CN204602153U - Liquid material recycling of condensed steam utilizes device - Google Patents

Liquid material recycling of condensed steam utilizes device Download PDF

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Publication number
CN204602153U
CN204602153U CN201520124321.2U CN201520124321U CN204602153U CN 204602153 U CN204602153 U CN 204602153U CN 201520124321 U CN201520124321 U CN 201520124321U CN 204602153 U CN204602153 U CN 204602153U
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CN
China
Prior art keywords
condenser
steam
reactor
bottle
communicated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201520124321.2U
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Chinese (zh)
Inventor
徐德伟
徐水荣
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Jiangxi Zhong Xiang Science And Technology Ltd
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Jiangxi Zhong Xiang Science And Technology Ltd
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Priority to CN201520124321.2U priority Critical patent/CN204602153U/en
Application granted granted Critical
Publication of CN204602153U publication Critical patent/CN204602153U/en
Expired - Fee Related legal-status Critical Current
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model relates to a kind of technical field of chemical, especially a kind of liquid material recycling of condensed steam utilizes device, a large amount of steam can be produced when being applicable to liquid charging stock reaction, comprise reactor, described reactor top is provided with condenser, described condenser comprises the first condenser, the second condenser, described first condenser, the second condenser all with the inner space of reactor.By condenser, the steam-condensation produced during raw material reaction is reused, improve raw material availability; Connected by two condensers, improve the efficiency of steam-condensation; The practicality of raw material and the state of drop bottle better can be observed by the drop bottle with graduated glass.

Description

Liquid material recycling of condensed steam utilizes device
Technical field
The utility model relates to a kind of technical field of chemical, and especially a kind of liquid material recycling of condensed steam utilizes device, can produce a large amount of steam when being applicable to liquid charging stock reaction.
Background technology
At present, during production bromination series of products, raw material is the liquid material that concentration is higher, often can cause the blocking of drop bottle, and the service condition of metal drop bottle also bad observation raw material; When raw material reacts in reactor, can produce a large amount of steam, need to carry out being condensed into liquid with condenser, backflow continues reaction, and the utilization rate of raw material is improved, but current most condenser can not meet demand when bromination series of products are produced.
The utility model, just based on above-mentioned consideration, with evaporative condenser principle for foundation, designs a kind of device recycled liquid material steam, and this device extends to allly to be existed in the reaction of liquid vapour.
Meanwhile, the technical solution of the utility model, also solves the observation control problem of liquid charging stock consumption.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, adapts to reality need, provides a kind of liquid material recycling of condensed steam to utilize device.
In order to realize the purpose of this utility model, the technical solution adopted in the utility model is:
A kind of liquid material recycling of condensed steam utilizes device, and comprise reactor, described reactor top is provided with condenser, and described condenser comprises the first condenser, the second condenser, described first condenser, the second condenser all with the inner space of reactor.
The outside of described first condenser, the second condenser is Bottle structure, the inner chamber of Bottle structure is provided with helix tube, the upper end of described helix tube is steam inlet, and lower end is condensation-water drain, and described steam inlet, condensation-water drain are all communicated with reactor top.
The top of described reactor is respectively equipped with steam drain and liquid backflow mouth, and described steam drain is communicated with the steam inlet of helix tube, and described liquid backflow mouth is communicated with the condensation-water drain of helix tube.
The external branch pipe of described steam drain, described branch pipe separates two arms and is communicated with the steam inlet of helix tube in the first condenser, the second condenser respectively; The reverse branch pipe of described liquid backflow mouth external, described reverse branch pipe separates two arms and is communicated with the condensation-water drain of helix tube in the first condenser, the second condenser respectively.
The bottle of described first condenser, the second condenser is arranged in series from top to bottom, the bottle bottom of the first condenser is communicated with the bottle top of the second condenser, the top of described first condenser is provided with cooling water inlet pipe, and the bottom of the second condenser is provided with cooling water outlet pipe.
Described cooling water inlet pipe, cooling water outlet pipe are equipped with valve, between the bottle of described first condenser, the second condenser, are provided with tube connector.
Also comprise the conventional drop bottle be arranged at above reactor, described conventional drop bottle is communicated with reactor by discharge nozzle, and described conventional drop bottle is provided with scale.
Also comprise the graduated reserve liquid drop bottle of band, described discharge nozzle is equipped with gate valve.
The beneficial effects of the utility model are:
1. by condenser, the steam-condensation produced during raw material reaction is reused, improve raw material availability;
2. connected by two condensers, improve the efficiency of steam-condensation;
3. better can observe the practicality of raw material and the state of drop bottle by the drop bottle of the graduated glass of band.
Accompanying drawing explanation
Fig. 1 is the structural representation that a kind of liquid material recycling of condensed steam of the utility model utilizes device;
1-reactor, 21-commonly uses drop bottle, 22-reserve liquid drop bottle, 31-first condenser, 32-second condenser, 4-tube connector, 5-steam drain, 6-branch pipe, 7-steam inlet, 8-helix tube, 10-liquid backflow mouth, the reverse branch pipe of 11-, 12-condensation-water drain, 14-enters cooling water pipe, and 15-goes out cooling water pipe, 17-discharge nozzle.
Detailed description of the invention
Below in conjunction with Fig. 1 and embodiment, embodiment of the present utility model is elaborated.
A kind of liquid material recycling of condensed steam utilizes device, comprise reactor 1, described reactor 1 top is provided with condenser, described condenser comprises the first condenser 31, second condenser 32, described first condenser 31, second condenser 32 all with the inner space of reactor 1, raw material produces a large amount of steam in reactor 1, becomes liquid by the first condenser 31 with the second condenser 32 rapid condensation, be back in the inner chamber of reactor 1, continue reaction.
The outside of described first condenser 31, second condenser 32 is Bottle structure, the inner chamber of Bottle structure is provided with helix tube 8, the upper end of described helix tube 8 is steam inlet 7, lower end is condensation-water drain 12, described steam inlet 7, condensation-water drain 12 are all communicated with reactor 1 top, steam enters helix tube 8 by steam inlet 7 and carries out condensation, and condensed condensed water is flowed out by condensation-water drain 12; The top of described reactor 1 is respectively equipped with steam drain 5 and liquid backflow mouth 10, described steam drain 5 is communicated with the steam inlet 7 of helix tube 8, described liquid backflow mouth 10 is communicated with the condensation-water drain 12 of helix tube 8, steam drain 5 is communicated with steam inlet 7, steam can be made to flow in condenser in reactor 1, liquid backflow mouth 10 is communicated with condensation-water drain 12, and condensed water can be made from condenser, is back in reactor 1 and continues reaction; The external branch pipe 6 of described steam drain 5, described branch pipe 6 separates two arms and is communicated with the steam inlet 7 of helix tube 8 in the first condenser 31, second condenser 32 respectively; The reverse branch pipe 11 of described liquid backflow mouth 10 external, described reverse branch pipe 11 separates two arms and is communicated with the condensation-water drain 12 of helix tube 8 in the first condenser 31, second condenser 32 respectively, by the Liang Ge branch of branch pipe 6, first condenser 31 is connected with the steam drain on reactor 1 with the steam inlet 7 on the second condenser 32, by reverse branch pipe 11, condensation-water drain 12 is communicated with liquid backflow mouth 10.
The bottle of described first condenser 31, second condenser 32 is arranged in series from top to bottom, the bottle bottom of the first condenser 31 is communicated with the bottle top of the second condenser 32, the top of described first condenser 31 is provided with cooling water inlet pipe 14, the bottom of the second condenser 32 is provided with cooling water outlet pipe 15, cooling water flows to from entering cooling water pipe 14, filled by condenser, when cooling water temperature is too high, the gate valve opened out on cooling water pipe 15 is discharged, also comprise the conventional drop bottle 21 be arranged at above reactor 1, described conventional drop bottle 21 is communicated with reactor by discharge nozzle 17, described conventional drop bottle 21 is provided with scale, also comprise the graduated reserve liquid drop bottle 22 of band, described discharge nozzle 17 is equipped with gate valve, the product of bromination series, raw material used is high concentration liquid mixture, easily cause the blocking of drop bottle, when conventional drop bottle 21 blocks, reserve liquid drop bottle 22 can be used, production can not be delayed, also better can observe the state of drop bottle as drop bottle with vial, scale is set, better can observe the service condition of raw material.

Claims (8)

1. a liquid material recycling of condensed steam utilizes device, comprise reactor (1), it is characterized in that: described reactor (1) top is provided with condenser, described condenser comprises the first condenser (31), the second condenser (32), described first condenser (31), the second condenser (32) all with the inner space of reactor (1).
2. liquid material recycling of condensed steam according to claim 1 utilizes device, it is characterized in that: the outside of described first condenser (31), the second condenser (32) is Bottle structure, the inner chamber of Bottle structure is provided with helix tube (8), the upper end of described helix tube (8) is steam inlet (7), lower end is condensation-water drain (12), and described steam inlet (7), condensation-water drain (12) are all communicated with reactor (1) top.
3. liquid material recycling of condensed steam according to claim 2 utilizes device, it is characterized in that: the top of described reactor (1) is respectively equipped with steam drain (5) and liquid backflow mouth (10), described steam drain (5) is communicated with the steam inlet (7) of helix tube (8), and described liquid backflow mouth (10) is communicated with the condensation-water drain (12) of helix tube (8).
4. liquid material recycling of condensed steam according to claim 3 utilizes device, it is characterized in that: the external branch pipe (6) of described steam drain (5), described branch pipe (6) separates two arms and is communicated with the steam inlet (7) of helix tube (8) in the first condenser (31), the second condenser (32) respectively; The reverse branch pipe (11) of described liquid backflow mouth (10) external, described reverse branch pipe (11) separates two arms and is communicated with the condensation-water drain (12) of helix tube (8) in the first condenser (31), the second condenser (32) respectively.
5. liquid material recycling of condensed steam according to claim 4 utilizes device, it is characterized in that: the bottle of described first condenser (31), the second condenser (32) is arranged in series from top to bottom, the bottle bottom of the first condenser (31) is communicated with the bottle top of the second condenser (32), the top of described first condenser (31) is provided with cooling water inlet pipe (14), and the bottom of the second condenser (32) is provided with cooling water outlet pipe (15).
6. liquid material recycling of condensed steam according to claim 5 utilizes device, it is characterized in that: (15) are equipped with valve for described cooling water inlet pipe (14), cooling water outlet pipe, between the bottle of described first condenser (31), the second condenser (32), be provided with tube connector (4).
7. the liquid material recycling of condensed steam according to claim arbitrary in claim 1 to claim 6 utilizes device, it is characterized in that: also comprise the conventional drop bottle (21) being arranged at reactor (1) top, described conventional drop bottle (21) is communicated with reactor by discharge nozzle (17), and described conventional drop bottle (21) is provided with scale.
8. liquid material recycling of condensed steam according to claim 7 utilizes device, it is characterized in that: also comprise the graduated reserve liquid drop bottle (22) of band, (17) are equipped with gate valve with described discharge nozzle, and described drop bottle is vial.
CN201520124321.2U 2015-03-04 2015-03-04 Liquid material recycling of condensed steam utilizes device Expired - Fee Related CN204602153U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520124321.2U CN204602153U (en) 2015-03-04 2015-03-04 Liquid material recycling of condensed steam utilizes device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520124321.2U CN204602153U (en) 2015-03-04 2015-03-04 Liquid material recycling of condensed steam utilizes device

Publications (1)

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CN204602153U true CN204602153U (en) 2015-09-02

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108043343A (en) * 2018-01-04 2018-05-18 洛阳乐森石化新材料有限公司 A kind of reaction kettle cooling water circulation recovery system
CN110006774A (en) * 2018-01-04 2019-07-12 中电电气(上海)太阳能科技有限公司 A kind of cross linking degree tester of recyclable dimethylbenzene and its application

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108043343A (en) * 2018-01-04 2018-05-18 洛阳乐森石化新材料有限公司 A kind of reaction kettle cooling water circulation recovery system
CN110006774A (en) * 2018-01-04 2019-07-12 中电电气(上海)太阳能科技有限公司 A kind of cross linking degree tester of recyclable dimethylbenzene and its application

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150902

Termination date: 20180304