CN201034987Y - Gas chromatograph gas analysis twice sample introduction device - Google Patents
Gas chromatograph gas analysis twice sample introduction device Download PDFInfo
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- CN201034987Y CN201034987Y CNU200720070507XU CN200720070507U CN201034987Y CN 201034987 Y CN201034987 Y CN 201034987Y CN U200720070507X U CNU200720070507X U CN U200720070507XU CN 200720070507 U CN200720070507 U CN 200720070507U CN 201034987 Y CN201034987 Y CN 201034987Y
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Abstract
The utility model discloses a novel twice sample introduction device for gas analysis using a gas phase chromatographic instrument, comprising six-way gas valves, a three-way sample introduction tube and a connecting pipe, characterized in that: two valve holes of the two six-way gas valves forms a , one port from one six-way valve, make up an injection pipeline for measured simple via a introduction pipe of sample to be tested via a three-way sample introduction tube, and meanwhile constitutes a discharging flow path with another two valve holes of the two six-way gas valves, one valve hole of the six-way valve is connected with an analysis chromatographic column, one valve hole serves as a carrier gas inlet of a detection flow path, and the other two valve holes are communicated with a quantitative tube, so as to form the detection flow path; one valve hole of the other six-way valve is connected with the analysis chromatographic column, wherein one valve hole serves as a carrier gas inlet of the detection flow path, and the other two valve holes are communicated with the quantitative tube, so as to form another detection flow path.
Description
Technical field
The utility model relates to twice sampling device of a kind of gas chromatograph gas analysis, belongs to the component class of gas chromatograph.
Background technology
The input mode of gas chromatograph argoshield analysis generally adopts the six-way valve sampling technique, twice sample introduction analysis if desired, then need two six-way valves, sample is replaced by two six-way valves respectively, distinguishes sample introduction then, whole process operation trouble, because time swap is inconsistent, may cause problems such as leakage, absorption, introduce personal error easily, impact analysis result's accuracy.
The utility model content
The purpose of the present utility model: aim to provide a kind of novel twice input mode of gas chromatograph gas analysis, overcome the troublesome poeration that existing universal method exists, introduce shortcomings such as personal error easily.
Twice sampling device of this gas chromatograph gas analysis is made up of two gas six-way valves, threeway sample introduction pipe and connecting line, it is characterized in that:
A, described gas six-way valve are one group of synthetic six-way valve 1 of matched group and six-way valve 2, wherein the valve opening 2-6 of the valve opening 1-3 of six-way valve 1 and six-way valve 2 forms sample gas sample introduction pipelines through a threeway sample introduction pipe 3, simultaneously again with six-way valve 1, six-way valve 2 in valve opening 1-2 and valve opening 2-1 constitute and discharge stream;
The valve opening 1-5 of B, described six-way valve 1 is connected with analysis chromatographic column 4-1, and the valve opening 1-6 in the six-way valve 1 detects the stream carrier gas inlet for this, valve opening 1-1 then is communicated with valve opening 1-4 by quantity tube 5-1, forms thus to analyze the detection stream of chromatographic column 4-1;
The valve opening 2-4 of C, described six-way valve 2 is connected with analysis chromatographic column 4-2, and the valve opening 2-3 in the six-way valve 2 detects the stream carrier gas inlet for this, valve opening 2-2 then is communicated with valve opening 2-5 by quantity tube 5-2, forms thus to analyze the detection stream of chromatographic column 4-2.
Twice sampling device of this gas chromatograph gas analysis according to above technical scheme proposition, compare with twice sampling device of existing conventional gas-phase chromatograph gas analysis, overcome the defective that existing fexible unit exists, reduced operation link, thereby reduced the chance of introducing error, made accuracy of analysis greatly improve.
Description of drawings
Accompanying drawing is a structural representation of the present utility model.
1-six-way valve 1-1 among the figure~1-6 valve opening 2-six-way valve 2-1~2-6 valve opening 3-threeway sample introduction pipe 4-1~4-2 chromatographic column 5-1~5-2 quantity tube
Embodiment:
Twice sampling device of this gas chromatograph gas analysis as shown in the figure, it is to general a kind of creationary improvement of twice sampling device of gas chromatograph gas analysis at present.Twice sampling device of this gas chromatograph gas analysis, form by gas six-way valve, threeway sample introduction pipe and connecting line, it is characterized in that: described gas six-way valve is one group of synthetic six-way valve 1 of matched group and six-way valve 2, wherein the valve opening 2-6 of the valve opening 1-3 of six-way valve 1 and six-way valve 2 forms the sample introduction pipeline of samples through a threeway sample introduction pipe 3, simultaneously again with six-way valve 1, six-way valve 2 in valve opening 1-2 and valve opening 2-1 constitute and discharge stream.
The valve opening 1-5 of described six-way valve 1 is connected with analysis chromatographic column 4-1, and the valve opening 1-6 in the six-way valve 1 is this detection stream carrier gas inlet, and valve opening 1-1 then is communicated with valve opening 1-4 by quantity tube 5-1, forms thus to analyze the detection stream of chromatographic column 4-1.
The valve opening 2-4 of described six-way valve 2 is connected with analysis chromatographic column 4-2, and the valve opening 2-3 in the six-way valve 2 is this detection stream carrier gas inlet, and valve opening 2-2 then is communicated with valve opening 2-5 by quantity tube 5-2, forms thus to analyze the detection stream of chromatographic column 4-2.
The testing process of said apparatus is: during working sampling, through threeway sample introduction pipe 3, valve opening 1-3 and the 2-6 by two six-way valves enters sample then, and be quantitative through quantity tube 5-1,5-2 earlier, by valve opening 1-2, the 2-1 discharge of two six-way valves.During measurement, the carrier gas of analyzing chromatographic column 1 is entered by valve opening 1-6, and 5-1 takes away sample through quantity tube, enters chromatographic column 4-1 by valve opening 1-4,1-5, through separating, is detected by detecting device.The carrier gas of analyzing chromatographic column 4-2 is entered by valve opening 2-3, and 5-2 takes away sample through quantity tube, enters chromatographic column 4-2 by valve opening 2-5,2-4, through separating, is detected by detecting device.
Claims (1)
1. twice sampling device of a gas chromatograph gas analysis is made up of gas six-way valve, threeway sample introduction pipe and connecting line, it is characterized in that:
A, described gas six-way valve are synthetic one group of six-way valve (1) and six-way valve (2) of matched group, wherein the valve opening (2-6) of the valve opening (1-3) of six-way valve (1) and six-way valve (2) is formed sample sample introduction pipeline through a threeway sample introduction pipe (3), simultaneously again with six-way valve (1), six-way valve (2) in valve opening (1-2) and valve opening (2-1) constitute the discharge stream;
The valve opening (1-5) of B, described six-way valve (1) is connected with analysis chromatographic column (4-1), and the valve opening (1-6) in the six-way valve (1) detects the stream carrier gas inlet for this, valve opening (1-1) then is communicated with valve opening (1-4) by quantity tube (5-1), forms thus to analyze the detection stream of chromatographic column (4-1);
The valve opening (2-4) of C, described six-way valve (2) is connected with analysis chromatographic column (4-2), and the valve opening (2-3) in the six-way valve (2) detects the stream carrier gas inlet for this, valve opening (2-2) then is communicated with valve opening (2-5) by quantity tube (5-2), forms thus to analyze the detection stream of chromatographic column (4-2).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CNU200720070507XU CN201034987Y (en) | 2007-05-31 | 2007-05-31 | Gas chromatograph gas analysis twice sample introduction device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CNU200720070507XU CN201034987Y (en) | 2007-05-31 | 2007-05-31 | Gas chromatograph gas analysis twice sample introduction device |
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CN201034987Y true CN201034987Y (en) | 2008-03-12 |
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CNU200720070507XU Expired - Fee Related CN201034987Y (en) | 2007-05-31 | 2007-05-31 | Gas chromatograph gas analysis twice sample introduction device |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103869093A (en) * | 2014-03-21 | 2014-06-18 | 四川材料与工艺研究所 | Device for performing on-line quick sampling on multi-component gas and sampling method thereof |
CN105353048A (en) * | 2015-09-23 | 2016-02-24 | 南京白云化工环境监测有限公司 | Device and method for determination of non-methane total hydrocarbon by gas chromatographic analysis |
CN106053667A (en) * | 2016-07-14 | 2016-10-26 | 湘潭大学 | Multi-position hydrocarbon online detection equipment and method |
CN106841483A (en) * | 2017-02-24 | 2017-06-13 | 苏州天蓝分析仪器有限公司 | A kind of sample introduction separator of ping-pong structure |
CN111220742A (en) * | 2020-03-23 | 2020-06-02 | 中国工程物理研究院材料研究所 | Micro sample gas automatic sampling system for gas chromatography |
-
2007
- 2007-05-31 CN CNU200720070507XU patent/CN201034987Y/en not_active Expired - Fee Related
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103869093A (en) * | 2014-03-21 | 2014-06-18 | 四川材料与工艺研究所 | Device for performing on-line quick sampling on multi-component gas and sampling method thereof |
CN103869093B (en) * | 2014-03-21 | 2015-05-20 | 四川材料与工艺研究所 | Device for performing on-line quick sampling on multi-component gas and sampling method thereof |
CN105353048A (en) * | 2015-09-23 | 2016-02-24 | 南京白云化工环境监测有限公司 | Device and method for determination of non-methane total hydrocarbon by gas chromatographic analysis |
CN106053667A (en) * | 2016-07-14 | 2016-10-26 | 湘潭大学 | Multi-position hydrocarbon online detection equipment and method |
CN106841483A (en) * | 2017-02-24 | 2017-06-13 | 苏州天蓝分析仪器有限公司 | A kind of sample introduction separator of ping-pong structure |
CN111220742A (en) * | 2020-03-23 | 2020-06-02 | 中国工程物理研究院材料研究所 | Micro sample gas automatic sampling system for gas chromatography |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080312 Termination date: 20110531 |