CN209287272U - A kind of vertical ultrasonic reaction kettle - Google Patents

A kind of vertical ultrasonic reaction kettle Download PDF

Info

Publication number
CN209287272U
CN209287272U CN201822191052.8U CN201822191052U CN209287272U CN 209287272 U CN209287272 U CN 209287272U CN 201822191052 U CN201822191052 U CN 201822191052U CN 209287272 U CN209287272 U CN 209287272U
Authority
CN
China
Prior art keywords
reaction kettle
ultrasonic
main body
valve
vertical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201822191052.8U
Other languages
Chinese (zh)
Inventor
魏鹏勃
魏新刚
王龙昌
高红强
胡敬海
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Hengjin Chemical Technology Co Ltd
Original Assignee
Guangzhou Hengjin Chemical Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Hengjin Chemical Technology Co Ltd filed Critical Guangzhou Hengjin Chemical Technology Co Ltd
Priority to CN201822191052.8U priority Critical patent/CN209287272U/en
Application granted granted Critical
Publication of CN209287272U publication Critical patent/CN209287272U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a kind of vertical ultrasonic reaction kettle, the vertical ultrasonic reaction kettle includes reactor main body;Wherein, ultrasonic unit is provided on the vertical ultrasonic reaction kettle, the ultrasonic unit can make the reactant into reaction kettle completely broken, keep the progress of reaction more thorough, improve the yield and production efficiency of reaction finished product.

Description

A kind of vertical ultrasonic reaction kettle
Technical field
The utility model relates to a kind of reaction kettles, in particular to a kind of vertical ultrasonic reaction kettle.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter It sets, realizes the mixed function for heating, evaporation, cooling and the low high speed that technique requires.Reaction kettle be widely used in petroleum, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Force container, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;The material of reaction kettle generally have carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composite materials.
Traditional reaction kettle has that stirring is insufficient, stir the insufficient reactant that can prevent inside reaction kettle from It is completely broken, it will lead to reaction and be not thorough, seriously affected the yield and production efficiency of reaction finished product.
Utility model content
A kind of in order to overcome the deficiencies of the prior art, the utility model provides vertical ultrasonic reaction kettle is described vertical super Ultrasonic unit is provided on phonoresponse kettle, ultrasonic unit can make the reactant into reaction kettle completely broken, make reaction It carries out more thorough.
Correspondingly, the utility model embodiment provides a kind of vertical ultrasonic reaction kettle, the vertical ultrasonic reaction kettle packet Reactor main body is included, motor is installed, the output end of the motor is provided with agitating shaft, described at the top of the reactor main body At least one propeller group is provided on agitating shaft;
It is additionally provided with helium valve port at the top of the reactor main body, multiple pan feeding valve ports, vacuumizes valve port, manhole, pressure Power table, observation is shown on trial and ultrasonic unit;The ultrasonic unit includes supersonic generator, ultrasonic transducer and surpasses Sound wave amplitude transformer, the supersonic generator are electrically connected with ultrasonic transducer, and the ultrasonic variable amplitude bar is fastened on super On acoustic wave transducer;
Outer coil pipe is wound in the middle part of the reactor main body, the bottom of the reaction kettle is provided with blowing valve port and thermometric Device.
Optional embodiment, the bottom of the reactor main body are provided with agitating shaft fixing seat;
The one end of the mixing shaft is fastened on the output end of motor, and the other end is based on bearing and is slidably connected at the stirring In axis fixing seat.
Optional embodiment, the propeller group include two opposite propellers in direction of rotation.
Optional embodiment, the helium valve port, multiple pan feeding valve ports, the inside for vacuumizing valve port and blowing valve port It is mounted on electromagnetic valve.
Optional embodiment, the material shown on trial of observing is organic glass.
Optional embodiment, the ultrasonic transducer are the ultrasonic transducer of piezoelectric ceramic type.
The both ends of optional embodiment, the outer coil pipe are respectively arranged with the first triple valve and the second triple valve.
Optional embodiment, first triple valve and the second triple valve are all solenoid valve.
The inner wall of optional embodiment, the reactor main body is uniformly coated with anti-stick coating.
The utility model embodiment provides a kind of vertical ultrasonic reaction kettle, is arranged on the vertical ultrasonic reaction kettle There is ultrasonic unit, the ultrasonic unit can make the reactant into reaction kettle completely broken, keep the progress of reaction more thorough Bottom improves the yield and production efficiency of reaction finished product.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it is clear that, the accompanying drawings in the following description is only It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor Under, it can also be obtained according to these attached drawings other attached drawings.
Fig. 1 is the structural schematic diagram of reactor main body in the utility model embodiment;
Fig. 2 is the top view of reactor main body in the utility model embodiment;
Fig. 3 is the structural schematic diagram of ultrasonic unit in the utility model embodiment.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without creative efforts All other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1 is the structural schematic diagram of reactor main body in the utility model embodiment, and Fig. 2 is in the utility model embodiment The top view of reactor main body.
As depicted in figs. 1 and 2, the utility model embodiment provides a kind of vertical ultrasonic reaction kettle, the vertical ultrasonic Reaction kettle includes reactor main body 1, and the middle part of the reactor main body 1 is cylinder, and upper and lower ends are hemisphere or approximate half Sphere.
The top of the reactor main body 1 is equipped with motor 11, it should be noted that the type of the motor 11 is in this reality It is not construed as limiting in new embodiment, it should be according to items such as the viscosity of reactant, revolving speed requirement and power requirements in actual production Part selects the type of motor 11.
The output end of the motor 11 is provided with agitating shaft 12, and the agitating shaft 12 stretches to the inside of reactor main body 1, The agitating shaft 12 is rotated with the rotation of 11 rotor of motor;Particularly, in order to enable agitating shaft 12 to rotate along same axis, institute The bottom for stating reactor main body 1 is provided with agitating shaft fixing seat 13, and the other end of the opposite motor 11 of the agitating shaft 12 is based on axis It holds and is slidably connected in agitating shaft fixing seat 13;In addition, at least one propeller group is provided on the agitating shaft 12, in order to make Stirring is more abundant, and each propeller group includes two opposite propellers in direction of rotation 14.
The upper end of the reactor main body 1 is provided with helium valve port 21, multiple pan feeding valve ports 22 and vacuumizes valve port 23, The bottom of the reactor main body 1 is provided with blowing valve port 24.It is the helium valve port 21, more in the utility model embodiment A pan feeding valve port 22 vacuumizes valve port 23 and the inside of blowing valve port 24 is mounted on electromagnetic valve, and the electromagnetic valve It is electrically connected with terminal device, the open and close of electromagnetic valve is controlled by terminal, to indirectly control the logical of helium Enter amount, feeding and blowing amount.In addition, the valve port 23 that vacuumizes is controlled to a vacuum pump by pipeline;It needs to illustrate It is that vacuum pump refers to using machinery, physics, chemically or physically chemical method is evacuated and obtains vacuum to being smoked container The concrete type of device or equipment, vacuum pump should be selected according to actual needs, not limited in the utility model embodiment It is fixed;When reaction needs to carry out under vacuum conditions, valve port 23 is vacuumized by terminal opening, and is opened corresponding true Empty pumping unit can carry out vacuumize process to reaction kettle.
The upper end of the reactor main body 1 is additionally provided with pressure gauge 25, observes show on trial 26 and manhole 27.Wherein, described Pressure gauge 25 is for being monitored the pressure inside reaction kettle.The observation is shown on trial 26 to be made of organic glass, organic glass There is the preferable transparency, is observed convenient for the inside to reaction kettle;In addition, organic glass anti-impact force is stronger, by organic glass Observation is shown on trial made of glass, and 26 is durable and safety is good.The manhole 27 uses fast-open type structure, opening and closing flexibly, convenient for personnel into Reactor main body 1 is out to install reaction kettle, be overhauled and the operation such as safety inspection;In addition, manhole 27 or reaction kettle Safety emergency air-breather, usually matches with flame damper, mechanical breather valve etc., caused by being both avoided that because of accidental cause in tank Sharply superpressure or vacuum cause storage tank to damage and cause safety accident, and can play the role of safe back-fire relief.
Fig. 3 is the structural schematic diagram of ultrasonic unit in the utility model embodiment.
As shown in figure 3, also setting up ultrasonic unit 3 in the upper end of reactor main body 1, the ultrasonic unit 3 can make Reactant is completely broken, keeps the progress of reaction more thorough, improves yield and production efficiency.Wherein, the ultrasonic wave dress It sets 3 and includes supersonic generator 4, ultrasonic transducer 5 and ultrasonic variable amplitude bar 6, the supersonic generator 4 and ultrasonic wave Energy converter 5 is electrically connected, and the ultrasonic variable amplitude bar 6 is fastened on ultrasonic transducer 5.
Specifically, the supersonic generator 4 is electrically connected with ultrasonic transducer 5, height is provided for ultrasonic transducer 5 Frequently, high pressure, high-power power supply.In practical work process, the supersonic generator 4 can be by 50 hertz or 60 hertz after being powered Alternating current hereby is converted to the alternating current of the frequencies such as the 20kHz that ultrasonic transducer 5 works required or 35kHz or 40kHz, to drive Dynamic ultrasonic transducer 5 works.
Specifically, the high frequency electrical signal that supersonic generator 4 provides can be converted to high frequency by the ultrasonic transducer 5 Mechanical shock (i.e. ultrasonic wave).In the present invention, the ultrasonic transducer 5 is the ultrasonic wave transducer of piezoelectric ceramic type Device, the main function element of the ultrasonic transducer 5 are piezoceramics crystal 51;The piezoceramics crystal 51 is based on material The inverse piezoelectric effect of material generates ultrasonic wave.It should be noted that inverse piezoelectric effect refers to if applying electric signal to piezoelectric material, Piezoelectric material can generate mechanical stress;In the utility model embodiment, the high frequency electrical signal that supersonic generator 4 provides is acted on On piezoceramics crystal 51, piezoceramics crystal 51 just generates the mechanical shock of corresponding high frequency, the mechanical shock of the high frequency Other components can be transmitted to.
Specifically, one end of the ultrasonic variable amplitude bar 6 is fastened on the back casing of ultrasonic transducer 5, it is another End is inserted into the inside of reactor main body 1.The ultrasonic variable amplitude bar 6 can particle displacement mechanical oscillation or speed put Greatly, and by the energy of ultrasonic wave it concentrates on lesser area, to improve electro-acoustic conversion efficiency.In the utility model embodiment In, 6 main function of ultrasonic variable amplitude bar is the amplitude and vibration velocity ratio for increasing ultrasonic transducer 5, to improve ultrasonic wave The working efficiency of energy converter 5;In addition, the ultrasonic variable amplitude bar 6 is using hardness, high, heat-resist material is made, ultrasonic wave The setting of amplitude transformer 6 is not necessarily to ultrasonic transducer 5 and material directly contact, and extend ultrasonic transducer 5 uses the longevity Life.
The middle part of the reactor main body 1 is provided with outer coil pipe 28, and the outer coil pipe 28 is wrapped in reactor main body 1 Portion, the outer coil pipe 28 is mainly used for logical cooling water or hot steam is cooled down or heated to reaction kettle.Wherein, the outer coil pipe The first triple valve 281 and the second triple valve 282, first triple valve 281 and the second triple valve 282 is respectively set in 28 both ends It is connect with cooling water recirculation system and the hot steam circulatory system;It should be noted that second triple valve 282 is cooling water Import, first triple valve 281 be cooling water outlet, the cooling water is from cooling water recirculation system through the second triple valve 282 enter outer coil pipe 28, then flow back to cooling water recirculation system through the first triple valve 281, to cool down to reaction kettle;And First triple valve 281 be hot steam import, second triple valve 282 be hot steam outlet, the hot steam from The hot steam circulatory system flows into outer coil pipe through the first triple valve 281, then flows back to the hot steam circulatory system through the second triple valve 282, To carry out heat temperature raising to reaction kettle.In addition, first triple valve 281 and the second triple valve 282 are solenoid valve, described One triple valve 281 and the second triple valve 282 are electrically connected with terminal device, by terminal to the first triple valve 281 and the two or three The open and close of port valve 282 are controlled, and are controlled with the temperature to reaction kettle.
Correspondingly, being additionally provided with temperature measuring equipment 29 in the bottom of reactor main body 1, the temperature measuring equipment extend into reaction kettle The inside of main body 1 is monitored the temperature of reaction kettle;In addition, the temperature measuring equipment 29 is also electrically connected with terminal, it is obtained Temperature data can be transmitted in terminal.
In addition, the inner wall of reactor main body 1 is evenly coated with anti-stick coating, anti-stick coating can effectively prevent reactant to stick in The inner wall of reactor main body 1.
The utility model embodiment provides a kind of vertical ultrasonic reaction kettle, the course of work of the vertical ultrasonic reaction kettle It is as follows: temperature and pressure in reaction kettle being checked by temperature measuring equipment 29, pressure gauge 25 first, it is ensured that temperature in reaction kettle with Pressure is temperature and pressure needed for reaction;If pressure is not inconsistent, opens helium valve port 21 and vacuumize valve port 23, by being passed through The pressure of reaction kettle is adjusted in helium or vaccum-pumping equipment;If temperature is not inconsistent, be passed through in outer coil pipe 28 cooling water or The temperature of reaction kettle is adjusted in hot steam.After ensuring that temperature of reaction kettle and pressure are normal, opens pan feeding valve port 22 and be added instead Object is answered, and opens ultrasonic unit 3 and motor 11, reacts material sufficiently;In reaction process, 26 pairs can be shown on trial by observation instead It should be observed;After reaction, blowing valve port 24 is opened, by reaction finished product discharge.
The utility model embodiment provides a kind of vertical ultrasonic reaction kettle, is provided on the vertical ultrasonic reaction kettle super Acoustic wave device, the ultrasonic unit can make the reactant into reaction kettle completely broken, keep the progress of reaction more thorough, mention The high yield and production efficiency of reaction finished product.
In addition, a kind of vertical ultrasonic reaction kettle provided by the utility model embodiment is described in detail above, Specific case should be used herein to be expounded the principles of the present invention and embodiment, the explanation of above embodiments It is merely used to help understand the method and its core concept of the utility model;At the same time, for those skilled in the art, according to According to the thought of the utility model, there will be changes in the specific implementation manner and application range, in conclusion this specification Content should not be construed as a limitation of the present invention.

Claims (9)

1. a kind of vertical ultrasonic reaction kettle, which is characterized in that the vertical ultrasonic reaction kettle includes reactor main body, the reaction Motor is installed, the output end of the motor is provided with agitating shaft, at least one is provided on the agitating shaft at the top of kettle main body A propeller group;
Be additionally provided at the top of the reactor main body helium valve port, multiple pan feeding valve ports, vacuumize valve port, manhole, pressure gauge, Observation is shown on trial and ultrasonic unit;The ultrasonic unit includes supersonic generator, ultrasonic transducer and ultrasonic wave Amplitude transformer, the supersonic generator are electrically connected with ultrasonic transducer, and the ultrasonic variable amplitude bar is fastened on ultrasonic wave On energy converter;
Outer coil pipe is wound in the middle part of the reactor main body, the bottom of the reaction kettle is provided with blowing valve port and thermometric dress It sets.
2. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the bottom of the reactor main body is provided with Agitating shaft fixing seat;
The one end of the mixing shaft is fastened on the output end of motor, and the other end is slidably connected at the agitating shaft based on bearing and consolidates In reservation.
3. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the propeller group includes two rotation sides To opposite propeller.
4. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the helium valve port, multiple pan feeding valve ports, The inside for vacuumizing valve port and blowing valve port is mounted on electromagnetic valve.
5. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the material shown on trial of observing is organic glass Glass.
6. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the ultrasonic transducer is piezoelectric ceramics The ultrasonic transducer of formula.
7. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the both ends of the outer coil pipe are respectively arranged with First triple valve and the second triple valve.
8. vertical ultrasonic reaction kettle according to claim 7, which is characterized in that first triple valve and the second triple valve It is all solenoid valve.
9. vertical ultrasonic reaction kettle according to claim 1, which is characterized in that the inner wall of the reactor main body is equably It is coated with anti-stick coating.
CN201822191052.8U 2018-12-25 2018-12-25 A kind of vertical ultrasonic reaction kettle Active CN209287272U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822191052.8U CN209287272U (en) 2018-12-25 2018-12-25 A kind of vertical ultrasonic reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201822191052.8U CN209287272U (en) 2018-12-25 2018-12-25 A kind of vertical ultrasonic reaction kettle

Publications (1)

Publication Number Publication Date
CN209287272U true CN209287272U (en) 2019-08-23

Family

ID=67648579

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201822191052.8U Active CN209287272U (en) 2018-12-25 2018-12-25 A kind of vertical ultrasonic reaction kettle

Country Status (1)

Country Link
CN (1) CN209287272U (en)

Similar Documents

Publication Publication Date Title
CN206715918U (en) A kind of reactor for circulating Hybrid Heating
CN106215793B (en) A kind of ultrasonic wave mixing vacuum stirring tank for natural esters insulating oil
CN209287272U (en) A kind of vertical ultrasonic reaction kettle
CN206304705U (en) A kind of use for laboratory high-pressure temperature control stirs small-sized reactor
CN209020351U (en) A kind of automatic agitating type autoclave
CN211754340U (en) Canned equipment is used in laundry liquid production
CN207822938U (en) A kind of automatic manufacturing device of aqueous high temperature lacquer
CN206778416U (en) A kind of multifunctional reaction still
CN211800753U (en) Be used for production of graphite alkene filter membrane to use raw materials rabbling mechanism
CN206184050U (en) Substrate glue water bubble system
CN210846390U (en) Enamel reaction tank
CN207237996U (en) A kind of chemical industry fiber-reactive kettle with cleaning filtering function
CN204147835U (en) Solid reaction still
CN206701281U (en) A kind of environmentally friendly medicament reactor
CN208727478U (en) A kind of energy-efficient reaction kettle
CN208200935U (en) The agitating device and probiotics fermention tank of fermentor
CN208526555U (en) A kind of high pressure form reaction kettle of pressure adjustable
CN216093619U (en) High-efficient reation kettle is used in amino salicylic acid production
CN209696878U (en) A kind of novel high-efficient reaction still
CN206304751U (en) A kind of pyroreaction device for producing trioxy- cyclobutane yl carboxylic acid
CN206082514U (en) Fertile production response cauldron of marine alga
CN110586007A (en) Environment-friendly heating device's reation kettle
CN204952884U (en) Reation kettle that adjustable control by temperature change was pressed
CN110237799A (en) A kind of biomass cellulose hydrothermal liquefaction high pressure reaction assembly
CN215086902U (en) From pesticide production of taking high-efficient fast hot structure with shearing cauldron

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant