CN205007613U - Lactide rapid condensation crystallization device - Google Patents
Lactide rapid condensation crystallization device Download PDFInfo
- Publication number
- CN205007613U CN205007613U CN201520587293.8U CN201520587293U CN205007613U CN 205007613 U CN205007613 U CN 205007613U CN 201520587293 U CN201520587293 U CN 201520587293U CN 205007613 U CN205007613 U CN 205007613U
- Authority
- CN
- China
- Prior art keywords
- pipe
- condensation
- condenser pipe
- lactide
- connects
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000009833 condensation Methods 0.000 title claims abstract description 36
- 230000005494 condensation Effects 0.000 title claims abstract description 35
- JJTUDXZGHPGLLC-UHFFFAOYSA-N lactide Chemical compound CC1OC(=O)C(C)OC1=O JJTUDXZGHPGLLC-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 238000002425 crystallisation Methods 0.000 title claims abstract description 11
- 230000008025 crystallization Effects 0.000 title claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 238000003860 storage Methods 0.000 claims abstract description 19
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 8
- 229910052802 copper Inorganic materials 0.000 claims description 8
- 239000010949 copper Substances 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000009434 installation Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
Landscapes
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
Abstract
The utility model discloses a lactide rapid condensation crystallization device, including condenser pipe, inner tube, outlet pipe, storage water tank, water pump, inlet tube, condensation entry and condensation export, installation inner tube in the condenser pipe, the condensation export is connected to the condenser pipe upper end, and the condensation entry is connected to the condenser pipe lower extreme, condensation entry linkage inlet tube, and condensation exit linkage outlet pipe goes out water piping connection storage water tank upper end, advances water piping connection storage water tank lower extreme, and the water pump is connected to storage water tank one side. Compared with the prior art, the utility model discloses simple structure, convenient to use, manufacturing cost are than lower.
Description
Technical field
The utility model relates to PLA production technical field, is specifically related to a kind of lactide rapid condensation crystallization apparatus.
Background technology
In PLA preparation process, the lactide that Pfansteihl mixture Pintsch process generates is a kind of rough lactide, the inside is containing a large amount of impurity, therefore need to carry out reaction further by rough that lactide is refined, carry out at lactide needing condensation process in the process of refining, and traditional condensation process is too slow, operating efficiency is lower.
Utility model content
The purpose of this utility model is to provide the lactide rapid condensation crystallization apparatus that a kind of structure is simple, easy to use, manufacturing cost is lower.
For achieving the above object, the utility model provides following technical scheme:
A kind of lactide rapid condensation crystallization apparatus, comprise condenser pipe, interior pipe, outlet pipe, storage tank, water pump, water inlet pipe, condensation entrance and condensate outlet, pipe in installing in condenser pipe, condenser pipe upper end connects condensate outlet, and condenser pipe lower end connects condensation entrance, and condensation entrance connects water inlet pipe, condensate outlet connects outlet pipe, outlet pipe connects storage tank upper end, and water inlet pipe connects storage tank lower end, and storage tank side connects water pump.
As the further improvement of above-mentioned technology, described interior pipe adopts copper product to make.
As the further improvement of above-mentioned technology, described condenser pipe carries out slant setting.
Compared with prior art, the beneficial effects of the utility model are: interior pipe adopts copper product to make, because copper has good thermal conductivity, condensation work fast and effectively can be carried out, condenser pipe carries out slant setting, add condensation effect, the utility model structure is simple, easy to use simultaneously, manufacturing cost is lower.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: pipe, 3-outlet pipe, 4-storage tank, 5-water pump, 6-water inlet pipe, 7-condensation entrance, 8-condensate outlet in 1-condenser pipe, 2-.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
A kind of lactide rapid condensation crystallization apparatus, comprise condenser pipe 1, interior pipe 2, outlet pipe 3, storage tank 4, water pump 5, water inlet pipe 6, condensation entrance 7 and condensate outlet 8, condenser pipe 1 carries out slant setting, increase condensation effect, pipe 2 in installing in condenser pipe 1, interior pipe 2 adopts copper product to make, be convenient to carry out condensation fast, condenser pipe 1 upper end connects condensate outlet 8, condenser pipe 1 lower end connects condensation entrance 7, condensation entrance 7 connects water inlet pipe 6, condensate outlet 8 connects outlet pipe 3, the outlet pipe 3 that condensate outlet 8 connects connects storage tank 4 upper end, the water inlet pipe 6 that condensation entrance 7 connects connects storage tank 4 lower end, storage tank 4 side connects water pump.
During utility model works, start water pump 5, water inside storage tank 4 is by water inlet pipe 6, arrive condensation entrance 7, water enters condenser pipe 1 from condensation entrance 7, pipe 2 in installing in condenser pipe 1, interior pipe 2 adopts copper product to make, pure lactide steam is passed in interior pipe 2, due to the thermal conductive resin of copper and under the effect passing through cold water in condenser pipe 1 outside copper pipe, be liquid by the rapid cooling down of pure lactide steam, thus reach the object of rapid condensation crystallization, the condensate outlet 8 that water in condenser pipe 1 after heat absorption passed through condenser pipe 1 upper end flows into outlet pipe 3, and finally flow back to storage tank 4, thus reach the object recycled.
The foregoing is only preferred embodiment of the present invention; not thereby embodiments of the present invention and protection domain is limited; to those skilled in the art; the equivalent replacement that all utilizations description of the present invention and diagramatic content are made and the scheme that apparent change obtains should be recognized, all should be included in protection scope of the present invention.
Claims (3)
1. a lactide rapid condensation crystallization apparatus, comprise condenser pipe, interior pipe, outlet pipe, storage tank, water pump, water inlet pipe, condensation entrance and condensate outlet, it is characterized in that, pipe in installing in condenser pipe, condenser pipe upper end connects condensate outlet, condenser pipe lower end connects condensation entrance, condensation entrance connects water inlet pipe, and condensate outlet connects outlet pipe, and outlet pipe connects storage tank upper end, water inlet pipe connects storage tank lower end, and storage tank side connects water pump.
2. lactide rapid condensation crystallization apparatus according to claim 1, is characterized in that, described interior pipe adopts copper product to make.
3. lactide rapid condensation crystallization apparatus according to claim 1, it is characterized in that, described condenser pipe carries out slant setting.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520587293.8U CN205007613U (en) | 2015-08-07 | 2015-08-07 | Lactide rapid condensation crystallization device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520587293.8U CN205007613U (en) | 2015-08-07 | 2015-08-07 | Lactide rapid condensation crystallization device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205007613U true CN205007613U (en) | 2016-02-03 |
Family
ID=55206243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520587293.8U Expired - Fee Related CN205007613U (en) | 2015-08-07 | 2015-08-07 | Lactide rapid condensation crystallization device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205007613U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2621342C1 (en) * | 2016-07-29 | 2017-06-02 | Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский государственный университет" (ТГУ, НИ ТГУ) | Receiver of vacuum chamber reactor of synthesis of glycolide and lactid |
-
2015
- 2015-08-07 CN CN201520587293.8U patent/CN205007613U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2621342C1 (en) * | 2016-07-29 | 2017-06-02 | Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский государственный университет" (ТГУ, НИ ТГУ) | Receiver of vacuum chamber reactor of synthesis of glycolide and lactid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160203 Termination date: 20160807 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |