CN209317692U - A kind of substance purifies and separates system - Google Patents
A kind of substance purifies and separates system Download PDFInfo
- Publication number
- CN209317692U CN209317692U CN201821582962.2U CN201821582962U CN209317692U CN 209317692 U CN209317692 U CN 209317692U CN 201821582962 U CN201821582962 U CN 201821582962U CN 209317692 U CN209317692 U CN 209317692U
- Authority
- CN
- China
- Prior art keywords
- ion exchange
- exchange column
- purifies
- separates
- column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model discloses a kind of substance purifies and separates systems, including sample injection bottle, separator and automatic collecting device, separator includes ion exchange column, resin is filled in ion exchange column, ion exchange column lower part is provided with flow control valve, automatic collecting device is set to flow control valve rear portion, and constant flow pump is provided between sample injection bottle and separator;The substance purifies and separates system of the utility model, that realizes mixed solution is automatically separated, purifies and collects automatically filtrate, and purifies and separates device volume is small, and capacity is small, is suitble to the purifies and separates of a small amount of solution.
Description
Technical field
The utility model belongs to extraction and separation field, more specifically to a kind of substance purifies and separates system.
Background technique
Purifying and separation are the steps that the most common means are either necessary in some experiments, but due to different realities
It tests, it is different to the required precision of purifies and separates.In the prior art, the ion exchange column in purifies and separates system more one is whole, and
Its volume and volume are bigger, are not suitable for the separation of a small amount of former mixed solution, so that the experiment of some purifies and separates is unable to complete.
Utility model content
The purpose of this utility model is to provide a kind of substance purifies and separates systems, realize the automatic purifying of former mixed solution
Separation, filtrate are collected automatically, and purifies and separates device volume is small, and capacity is small, are suitble to the purifies and separates of a small amount of mixed solution, while this
The ion exchange column of utility model is oneself potting resin as needed inside hollow column tube, can be selected the amount of the type of resin
It selects, convenient for experiment.
A kind of substance purifies and separates system of technical solutions of the utility model, including sample injection bottle, separator and automatic collection
Device, the separator include ion exchange column, and resin, the ion exchange column lower part are filled in the ion exchange column
Be provided with flow control valve, the automatic collecting device is set to flow control valve rear portion, the sample injection bottle and separator it
Between be provided with constant flow pump, the ion exchange column includes column tube and the spiral cover that column tube oral area is arranged in, the spiral cover center
It is provided with pore, passing through in the pore has diversion pipe, and locking lid, the locking lid and pore spiral shell are provided with outside the pore
Line connection, the spiral cover are connect with column tube mouth thread.
Preferably, the ion exchange column bottom is provided with outlet tube, and the flow control valve is arranged on outlet tube, institute
It states column tube inside bottom and is provided with sieve plate, the aperture of sieve pore is less than resin diameter on the sieve plate.
Preferably, the automatic collecting device includes turntable, and the turntable bottom is provided with intermittent rotary device, on turntable
Portion is provided with circular collection slot, and collecting pipe is provided in circular collection slot, and the collecting pipe shape arranged in a ring is arranged in circle
In collecting tank, it is provided with cover board on circular collection slot, circular collection groove radius direction is provided with a receipts on the cover board
Ji Kou, the outlet end of the outlet tube pass through collection port towards collection spout part.
Preferably, the intermittent rotary device includes the annular disk fixed with turntable, is set on the annular disk inner peripheral surface
It is equipped with card slot, annular disk is internally provided with driving disc spacing pressing, driving lever is provided on the driving disc spacing pressing outer circumference surface, and the driving lever is placed in it
In in a card slot.
Preferably, the driving disc spacing pressing is not overlapped with the annular disk center of circle, and servo motor, the column are connected on the driving disc spacing pressing
Tubing matter is polypropylene.
The utility model technology the utility model has the advantages that
A kind of substance purifies and separates system of technical solutions of the utility model collects separating liquid, behaviour using automatic collecting device
Facilitate, may be implemented to automate unattended, raising conventional efficient.
A kind of substance purifies and separates system of technical solutions of the utility model, ion exchange column are the open tubular column that can be uncapped
Pipe, the potting resin in hollow column tube, experimenter, which can according to need, selects different resin and amount of resin, and column tube volume is small,
Volume is small, and the purifies and separates of a small amount of or even micro original solution may be implemented, and improves the precision that microminiature realizes purifies and separates.
A kind of substance purifies and separates system of technical solutions of the utility model, the design of spiral cover on ion exchange column, on the one hand
Convenient for being placed or taken out resin in the column tube to ion exchange column, liquid is by ion after on the other hand avoiding ion exchange column from expiring liquid
Exchange column upper oral part overflows.
A kind of substance purifies and separates system of technical solutions of the utility model needs in the experiment of certain some purifies and separates
With strong acid and pretreatment by strong alkali resin, this requires that ion exchange column has a good acidproof alkali ability, and the utility model
Ion exchange column be made of polypropylene, compared to the prior art in glass material ion exchange column it is at low cost, price is just
Preferably, acidproof alkali ability is good.
Detailed description of the invention
Fig. 1 is a kind of substance purifies and separates system structure diagram of the utility model,
Fig. 2 is ion exchange column structural schematic diagram,
Fig. 3 is spiral cover top plan,
Fig. 4 is intermittent rotary schematic device,
Fig. 5 is collection device top view.
Specific embodiment
For convenient for those skilled in the art understand that technical solutions of the utility model, practical new to this now in conjunction with Figure of description
Type technical solution is described further.
As shown in Figures 1 to 4, a kind of substance purifies and separates system, including sample injection bottle 1, separator 3 and automatic collect fill
5 are set, separator 3 includes ion exchange column 9, is filled with resin 10 in ion exchange column 9,9 lower part of ion exchange column is provided with
Flow control valve 4, automatic collecting device 5 are set to 4 rear portion of flow control valve, are provided with perseverance between sample injection bottle 1 and separator 3
Stream pump 2, ion exchange column 9 includes column tube and the spiral cover 8 that column tube oral area is arranged in, and 8 center of spiral cover is provided with pore 6, is managed
Passing through in hole 6 has diversion pipe 19, locking lid 7 is provided with outside pore 6, locking lid 7 is threadedly coupled with pore 6, spiral cover 8 and ion
The connection of 9 mouth thread of exchange column, 9 bottom of ion exchange column are provided with outlet tube 20, and flow control valve 4 is arranged in outlet tube 20
On, column tube inside bottom is provided with sieve plate 21, and the aperture of sieve pore is less than resin diameter on sieve plate 21, and automatic collecting device 5 includes
Turntable 18,18 bottom of turntable are provided with intermittent rotary device, and 18 top of turntable is provided with circular collection slot, sets in circular collection slot
It is equipped with collecting pipe 17, the shape arranged in a ring of collecting pipe 17 is arranged in circular collection slot, cover board 22 is provided on circular collection slot,
Circular collection groove radius direction is provided with a collection port 23 on cover board 22, the outlet end of outlet tube 20 passes through collection port 23
Towards 17 oral area of collecting pipe, intermittent rotary device includes the annular disk 13 that 18 are fixed with turntable, is set on 13 inner peripheral surface of annular disk
It is equipped with card slot 16, annular disk 13 is internally provided with driving disc spacing pressing 14, driving lever 15 is provided on 14 outer circumference surface of driving disc spacing pressing, and driving lever 15 is set
In in a wherein card slot 16, driving disc spacing pressing 14 is not overlapped with 13 center of circle of annular disk, and servo motor, column tube material are connected on driving disc spacing pressing 14
Matter is polypropylene.
As shown in Figures 1 to 4, a kind of substance purifies and separates system of the utility model when work, opens ion exchange column
The resin of appropriate volume and weight is placed in ion exchange column 9, the spiral cover 8 of ion exchange column 9 is covered, diversion pipe 19 is installed
It is good, and locking lid 7 is screwed on, diversion pipe 19 and spiral cover 8 is fixed, and fixation is to open 2 He of constant flow pump on ion exchange column 9
Servo motor in flow control valve 5 and automatic collecting device, so that the solution to be separated of sample injection bottle 1 passes through ion exchange column 9
It is separated, by Resin Absorbent, solution is directly separated out to the collecting pipe 17 in automatic collecting device 5 substances such as some impurity
Interior, the servo motor in automatic collecting device 5 drives driving disc spacing pressing 14 to rotate, and the driving lever 15 on driving disc spacing pressing 14 is stirred by card slot 16
Annular disk 13, so that the intermittent rotation of annular disk 13, by adjusting servo motor revolving speed, so that driving disc spacing pressing 14 rotates a circle just
It is the time that collecting pipe 17 collects a pipe liquid well, avoids and change pipe manually, realizes full-automatic.
A kind of substance purifies and separates system of the utility model, mixed solution are separated by ion exchange column, are needed
For the substance separated by Resin Absorbent, remaining solution reserves after ion exchange column is finally collected pipe mobile phone, then will
The substance adsorbed on ion exchange column obtains the substance for needing purifies and separates by cleaning out.
Technical solutions of the utility model are exemplarily described utility model above in conjunction with attached drawing, it is clear that this is practical
Novel specific implementation is not subject to the restrictions described above, as long as using the method concept and technical solution progress of the utility model
Various unsubstantialities improve, or it is not improved the conception and technical scheme of utility model are directly applied into other occasions,
It both is within the protection scope of the present invention.
Claims (5)
1. a kind of substance purifies and separates system, including sample injection bottle, separator and automatic collecting device, which is characterized in that described
Separator includes ion exchange column, resin is filled in the ion exchange column, the ion exchange column lower part is provided with stream
Control valve, the automatic collecting device are set to flow control valve rear portion, are provided between the sample injection bottle and separator
Constant flow pump, the ion exchange column include column tube and the spiral cover that column tube oral area is arranged in, and the spiral cover center is provided with pipe
Hole, interior pass through of the pore have diversion pipe, locking lid are provided with outside the pore, and the locking lid is threadedly coupled with pore,
The spiral cover is connect with column tube mouth thread.
2. a kind of substance purifies and separates system according to claim 1, which is characterized in that the ion exchange column bottom is set
It is equipped with outlet tube, the flow control valve is arranged on outlet tube, and the column tube inside bottom is provided with sieve plate, on the sieve plate
The aperture of sieve pore is less than resin diameter.
3. a kind of substance purifies and separates system according to claim 2, which is characterized in that the automatic collecting device includes
Turntable, the turntable bottom are provided with intermittent rotary device, and turntable top is provided with circular collection slot, setting in circular collection slot
There is collecting pipe, the collecting pipe shape arranged in a ring is arranged in circular collection slot, and cover board is provided on circular collection slot, described
Circular collection groove radius direction is provided with a collection port on cover board, the outlet end of the outlet tube passes through collection port direction
Collect spout part.
4. a kind of substance purifies and separates system according to claim 3, which is characterized in that the intermittent rotary device includes
The fixed annular disk with turntable is provided with card slot on the annular disk inner peripheral surface, and annular disk is internally provided with driving disc spacing pressing, described
Driving lever is provided on driving disc spacing pressing outer circumference surface, the driving lever is placed in one in a card slot.
5. a kind of substance purifies and separates system according to claim 4, which is characterized in that the driving disc spacing pressing and annular disk circle
The heart is not overlapped, and servo motor is connected on the driving disc spacing pressing, and the column tube material is polypropylene.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821582962.2U CN209317692U (en) | 2018-09-27 | 2018-09-27 | A kind of substance purifies and separates system |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821582962.2U CN209317692U (en) | 2018-09-27 | 2018-09-27 | A kind of substance purifies and separates system |
Publications (1)
Publication Number | Publication Date |
---|---|
CN209317692U true CN209317692U (en) | 2019-08-30 |
Family
ID=67707326
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201821582962.2U Expired - Fee Related CN209317692U (en) | 2018-09-27 | 2018-09-27 | A kind of substance purifies and separates system |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN209317692U (en) |
-
2018
- 2018-09-27 CN CN201821582962.2U patent/CN209317692U/en not_active Expired - Fee Related
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190830 Termination date: 20210927 |
|
CF01 | Termination of patent right due to non-payment of annual fee |