CN209333235U - A kind of extraction structure of novel distillation system - Google Patents

A kind of extraction structure of novel distillation system Download PDF

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Publication number
CN209333235U
CN209333235U CN201821830984.6U CN201821830984U CN209333235U CN 209333235 U CN209333235 U CN 209333235U CN 201821830984 U CN201821830984 U CN 201821830984U CN 209333235 U CN209333235 U CN 209333235U
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return tank
condenser
cooler
pipe
connection
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CN201821830984.6U
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Chinese (zh)
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淡周利
韩增磊
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Shandong Mitutoyo New Materials Co Ltd
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Shandong Mitutoyo New Materials Co Ltd
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Abstract

The utility model discloses a kind of extraction structures of novel distillation system, including first-stage condenser, secondary condenser, new extraction mouth, cooler, return tank A and return tank B, the energy-saving appliance side passes through piping connection rectifying column, the energy-saving appliance other side passes through piping connection first-stage condenser, new extraction mouth is provided with below the first-stage condenser, the first-stage condenser passes through piping connection secondary condenser, the secondary condenser other side is provided with liquid outlet, the liquid outlet passes through piping connection cooler, the cooler produces pipe by cold methanol and connects return tank B, the return tank B bottom conduit connects dnockout pumps B, the other side dnockout pumps B connection cold methanol gets pipe, the new extraction mouth produces pipe by hot methanol and connects return tank A, the system designs a kind of novel extraction structure, it realizes The purpose of two kinds of state of temperature solvents is received in one distillation system, easy to operate, practicability is high.

Description

A kind of extraction structure of novel distillation system
Technical field
The utility model relates to a kind of chemical process device, specially a kind of extraction structure of novel distillation system.
Background technique
In chemical plant installations, crystallized stock is subjected to carrying out washing treatment, washed crystallization with cleaning solvent in centrifuge Material is discharged through drying, or directly uses, or becomes finished product after drying.And what is thrown away contains impurity solvent liquid, it is necessary to pass through Rectification process system working process separates impurity from solvent liquid.
And conventional rectification process system only one extraction point, produce a kind of solvent of lower temperature state.And molten Agent in use, only in the solvent of centrifuge washing process temperature lower (general 20 degree or less).And reaction kettle, hot melt is being added It kettle, crystallization kettle and alters when washing process pipe, it is necessary to use the higher solvent of temperature (50-60 degree is advisable).
Utility model content
A kind of solvent drawbacks described above of temperature can only be produced in view of existing conventional rectification process system, the utility model Purpose is to design a kind of novel extraction structure in conventional rectification process system, to solve to use existing conventional rectifying Process system cannot produce the disadvantage of two kinds of temperature solvents.
To achieve the above object, the utility model provides the following technical solutions:
A kind of extraction structure of novel distillation system, including energy-saving appliance, first-stage condenser, secondary condenser, newly produce mouth, Liquid outlet, cooler, return tank A, return tank B, dnockout pumps A, dnockout pumps B and rectifying column, the energy-saving appliance side pass through pipeline Rectifying column is connected, the energy-saving appliance other side is provided with new by piping connection first-stage condenser, the first-stage condenser lower section Mouth is produced, the first-stage condenser is provided with liquid outlet by piping connection secondary condenser, the secondary condenser other side, The liquid outlet produces pipe by cold methanol and connects return tank B, the return tank by piping connection cooler, the cooler B bottom conduit connects dnockout pumps B, and the other side dnockout pumps B connection cold methanol gets pipe, and the new extraction mouth passes through hot methanol It produces pipe and connects return tank A, the return tank A bottom conduit connects dnockout pumps A, and the other side the dnockout pumps A connects hot methanol Get pipe.
Furthermore, control valve is provided on the pipeline of the device.
Furthermore, cooling water inlet and cooling water outlet, and cooling water inlet and cooling water outlet are provided on the cooler It is arranged in cooler two sides.
Furthermore, the rectifying column exterior line connection and return pipe.
Furthermore, recirculated water inlet/outlet pipe is all connected with outside the first-stage condenser and secondary condenser.Further For, the energy-saving appliance exterior line connection evaporator and mother liquor coming expects pipe.
Compared with prior art, the utility model has the beneficial effects that the novel distillation system is in conventional rectification process A kind of novel extraction structure is designed in system, the new extraction mouth of design installation one in first-stage condenser, to realize The purpose of two kinds of state of temperature solvents is received in a distillation system, easy to operate, practicability is high.
Detailed description of the invention
Fig. 1 is the utility model embodiment structural schematic diagram.
Fig. 2 is that conventional rectification process system produces structural schematic diagram.
In figure: 1, energy-saving appliance;2, first-stage condenser;3, secondary condenser;4, mouth is newly produced;5, liquid outlet;6, cooler; 7, return tank A;8, return tank B;9, dnockout pumps A;10, dnockout pumps B;11, rectifying column.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
It is in the description of the present invention, it should be noted that term " center ", "upper", "lower", "left", "right", " perpendicular Directly ", the orientation or positional relationship of the instructions such as "horizontal", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, and is only For ease of description the utility model and simplify description, rather than the device or element of indication or suggestion meaning must have it is specific Orientation, be constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention.In addition, term " the One ", " second ", " third " are used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance.
The utility model provides a kind of technical solution referring to FIG. 1-2:
A kind of extraction structure of novel distillation system, including energy-saving appliance 1, first-stage condenser 2, secondary condenser 3, new extraction Mouth 4, liquid outlet 5, cooler 6, return tank A7, return tank B8, dnockout pumps A9, dnockout pumps B10 and rectifying column 11, the energy-saving appliance 1 side is by piping connection rectifying column 11, and by piping connection first-stage condenser 2, the level-one is cold for 1 other side of energy-saving appliance New extraction mouth 4 is provided with below condenser 2, the first-stage condenser 2 passes through piping connection secondary condenser 3, the B-grade condensation 3 other side of device is provided with liquid outlet 5, and the liquid outlet 5 is adopted by piping connection cooler 6, the cooler 6 by cold methanol Outlet pipe connects return tank B8, and the return tank B8 bottom conduit connects dnockout pumps B10, and the connection of the other side the dnockout pumps B10 is cold Methanol gets pipe, and the new extraction mouth 4 produces pipe by hot methanol and connects return tank A7, the return tank A7 bottom conduit connection Dnockout pumps A9, the other side dnockout pumps A9 connection hot methanol get pipe.Regulating valve is provided on the pipeline of the device , cooling water inlet and cooling water outlet are provided on the cooler 6, and cooling water inlet and cooling water outlet are arranged at 6 liang of cooler Side, 11 exterior line of rectifying column connects and return pipe, is all connected with and follows outside the first-stage condenser 2 and secondary condenser 3 Ring water entrance pipe, 1 exterior line of the energy-saving appliance connection evaporator and mother liquor coming expects pipe.
Working principle: the extraction structure of the distillation system designs the new extraction mouth 4 of installation in first-stage condenser 2, through celebrating a festival The methanol of energy device 1 and first-stage condenser 2, is only that methanol solvate just becomes liquid from gaseous state herein at this time, relatively high in its temperature When a part be plucked out of, and enter return tank A7 in, without the solvent material of extraction, go successively to secondary condenser 3 It further cools with cooler 6, eventually becomes the relatively low methanol solvate of temperature, realize and connect in a distillation system Receive the purpose of two kinds of state of temperature solvents.
Although the utility model is described in detail with reference to the foregoing embodiments, come for those skilled in the art Say, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic into Row equivalent replacement, within the spirit and principle of the utility model, any modification, equivalent replacement, improvement and so on should all It is included within the scope of protection of this utility model.

Claims (5)

1. a kind of extraction structure of novel distillation system, including it is energy-saving appliance (1), first-stage condenser (2), secondary condenser (3), new Produce mouth (4), liquid outlet (5), cooler (6), return tank A (7), return tank B (8), dnockout pumps A (9), dnockout pumps B (10) and Rectifying column (11), it is characterised in that: by piping connection rectifying column (11), the energy-saving appliance (1) is another for energy-saving appliance (1) side Side is provided with new extraction mouth (4), the level-one by piping connection first-stage condenser (2), first-stage condenser (2) lower section For condenser (2) by piping connection secondary condenser (3), secondary condenser (3) other side is provided with liquid outlet (5), institute Liquid outlet (5) are stated by piping connection cooler (6), the cooler (6) produces pipe connection return tank B (8) by cold methanol, Return tank B (8) bottom conduit connects dnockout pumps B (10), and (10) other side the dnockout pumps B connection cold methanol gets pipe, The new extraction mouth (4) produces pipe connection return tank A (7) by hot methanol, and return tank A (7) bottom conduit connects dnockout It pumps A (9), (9) other side the dnockout pumps A connection hot methanol gets pipe.
2. a kind of extraction structure of novel distillation system according to claim 1, it is characterised in that: the cooler (6) On be provided with cooling water inlet and cooling water outlet, and cooling water inlet and cooling water outlet are arranged in cooler (6) two sides.
3. a kind of extraction structure of novel distillation system according to claim 1, it is characterised in that: the rectifying column (11) Exterior line connection and return pipe.
4. a kind of extraction structure of novel distillation system according to claim 1, it is characterised in that: the first-stage condenser (2) and outside secondary condenser (3) it is all connected with recirculated water inlet/outlet pipe.
5. a kind of extraction structure of novel distillation system according to claim 1, it is characterised in that: the energy-saving appliance (1) Exterior line connects evaporator and mother liquor coming expects pipe.
CN201821830984.6U 2018-11-08 2018-11-08 A kind of extraction structure of novel distillation system Active CN209333235U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821830984.6U CN209333235U (en) 2018-11-08 2018-11-08 A kind of extraction structure of novel distillation system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821830984.6U CN209333235U (en) 2018-11-08 2018-11-08 A kind of extraction structure of novel distillation system

Publications (1)

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CN209333235U true CN209333235U (en) 2019-09-03

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110041998A (en) * 2019-05-16 2019-07-23 南安市蒂巧工艺品有限公司 A kind of fatty acid refining plant
CN110508022A (en) * 2019-10-11 2019-11-29 唐山三孚电子材料有限公司 The device and method of on-condensible gas control rectifying tower pressure is not utilized

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110041998A (en) * 2019-05-16 2019-07-23 南安市蒂巧工艺品有限公司 A kind of fatty acid refining plant
CN110508022A (en) * 2019-10-11 2019-11-29 唐山三孚电子材料有限公司 The device and method of on-condensible gas control rectifying tower pressure is not utilized

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