mixture response function of heating, evaporation that technique requires, cooling and low high speed.Reaction kettle is according to different production works Skill, operating condition etc. are not quite similar, and the design structure and parameter of reaction kettle are different, i.e. the structural style of reaction kettle is different, belong to Nonstandard tankage.
Existing solid-liquid reaction kettle during the reaction, finds mechanical seal or packing seal easily by fugitive dust, crystallization It influences, causes sealing element or agitating shaft excessive wear, cause equipment shut-down (breakdown) mainteance even to scrap, it is difficult to reach quantity-produced and want It asks.
Summary of the invention
Purpose of the utility model is to solve the deficiencies of above-mentioned technology, provide a kind of solid-liquid hybrid reactor, with every High efficiency non-contact seal structure from dust greatly prolongs the duty cycle while completely isolated, realizes continuous production.
For this purpose, the utility model provides a kind of solid-liquid hybrid reactor, it is equipped with autoclave body, the kettle being arranged at the top of autoclave body The decelerating motor for covering, the intracorporal agitating shaft of kettle being set and is arranged on the outside of autoclave body;The upper end of agitating shaft extends to the outer of autoclave body Side is sequentially connected across the output shaft of sealing device and decelerating motor;Sealing device is equipped with tubular rack and seal assembly, sealing Component is arranged in rack, and rack is connected with kettle cover;Kettle cover is equipped with feed inlet, and the bottom of autoclave body is equipped with discharge port, sealing group Part is equipped with rotating ring, stationary ring and pivot flange disk;Rotating ring is cup-shaped structure, and agitating shaft passes through the central axes of the bottom of a cup of rotating ring, and It is sealedly and fixedly connected with bottom of a cup;Stationary ring is equipped with cylinder and goblet, and the outer wall of cylinder is connected with the cup-shaped upwardly extended Body, cylinder and goblet form cavity, the liquid of injection non-aggressive or weak erosive in cavity;Agitating shaft passes through cylinder Inner cavity, and be mutually not connected between the outer wall of agitating shaft and the inner wall of cylinder;The wall of cup of rotating ring is downwardly into cavity, and dynamic The cup edge of ring is located under the liquid level of liquid, is mutually not connected between rotating ring and stationary ring;Goblet is connected with pivot flange disk, branch Support ring flange is connected with rack;The bottom of the rack place that is connected with kettle cover is equipped with stirring port, the lower section of stirring port and stirs The upper end of axis is equipped with backgauge umbrella, and backgauge umbrella covers stirring port, and backgauge umbrella is disk-like structure, and the center is equipped with shaft mounting hole; Agitating shaft passes through shaft mounting hole, and is sealedly and fixedly connected by the first axle sleeve and backgauge umbrella.
Preferably, backgauge umbrella is disc-shaped structure, is longitudinally extended downwards at the surrounding edge of backgauge umbrella.
Preferably, the upper end of agitating shaft is socketed with defoaming stirrer by the second axle sleeve, and defoaming stirrer is arranged in backgauge The lower section of umbrella, defoaming stirrer are managed equipped with snakelike defoaming.
Preferably, also connection is equipped with radar level gauge on kettle cover.
Preferably, autoclave body internal upper part is equipped with flusher, and flusher is equipped with inlet tube, flushing pipe and spray head;Feed liquor One end of pipe is connected with flushing pipe, and the other end of inlet tube passes through kettle cover and stretches out;Flushing pipe is cyclic structure, and flushing pipe Upper uniformly distributed connection is equipped with spray head, the inner wall of the spray port of spray head towards autoclave body.
Preferably, the upper section of agitating shaft is equipped with three narrow leaves rotation paddle, and the lower section of agitating shaft is equipped with three leaf swept-backs and revolves paddle, formed The stirring of second level combined type.
Preferably, longitudinal strip-shaped baffle and lateral rib are equipped in autoclave body, longitudinal strip-shaped baffle passes through lateral rib and kettle The inner wall of body is connected, and there are gaps between longitudinal strip-shaped baffle and the inner wall of autoclave body;Longitudinal strip-shaped baffle and lateral rib It is distributed by center axis circular array of agitating shaft.
Preferably, liquid is water.
Preferably, the bottom of a cup of agitating shaft and rotating ring is tightly connected by O-ring;The top of hypanthial wall of cup is equipped with ring-type Cover edge, one end of cyclic annular cover edge are connected with hypanthial wall of cup, and the other end of cyclic annular cover edge extends to the direction of cylinder, and It is mutually not connected to cylinder.
Preferably, the bottom of autoclave body, which is also connected to, is equipped with air inlet pipe.
The beneficial effects of the utility model are: the utility model provides a kind of solid-liquid hybrid reactor, has structure letter The significant advantages such as single, easy to clean, the operation is stable, with short production cycle, efficient high production capacity, can satisfy industrialization, serialization The requirement of production.
(1) sealing device, backgauge umbrella, a kind of stirred autoclave of defoaming stirrer combination are non-with the high efficiency of isolation dust Sealing structure is contacted, the duty cycle is greatly prolonged while completely isolated, reaches quantity-produced purpose.
(2) flusher, three narrow leaves rotation paddle, a kind of stirring suitable for solid-liquid mixing of three leaf swept-backs rotation paddle combination are anti- Kettle is answered, avoids powder solid from adhering to inner wall using withdrawing fluid, while by three narrow leaves rotation paddle and the rotation paddle cooperation of three leaf swept-backs Multithread to and peptizaiton achieve the effect that binary states material substantially uniformity mix.
(3) defoaming stirrer and radar level gauge cooperate, and solid-liquid are improved in quite big degree, reaction kettle is mixed Liquid level monitoring precision, and avoid the generation of traditional liquid level meter stopping state.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the structural schematic diagram of the portion A shown in FIG. 1 enlarged drawing;
Fig. 3 is the structural schematic diagram of the cross-sectional view of backgauge umbrella shown in FIG. 1;
Fig. 4 is the structural schematic diagram of the bottom view of Fig. 3;
Fig. 5 is the structural schematic diagram of flusher shown in FIG. 1;
Fig. 6 is the structural schematic diagram of bottom view shown in fig. 5;
Fig. 7 is the structural schematic diagram of defoaming stirrer shown in FIG. 1;
Fig. 8 is the structural schematic diagram of the A-A cross-sectional view of longitudinal strip-shaped baffle shown in FIG. 1.
Marked in the figure: 1. autoclave bodies, 2. kettle covers, 3. agitating shafts, 4. motors, 5. gear reduction units, 6. feed inlets, 7. dischargings Mouthful, 8. air inlet pipe, 9. racks, 10. rotating rings, 11. stationary rings, 12. pivot flange disks, 13.O type circle, 14. cylinders, 15. cup-shapeds Body, 16. cavitys, 17. liquid, 18. cyclic annular cover edges, 19. stirring ports, 20. backgauge umbrellas, 21. shaft mounting holes, 22. first axle sleeves, 23. the second axle sleeve, 24. defoaming stirrers, 25. snakelike defoaming pipes, 26. radar level gauges, 27. flushers, 28. inlet tubes, 29. flushing pipe, 30. spray heads, 31. 3 narrow leaves revolve paddle, 32. 3 leaf swept-backs revolve paddle, 33. longitudinal strip-shaped baffles, 34. horizontal bars Item, 35. gaps.
Specific embodiment
The utility model is described in further detail in the following with reference to the drawings and specific embodiments, to help the utility model is understood Content.Method used in the utility model is conventional method unless otherwise required;Used raw material and dress It sets, is conventional commercial product unless otherwise required.
As shown in Figure 1, the utility model provides a kind of solid-liquid hybrid reactor, is equipped with autoclave body 1, setting is pushed up in autoclave body 1 The kettle cover 2 in portion, the agitating shaft 3 being arranged in autoclave body 1 and the decelerating motor that 1 outside of autoclave body is arranged in, decelerating motor is by motor 4 It is composed with gear reduction unit 5, the top of tubular rack 9 is arranged in decelerating motor, and the upper end of agitating shaft 3 extends to autoclave body 1 Outside, across the pto shaft drive of sealing device and decelerating motor connect.Kettle cover 2 is equipped with feed inlet 6, the feed inlet 6 For manhole structure, solid and liquid charging stock is added for inside.The bottom of autoclave body 1 is respectively equipped with discharge port 7 and air inlet pipe 8, out Material mouth 7 is used to be discharged product after the reaction was completed from inside to outside from autoclave body 1, and air inlet pipe 8 is used to be passed through in reaction into autoclave body 1 lazy Property gas, such as nitrogen etc. carry out solid-liquid reaction in an inert atmosphere, avoid reacting the influence by oxygen.
As shown in Fig. 1, Fig. 2, the utility model sealing device is equipped with rack 9 and seal assembly, and seal assembly is arranged in machine In frame 9, rack 9 is connected with kettle cover 2;Seal assembly is equipped with rotating ring 10, stationary ring 11 and pivot flange disk 12;Rotating ring 10 is cup Shape structure, agitating shaft 3 pass through the central axes of the bottom of a cup of rotating ring 10, and are sealedly and fixedly connected with the bottom of a cup of rotating ring 10, preferably stir It mixes axis 3 and the bottom of a cup of rotating ring 10 is tightly connected by O-ring 13;Stationary ring 11 is equipped with cylinder 14 and goblet 15, cylinder 14 Outer wall be connected with the goblet 15 upwardly extended, cylinder 14 and goblet 15 form cavity 16, and injection is non-in cavity 16 The liquid 17 of corrosivity or weak erosive, liquid 17 are preferably water, and kettle temperature can be used less than 100 DEG C;Agitating shaft 3 passes through cylinder The inner cavity of body 14, and be mutually not connected between the outer wall of agitating shaft 3 and the inner wall of cylinder 14;The wall of cup of rotating ring 10 is downwardly into sky In chamber 16, and the cup edge of rotating ring 10 is located under the liquid level of liquid 17, is mutually not connected between rotating ring 10 and stationary ring 11;Goblet 15 are fixedly connected with pivot flange disk 12, and pivot flange disk 12 is fixedly connected with rack 9;The top of the wall of cup of goblet 15 is best Equipped with cyclic annular cover edge 18, one end of cyclic annular cover edge 18 is connected with the wall of cup of goblet 15, and the other end of cyclic annular cover edge 18 is to circle The direction of cylinder 14 extends, and is mutually not connected to cylinder 14, and introduced contaminants is avoided to enter contaminated fluid 17 in cavity 16.? On drive mechanism, the mechanical seal of traditional form is replaced using the simple water tight fashion of structure, existing dynamic and static ring is frictionally close Envelope is changed to non-contacting seal under the utility model liquid level, not only effectively avoids solid particle to the mill of sealing surface Damage, and the leakage of completely isolated powder fugitive dust, or even transmission power loss of tests is reduced to zero.
As shown in Fig. 1, Fig. 3, Fig. 4, the bottom of rack 9 is connected place with kettle cover 2 equipped with stirring port 19, stirring port 19 Lower section and the upper end of agitating shaft 3 be equipped with backgauge umbrella 20, the size of backgauge umbrella 20 can cover stirring port 19, and backgauge umbrella 20 is disk Shape structure, and the center is equipped with shaft mounting hole 21;Agitating shaft 3 passes through shaft mounting hole 21, and passes through the first axle sleeve 22 and backgauge Umbrella 20 is sealedly and fixedly connected.Backgauge umbrella 20 is disc-shaped structure, is longitudinally extended downwards at the surrounding edge of backgauge umbrella 20.It is stirred Material is sufficiently mixed under the action of blender in kettle in journey, and backgauge umbrella 20 is rotated with agitating shaft 3, and high degree avoids fugitive dust object Material enters in sealing device from stirring port 19, lengthens the water seal service intervals time, splashes backgauge umbrella for the solution in autoclave body 1 20 bottom surface, can downward longitudinal flow at the surrounding edge along backgauge umbrella 20, run up to and a certain amount of drop into reaction kettle again It is interior.
As shown in Fig. 1, Fig. 7, the upper end of agitating shaft 3 is socketed with defoaming stirrer 24, defoaming stirring by the second axle sleeve 23 The lower section of backgauge umbrella 20 is arranged in device 24, and defoaming stirrer 24 is equipped with snakelike defoaming pipe 25.Also connection is equipped with radar liquid on kettle cover 2 Position meter 26.Increase defoaming stirrer 24 in stirring system, and liquidometer uses the radar level gauge 26 of top installation, instead of The snakelike defoaming pipe 25 scraper defoaming effect of existing simple glass tube type liquid level gage, defoaming stirrer 24 very effectively removes The liquid levels layer bubble generated is stirred, had both prevented bubble rising from taking up solid material, and had in turn ensured 26 liquid level data of radar level gauge Accuracy, in addition, the apical dominance of radar level gauge 26, which completely avoids in autoclave body 1 solid material, blocks existing liquidometer Pipe.
As shown in Fig. 1, Fig. 5, Fig. 6,1 internal upper part of autoclave body be equipped with flusher 27, flusher 27 be equipped with inlet tube 28, Flushing pipe 29 and spray head 30;One end of inlet tube 28 is connected with flushing pipe 29, and the other end of inlet tube 28 passes through kettle cover 2 simultaneously It stretches out;Flushing pipe 29 is cyclic structure, and uniformly connection is equipped with spray head 30, the spray port direction of spray head 30 in flushing pipe 29 The inner wall of autoclave body 1.Because solid-liquid reaction technical process mixes for powder with liquid phase in autoclave body 1, and often adjoint in technical process Crystallization generates, and therefore, flusher 27 is equipped with spray head 30, using the reflux electrolyte of reaction kettle from feed liquor in whipping process Pipe 28 enters, and by flushing pipe 29, then sprays from the spray port of spray head 30, washes away to be attached to and adheres on 1 inner wall of autoclave body Powder reduces fugitive dust.
As shown in Fig. 1, Fig. 8, the upper section of agitating shaft 3 is equipped with commercially available three narrow leaf and revolves paddle 31, and the lower section of agitating shaft 3 is equipped with city Three leaf swept-backs rotation paddle 32 is sold, the stirring of second level combined type is formed.Longitudinal strip-shaped baffle 33 and lateral rib 34 are equipped in autoclave body 1, Longitudinal strip-shaped baffle 33 is connected by lateral rib 34 with the inner wall of autoclave body 1, and longitudinal direction strip-shaped baffle 33 and autoclave body 1 is interior There are gap 35 between wall, prevent solid-liquid mixture from accumulating;During longitudinal strip-shaped baffle 33 and lateral rib 34 with agitating shaft 3 be The distribution of mandrel line circular array.Three leaf swept-backs revolve paddle 32 based on slipstream, have both axial properties of flow, the rotation of three leaf swept-backs It is upward along chamber wall spiral that the certain inclination angle of the blade of paddle 32 achievees the effect that outside liquid stream, and intermediate flow rotation is downwards, gathers around There are dispersion, shearing material, it is Axial-flow stirrer that three narrow leaf of upper layer, which revolves paddle 31, and auxiliary three leaf swept-back of lower layer rotation paddle 32 stirs Effect is mixed, largely the systemic circulation of enhancing stirring liquid stream, then longitudinal 33 flow-disturbing of strip-shaped baffle is cooperated to act on, so that center whirlpool Whirlpool reduces, and shearing force is obviously improved, and solid-liquid mixture is promoted to be separated into fine droplets, and suspended state is in inside autoclave body 1, will not Agglomeration accumulation, to achieve the effect that uniformly to be sufficiently mixed, refine crystal grain and make crystal grain spheroidization.
The utility model is suitable for reaction kettle solid-liquid hybrid reaction, with LiFePO4 (LiFePO4) for synthesis, from Electrolyte is added into autoclave body 1 for feed inlet 6, then source of iron, phosphorus source and lithium source powder are added into electrolyte, then from air inlet pipe 8 N is continually fed into autoclave body 12, in N2Paddle 31 is revolved by three narrow leaves under environmental protection and three leaf swept-backs revolve paddle 32 and combine, and is utilized The mode of enhancing stirring liquid stream systemic circulation achievees the effect that electrolyte is uniformly sufficiently mixed, refines crystal grain and stirs crystal grain spheroidization Work is mixed, while utilizing flusher 27, reaction kettle constantly feeds electrolyte extremely during the reaction, by inlet tube 28 outside kettle The flusher 27 being fixed in kettle, then electrolyte washes away the powder or knot of 1 inner wall of autoclave body attachment by spray head 30 Crystalline substance, to prevent from having stirring dead zone in autoclave body 1, is provided with longitudinal strip-shaped baffle 33, it can make cutting for fluid to guarantee to be uniformly mixed It is changed into flowing and axially and radially flows, while increasing the less turbulence of the liquid in autoclave body 1, so as to improve mixing effect; Sealing device can effectively obstruct powder and overflow outside kettle during this, and completely avoid tradition using contactless simple seal The mechanical wear of transmission seal prevents dust-raising materials from entering water seal, greatly reduces wash number with the synergistic effect of backgauge umbrella 20, The production cycle is extended, quantity-produced purpose is reached;Defoaming stirrer 24 in stirring system prevents fugitive dust from arriving with crystallization Cooperate up to transmission shaft upper end, and with radar level gauge 26, avoids the blocking maintenance of traditional liquid level meter, improve working efficiency and monitoring Precision.
It is clean to have simple structure, the operation is stable, reaction environment compared with existing equipment operates operating condition for the utility model Only, the significant advantages such as with short production cycle, efficient high production capacity, can satisfy the requirement of industrialization, continuous production.
In the description of the present invention, it should be understood that term "left", "right", "upper", "lower", "top", "bottom", The orientation or positional relationship of the instructions such as "front", "rear", "inner", "outside", " back ", " centre " is orientation based on the figure or position Relationship is set, is merely for convenience of describing the present invention and simplifying the description, rather than the device or element of indication or suggestion meaning Must have specific orientation, be constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention.
Only as described above, only specific embodiment of the utility model, when the utility model cannot be limited with this The range of implementation, therefore the displacement of its equivalent assemblies, or according to equivalent changes and modifications made by the utility model patent protection scope, It should still belong to the scope that the utility model claims book is covered.

Claims (10)

1. a kind of solid-liquid hybrid reactor is equipped with autoclave body, the kettle cover being arranged at the top of the autoclave body, is arranged in the autoclave body Agitating shaft and the decelerating motor that is arranged on the outside of the autoclave body;The upper end of the agitating shaft extends to the outside of the autoclave body, It is sequentially connected across the output shaft of sealing device and the decelerating motor;The sealing device is equipped with tubular rack and sealing group Part, the seal assembly are arranged in the rack, and the rack is connected with the kettle cover;The kettle cover is equipped with feed inlet, The bottom of the autoclave body is equipped with discharge port, which is characterized in that the seal assembly is equipped with rotating ring, stationary ring and pivot flange disk;Institute Stating rotating ring is that cup-shaped structure, the agitating shaft are sealed with the bottom of a cup and fixed across the central axes of the bottom of a cup of the rotating ring Connection;The stationary ring is equipped with cylinder and goblet, and the outer wall of the cylinder is connected with the goblet upwardly extended, The cylinder and the goblet form cavity, the liquid of injection non-aggressive or weak erosive in the cavity;It is described to stir It mixes axis and passes through the inner cavity of the cylinder, and be mutually not connected between the outer wall of the agitating shaft and the inner wall of the cylinder;Institute The wall of cup for stating rotating ring is downwardly into the cavity, and the cup edge of the rotating ring is located under the liquid level of the liquid, described dynamic It is mutually not connected between ring and the stationary ring;The goblet is connected with the pivot flange disk, the pivot flange disk and institute Rack is stated to be connected;The bottom of the rack be connected with the kettle cover place be equipped with stirring port, the lower section of the stirring port and The upper end of the agitating shaft is equipped with backgauge umbrella, and the backgauge umbrella covers the stirring port, and the backgauge umbrella is disk-like structure, and its Shaft mounting hole is equipped at center;The agitating shaft passes through the shaft mounting hole, and is sealed by the first axle sleeve and the backgauge umbrella It is fixedly connected.
2. a kind of solid-liquid hybrid reactor according to claim 1, which is characterized in that the backgauge umbrella is discoid knot Structure longitudinally extends downwards at the surrounding edge of the backgauge umbrella.
3. a kind of solid-liquid hybrid reactor according to claim 1 or 2, which is characterized in that the upper end of the agitating shaft is logical It crosses the second axle sleeve and is socketed with defoaming stirrer, the lower section of the backgauge umbrella, the defoaming stirring is arranged in the defoaming stirrer Device is managed equipped with snakelike defoaming.
4. a kind of solid-liquid hybrid reactor according to claim 3, which is characterized in that also connection is equipped with thunder on the kettle cover Up to liquidometer.
5. a kind of solid-liquid hybrid reactor according to claim 1, which is characterized in that the autoclave body internal upper part, which is equipped with, to be rinsed Device, the flusher are equipped with inlet tube, flushing pipe and spray head;One end of the inlet tube is connected with the flushing pipe Logical, the other end of the inlet tube passes through the kettle cover and stretches out;The flushing pipe is cyclic structure, and in the flushing pipe Cloth connection is equipped with the spray head, the inner wall of the spray port of the spray head towards the autoclave body.
6. a kind of solid-liquid hybrid reactor according to claim 1 or 5, which is characterized in that the upper section of the agitating shaft is set There are three narrow leaves to revolve paddle, the lower section of the agitating shaft is equipped with three leaf swept-backs and revolves paddle, forms the stirring of second level combined type.
7. a kind of solid-liquid hybrid reactor according to claim 6, which is characterized in that be equipped with longitudinal bar shaped in the autoclave body Baffle and lateral rib, the longitudinal direction strip-shaped baffle are connected by the lateral rib with the inner wall of the autoclave body, and described There are gaps between longitudinal strip-shaped baffle and the inner wall of the autoclave body;The longitudinal direction strip-shaped baffle and the lateral rib are with described Agitating shaft is the distribution of center axis circular array.
8. a kind of solid-liquid hybrid reactor according to claim 1, which is characterized in that the liquid is water.
9. a kind of solid-liquid hybrid reactor according to claim 1, which is characterized in that the agitating shaft and the rotating ring The bottom of a cup is tightly connected by O-ring;The top of the hypanthial wall of cup is equipped with cyclic annular cover edge, and the one of the ring-type cover edge End be connected with the hypanthial wall of cup, it is described ring-type cover edge the other end to the direction of the cylinder extension, and with institute Cylinder is stated mutually to be not connected to.
10. a kind of solid-liquid hybrid reactor according to claim 1, which is characterized in that the bottom of the autoclave body is also connected to Equipped with air inlet pipe.
CN201822195307.8U 2018-12-25 2018-12-25 A kind of solid-liquid hybrid reactor Active CN209333755U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822195307.8U CN209333755U (en) 2018-12-25 2018-12-25 A kind of solid-liquid hybrid reactor

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Application Number Priority Date Filing Date Title
CN201822195307.8U CN209333755U (en) 2018-12-25 2018-12-25 A kind of solid-liquid hybrid reactor

Publications (1)

Publication Number Publication Date
CN209333755U true CN209333755U (en) 2019-09-03

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115282917A (en) * 2022-08-30 2022-11-04 湖南长城科技有限公司 Reaction kettle for preparing magnesium sulfate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115282917A (en) * 2022-08-30 2022-11-04 湖南长城科技有限公司 Reaction kettle for preparing magnesium sulfate

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