CN209280390U - A kind of sample injector for environmental gas precise quantitative - Google Patents

A kind of sample injector for environmental gas precise quantitative Download PDF

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Publication number
CN209280390U
CN209280390U CN201821890201.3U CN201821890201U CN209280390U CN 209280390 U CN209280390 U CN 209280390U CN 201821890201 U CN201821890201 U CN 201821890201U CN 209280390 U CN209280390 U CN 209280390U
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China
Prior art keywords
solenoid valve
air passage
passage block
sample injector
sample
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CN201821890201.3U
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Inventor
黄华
倪有强
李娟�
李涛
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SHANGHAI INESA ANALYTICAL INSTRUMENT CO Ltd
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SHANGHAI INESA ANALYTICAL INSTRUMENT CO Ltd
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Abstract

A kind of sample injector for environmental gas precise quantitative of the utility model, is related to technical field of analytical instruments.Comprising filter, the first solenoid valve, second solenoid valve, third solenoid valve, the 4th solenoid valve, the 5th solenoid valve are passivated air passage block, and quantitative loop, aspiration pump is connected in a manner of pipeline and control circuit is constituted.The use of the sample injector of the utility model operates, it further include six control flows, that is sample phase, the sample introduction stage, the cavity pressure period during pipeline-cleaning, filter blowback stage during pipeline-cleaning, the cavity repressurization stage during pipeline-cleaning, the quantitative loop rinse stage during pipeline-cleaning.The utility model proposes a kind of micromations, modularization, low-power consumption, the sampling device of low cost, it is ensured that the accurate quantitative analysis of sample acquisition, stability, repeatability, to the following analysis instrument, especially online and portable analysers preprocessing system, provides solid technology material base, has very far-reaching reference reference significance.

Description

A kind of sample injector for environmental gas precise quantitative
Technical field
The utility model relates to technical field of analytical instruments, refer specifically to a kind of sample introduction for environmental gas precise quantitative Device.
Background technique
Sample injector is the preprocessing system of analysis instrument.Its major function is the acquisition for completing to analyze sample, and sample To the stability of analysis instrument, repeatability is most important for accurate quantitative analysis and sample introduction in collection process.Currently, in the acquisition of sample In the process, six-way valve or ten-way valve are used mostly for site environment detecting instrument, especially portable analysers, Realize along with switch electromagnetic valve etc. acquisition and the sample introduction of sample.This method is not only at high cost, but also in bad environments In the case where, being easy, which pollutes six-way valve or ten-way valve, even blocks.This not only adds the maintenance cost of instrument, and it is right In the stability of analysis instrument, repeatability is very unfavorable.
Utility model content
The purpose of this utility model overcomes missing and deficiency of the existing technology, proposes a kind of for site environment detection The accurate quantitative sampling of instrument and sample injector.
A kind of sample injector for environmental gas precise quantitative of the utility model includes filter, the first solenoid valve, second Solenoid valve, third solenoid valve, the 4th solenoid valve, the 5th solenoid valve, are passivated air passage block, quantitative loop, and aspiration pump is connected in a manner of pipeline It connects and control circuit board is constituted.
Wherein, first solenoid valve one end is connected to the filter, and the sample injector entrance of the other end and passivation air passage block connects It connects;
Second solenoid valve one end is connect with aspiration pump, and the other end is connect with the drain of passivation air passage block;
Third solenoid valve one end is connect with the drain of passivation air passage block, and the analysis instrument of the other end and passivation air passage block enters Mouth connection;
4th solenoid valve one end is connect with the carrier gas inlet of passivation air passage block, the analysis instrument of the other end and passivation air passage block Entrance connection;
5th solenoid valve one end is connect with the carrier gas inlet of passivation air passage block, and the sample injector of the other end and passivation air passage block enters Mouth connection;
Described quantitative loop one end is connect with the sample injector entrance of passivation air passage block, the drain of the other end and passivation air passage block Connection;
The passivation air passage block uses aluminium alloy or stainless steel material, and passes through Passivation Treatment.The quantitative loop For stainless steel material, and pass through Passivation Treatment.
A kind of sample injector for environmental gas precise quantitative of the utility model further includes six control streams using operation Journey, i.e. sample phase, sample introduction stage, the cavity pressure period during pipeline-cleaning, the filter during pipeline-cleaning are anti- It blows the stage, the cavity repressurization stage during pipeline-cleaning, the quantitative loop rinse stage during pipeline-cleaning.
The sample phase, the first solenoid valve, second solenoid valve, the 4th solenoid valve are opened, third solenoid valve, the 5th electromagnetism Valve is closed, and aspiration pump is opened, environmental gas by sampler entrance via being vented after filter, quantitative loop, aspiration pump, carrier gas then by Carrier gas inlet enters analysis instrument entrance.
The sample introduction stage, the first solenoid valve, second solenoid valve, the 4th solenoid valve are closed, third solenoid valve, the 5th electromagnetism Valve is opened, and aspiration pump is closed, and carrier gas enters from carrier gas inlet, is brought the under test gas in quantitative loop into analysis instrument and is examined It surveys.
Cavity pressure period during the pipeline-cleaning, the first solenoid valve, second solenoid valve, third solenoid valve, Four solenoid valves are closed, and the 5th solenoid valve is opened, and aspiration pump is in close state, and carrier gas enters quantitative loop from carrier gas inlet, and right Cavity pressurizes.
Filter blowback stage during the pipeline-cleaning, second solenoid valve, third solenoid valve, the 4th solenoid valve close It closes, the first solenoid valve, the 5th solenoid valve are opened, and pressurization carrier gas is discharged via sample injector entrance, thus to filter blowback.
Cavity repressurization stage during the pipeline-cleaning, the first solenoid valve, second solenoid valve, third electromagnetism Valve, the 4th solenoid valve are closed, and the 5th solenoid valve is opened, and aspiration pump is in close state, and carrier gas enters quantitative loop from carrier gas inlet, And repressurization is carried out to cavity.
Quantitative loop rinse stage during the pipeline-cleaning, the first solenoid valve, third solenoid valve are closed, the 4th electromagnetism Valve is closed, and second solenoid valve, the 5th solenoid valve are opened, and pressurization carrier gas is discharged via drain, to be rinsed to quantitative loop.
The utility model has the beneficial effects that having broken the defect in existing sampling technique, a kind of micromation, mould are provided Block, low-power consumption, inexpensive sampling device, it is ensured that the accurate quantitative analysis of sample acquisition especially exists to the following analysis instrument The preprocessing system of line and portable analysers has very far-reaching reference reference significance.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram for environmental gas precise quantitative sample injector of the utility model.
Wherein:
1 --- filter;
21 --- the first solenoid valve;
22 --- second solenoid valve;
23 --- third solenoid valve;
24 --- the 4th solenoid valve;
25 --- the 5th solenoid valve;
3 --- passivation air passage block;
4 --- quantitative loop;
5 --- aspiration pump.
Specific embodiment
The utility model is further described below in conjunction with drawings and examples
A kind of sample injector (as shown in Figure 1) for environmental gas precise quantitative of the utility model includes filter 1, the One solenoid valve 21, second solenoid valve 22, third solenoid valve 23, the 4th solenoid valve 24, the 5th solenoid valve 25 are passivated air passage block 3, fixed Amount ring 4, aspiration pump 5 make piping connection and control circuit board is constituted.
Wherein, described first solenoid valve, 21 one end is connect with filter 1, and the sample injector of the other end and passivation air passage block 3 enters Mouth connection.
22 one end of second solenoid valve is connect with aspiration pump 5, and the other end is connect with the drain of passivation air passage block 3.
23 one end of third solenoid valve is connect with the drain of passivation air passage block 3, the analyzer of the other end and passivation air passage block 3 The connection of device entrance.
4th solenoid valve, 24 one end is connect with the carrier gas inlet of passivation air passage block 3, the analysis of the other end and passivation air passage block 3 The connection of instrument entrance.
5th solenoid valve, 25 one end is connect with the carrier gas inlet of passivation air passage block 3, the sample introduction of the other end and passivation air passage block 3 The connection of device entrance.
Described 4 one end of quantitative loop is connect with the sample injector entrance of passivation air passage block 3, and the other end is put with passivation air passage block 3 It eats dishes without rice or wine to connect.
The utility model includes six control flows: sample phase, sample introduction stage, the cavity pressurization during pipeline-cleaning Stage, the filter blowback stage during pipeline-cleaning, the cavity repressurization stage during pipeline-cleaning, pipeline-cleaning Quantitative loop rinse stage in the process.
Now it is described below:
Sample phase, in this process, the first solenoid valve 21, second solenoid valve 22, the 4th solenoid valve 24 are opened, third electricity Magnet valve 23, the 5th solenoid valve 25 close, aspiration pump 5 open, environmental gas by sampler entrance via filter 1, quantitative loop 4, It is vented after aspiration pump 5.Carrier gas then enters analysis instrument entrance by carrier gas inlet.
Sample introduction stage, in this process, the first solenoid valve 21, second solenoid valve 22, the 4th solenoid valve 24 close, third electricity Magnet valve 23, the 5th solenoid valve 25 are opened, and aspiration pump 5 is closed, and carrier gas enters from carrier gas inlet, by the under test gas in quantitative loop 4 Analysis instrument is brought into be detected.
Shown in the cavity pressure period during pipeline-cleaning, in this process, the first solenoid valve 21, second solenoid valve 22, third solenoid valve 23, the 4th solenoid valve 24 are closed, and the 5th solenoid valve 25 is opened, and aspiration pump 5 is in close state, carrier gas from Carrier gas inlet enters quantitative loop 4, and pressurizes to cavity.
The filter blowback stage during pipeline-cleaning, in this process, second solenoid valve 22, third solenoid valve 23, 4th solenoid valve 24 is closed, and the first solenoid valve 21, the 5th solenoid valve 25 are opened, and pressurization carrier gas is discharged via sample injector entrance, from And to sample injector entrance and filter blowback.
The cavity repressurization stage during pipeline-cleaning, in this process, the first solenoid valve 21, second solenoid valve 22, third solenoid valve 23, the 4th solenoid valve 24 are closed, and the 5th solenoid valve 25 is opened, and aspiration pump 5 is in close state, carrier gas from Carrier gas inlet enters quantitative loop 4, and carries out repressurization to cavity.
Quantitative loop rinse stage during pipeline-cleaning, in this process, the first solenoid valve of switch electromagnetic valve 21, third Solenoid valve 23 is closed, and the 4th solenoid valve 24 is closed, and second solenoid valve 22, the 5th solenoid valve 25 are opened, and carrier gas of pressurizeing is via emptying Mouth discharge, to be rinsed to quantitative loop 4.
Exist in the case where bad environments in conclusion the utility model overcomes existing sampling technique, is easy to make six Port valve or ten-way valve the pollution even defect of blocking propose a kind of micromation, modularization, low-power consumption, inexpensive sample introduction dress It sets, it is ensured that the accurate quantitative analysis of sample acquisition, stability, repeatability, to the following analysis instrument, especially online and portable point The preprocessing system of analyzer device provides solid technology material base, has very far-reaching reference reference significance.

Claims (3)

1. a kind of sample injector for environmental gas precise quantitative, which is characterized in that include filter (1), the first solenoid valve (21), second solenoid valve (22), third solenoid valve (23), the 4th solenoid valve (24), the 5th solenoid valve (25) are passivated air passage block (3), quantitative loop (4), aspiration pump (5) is connected in a manner of pipeline and control circuit is constituted;
Wherein, described first solenoid valve (21) one end is connect with filter (1), the sample injector of the other end and passivation air passage block (3) Entrance connection;
Described second solenoid valve (22) one end is connect with aspiration pump (5), and the other end is connect with the drain of passivation air passage block (3);
Described third solenoid valve (23) one end is connect with the drain of passivation air passage block (3), the other end and passivation air passage block (3) The connection of analysis instrument entrance;
4th solenoid valve (24) one end is connect with the carrier gas inlet of passivation air passage block (3), the other end and passivation air passage block (3) Analysis instrument entrance connection;
5th solenoid valve (25) one end is connect with the carrier gas inlet of passivation air passage block (3), the other end and passivation air passage block (3) Sample injector entrance connection;
Described quantitative loop (4) one end is connect with the sample injector entrance of passivation air passage block (3), the other end and passivation air passage block (3) Drain connection.
2. a kind of sample injector for environmental gas precise quantitative as described in claim 1, which is characterized in that the passivating gas Road block (3) uses aluminium alloy or stainless steel material, and passes through Passivation Treatment.
3. a kind of sample injector for environmental gas precise quantitative as described in claim 1, which is characterized in that described quantifies Ring (4) is stainless steel material, and passes through Passivation Treatment.
CN201821890201.3U 2018-11-16 2018-11-16 A kind of sample injector for environmental gas precise quantitative Active CN209280390U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821890201.3U CN209280390U (en) 2018-11-16 2018-11-16 A kind of sample injector for environmental gas precise quantitative

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821890201.3U CN209280390U (en) 2018-11-16 2018-11-16 A kind of sample injector for environmental gas precise quantitative

Publications (1)

Publication Number Publication Date
CN209280390U true CN209280390U (en) 2019-08-20

Family

ID=67601597

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821890201.3U Active CN209280390U (en) 2018-11-16 2018-11-16 A kind of sample injector for environmental gas precise quantitative

Country Status (1)

Country Link
CN (1) CN209280390U (en)

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