CN209123386U - A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant - Google Patents

A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant Download PDF

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Publication number
CN209123386U
CN209123386U CN201821363916.3U CN201821363916U CN209123386U CN 209123386 U CN209123386 U CN 209123386U CN 201821363916 U CN201821363916 U CN 201821363916U CN 209123386 U CN209123386 U CN 209123386U
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China
Prior art keywords
crystallizing tank
tank
crystallizing
liquid glucose
storage tank
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CN201821363916.3U
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刘孟亚
侯卫东
岳红春
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Henan Zhenghong pharmaceutical Accessories Co., Ltd
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Henan Zhenghong Pharmaceutical Adjuvant Co Ltd
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Abstract

The utility model patent belongs to pharmaceutic adjuvant processing equipment field, specifically disclose a kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant, it include: crystallizing tank, circulating line, input duct, liquid glucose storage tank, heating device and jet chimney, liquid glucose storage tank is located at the side of the crystallizing tank, liquid glucose storage tank connects the crystallizing tank with input duct by circulating line, the heating device is mounted on the lower section of crystallizing tank, jet chimney connects the lower part of crystallizing tank, and crystallization pot bottom is provided with steam (vapor) outlet.The utility model is pumped high-temperature steam to liquid glucose storage tank by vacuum pump, since temperature is lower in liquid glucose storage tank, high-temperature steam flashes, the dissolved drip of generation is mixed with the solution in liquid glucose storage tank, and when being in certain negative pressure in crystallizing tank, the solution in liquid glucose storage tank will be entered continuously in crystallizing tank, solve the problems, such as automatic feed liquor, it more saves cost and more efficiently meets the requirement in work.

Description

A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant
Technical field
The utility model relates to the technical field of pharmaceutic adjuvant process equipment, especially a kind of crystallization for pharmaceutic adjuvant Tank automatic circulation device.
Background technique
The effects of crystallizing tank is widely used in material stirring in pharmacy and mixes, cooling freezing, finished product crystallizes, crystallizing tank is also wide It is general to be used for the industry such as dairy industry, food, chemical industry, beverage.
Existing crystallizing tank fills interior injection liquid to be crystallized toward crystallization when starting, after the completion of crystallization, crystallization Body emits, and just can be carried out crystallization next time, often injected in crystallization liquid to be crystallized reach crystallizing tank capacity and The crystal for crystallizing output is less, is not able to satisfy the requirement of production, it is necessary to and repeatedly starting crystallizing tank can be only achieved scheduled production capacity, Since the beginning in crystallization process each time can all consume a large amount of energy, the waste of energy is also resulted in.
Based on this, how to realize solve crystallizing tank in once can the more crystal of output be that those skilled in the art are current The technical issues that need to address.
Utility model content
For the problems of the prior art, the purpose of this utility model is to provide for a kind of crystallizing tank for pharmaceutic adjuvant Automatic circulation device.
In order to achieve the above object, the technical solution of the present invention is:
A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant, comprising: crystallizing tank, circulating line, input duct, sugar Liquid storage tank, heating device and jet chimney;
The liquid glucose storage tank is located at the side of the crystallizing tank, and the liquid glucose storage tank is connected by circulating line and input duct The crystallizing tank is connect, the both ends of the circulating line are separately connected the top of liquid glucose storage tank and the top of crystallizing tank, the feed liquor The both ends of pipeline are separately connected the lower part of liquid glucose storage tank and the lower part of crystallizing tank, and vacuum pump, institute are provided on the circulating line It states and is provided with circulating pump in input duct, the heating device is mounted on the lower section of crystallizing tank, the jet chimney connection crystallization The lower part of tank, the lower part of the crystallizing tank are provided with seed entrance and crystal outlet.
Further, the heating device is any one of resistive heating device and electromagnetic heater.
Further, the vapor (steam) temperature in the jet chimney is greater than the boiling point of solution in the liquid glucose storage tank.
Further, cleaning pipeline, sampler and steam (vapor) outlet are provided on the crystallizing tank, the cleaning pipeline passes through Threeway connects the jet chimney, and the steam (vapor) outlet and sampler are separately positioned on the lower part of crystallizing tank.
Further, it is respectively arranged on the cleaning pipeline, steam (vapor) outlet, seed entrance, input duct and jet chimney Butterfly valve, the butterfly valve on the jet chimney is close to crystallizing tank.
Further, the input duct, jet chimney, steam (vapor) outlet and cleaning pipeline are connect by flange with crystallizing tank.
Further, peep hole, maintenance window, pressure gauge and sampler are additionally provided on the crystallizing tank.
It further, further include bracket, the bracket is mounted on the bottom of crystallizing tank.
Compared with prior art, a kind of crystallizing tank automatic circulation device knot for pharmaceutic adjuvant provided by the utility model Structure is unusual, easy to operate, and resistive heating device heats the solution in crystallizing tank, will after solution reaches boiling point The bubble for generating boiling, can accelerate being mutually mixed for solution, keep the temperature in solution uniformly, while logical from crystallizing tank lower part The steam entered, the speed that solution can be accelerated to mix, the temperature of steam are far longer than the boiling point of the solution, are observed by peep hole When steam in pipe reaches a certain amount and the pressure value of pressure gauge is met the requirements, and opens vacuum pump, and vacuum pump is by high-temperature steam It pumps to liquid glucose storage tank, since temperature is lower in liquid glucose storage tank, high-temperature steam is flashed, the dissolved drip and liquid glucose storage tank of generation Interior solution mixing, when in crystallizing tank being in certain negative pressure, i.e., pressure gauge shows that negative pressure, opening are arranged in input duct Butterfly valve, the solution in liquid glucose storage tank will be entered continuously in crystallizing tank by input duct, and are arranged in inlet tube Circulating pump on road can according to need the process for accelerating feed liquor.The utility model solves the problems, such as automatic feed liquor, realizes crystallization In tank once can the more crystal of output, more saving cost more efficiently meet the requirement in work.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor Under, it is also possible to obtain other drawings based on these drawings.
Attached drawing 1 is a kind of structural schematic diagram of crystallizing tank automatic circulation device for pharmaceutic adjuvant.
In figure: 1. liquid glucose storage tanks, 2. circulating lines, 3. vacuum pumps, 4. peep holes, 5. cleaning pipelines, 6. jet chimneys, 7. Pressure gauge, 8. butterfly valves, 9. flanges, 10. samplers, 11. seed entrances, 12. heating devices, 13. brackets, the outlet of 14. crystal, 15. steam (vapor) outlet, 16. input ducts, 17. circulating pumps, 18. maintenance windows, 19. crystallizing tanks.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe.Obviously, the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Figure 1, a kind of crystallizing tank for pharmaceutic adjuvant as one preferred embodiment of the utility model follows automatically Loop device characterized by comprising crystallizing tank 19, circulating line 2, input duct 16, liquid glucose storage tank 1, heating device 12 and steaming Steam pipe road 6;
The liquid glucose storage tank 1 is located at the side of the crystallizing tank 19, and the liquid glucose storage tank 1 passes through circulating line 2 and feed liquor Pipeline 16 connects the crystallizing tank 19, and the both ends of the circulating line 2 are separately connected top and the crystallizing tank 19 of liquid glucose storage tank 1 Top, the both ends of the input duct 16 are separately connected the lower part of liquid glucose storage tank 1 and the lower part of crystallizing tank 19, the circulating line It is provided with vacuum pump 3 on 2, circulating pump 17 is provided in the input duct 16, the heating device 12 is mounted on crystallizing tank 19 Lower section, crystallizing tank 19 is heated, it is preferable that heating device 12 is resistive heating device, the letter of resistive heating device structure It is single, it is easy for installation, electromagnetic heater can also be selected in other embodiments, when the solution in the crystallizing tank 19 reaches boiling The bubble that boiling will be generated after point, can accelerate being mutually mixed for solution, keep the temperature in solution uniformly, in addition, described Jet chimney 6 connects the lower part of crystallizing tank 19, the steam being passed through from 19 lower part of crystallizing tank, secondary acceleration solution mixing, in this reality It applies in example, the side of the crystallizing tank 19 is provided with peep hole 4 and pressure gauge 7, is reached by the steam in 4 observation tube of peep hole A certain amount and when pressure value reaches requirement, opens vacuum pump 3, vacuum pump 3 pumps the high-temperature steam in crystallizing tank 19 to sugar In liquid storage tank 1, since temperature is lower in liquid glucose storage tank 1, high-temperature steam can be flashed, in the dissolved drip and liquid glucose storage tank 1 of generation Solution mixing, to reduce the pressure in crystallizing tank 19, when in crystallizing tank 19 being in certain negative pressure, opening is mounted on feed liquor Butterfly valve 8 on pipeline 16, the solution in the liquid glucose storage tank 1 continuously will enter crystallizing tank by input duct 16 In 19, in addition, the circulating pump 17 being arranged in input duct 16 can according to need the process for accelerating feed liquor;The crystallizing tank 19 Lower part be provided with seed entrance 11, go in crystallizing tank 19 addition primer seed, the knot for what is crystallized in pharmaceutic adjuvant The lower part of brilliant tank 19 is additionally provided with crystal outlet 14, for releasing crystal in crystallizing tank 19, in the present embodiment, the crystallizing tank Bottom the bracket 13 is installed, be used to support entire crystallizer.
Preferably, the vapor (steam) temperature in the jet chimney 6 is greater than the boiling point of solution in the liquid glucose storage tank 1, so It is able to achieve and accelerates to heat solution by heat transfer while solution mixing in crystallizing tank 19, improve efficiency, if it is temperature Degree then can absorb heat from the solution in the crystallizing tank 1 by heat transfer lower than boiling point, be unfavorable for crystallizing.
In the present embodiment, cleaning pipeline 5 and steam (vapor) outlet 15, the steam (vapor) outlet 15 are provided on the crystallizing tank 19 The bottom of crystallizing tank 19 is set, and one end of the cleaning pipeline 5 connects the jet chimney 6, other end connection by threeway The top of crystallizing tank 19, in addition, being respectively set on the cleaning pipeline 5, input duct 16, steam (vapor) outlet 15 and jet chimney 6 There is butterfly valve 8, the butterfly valve 8 on the jet chimney 6 passes through the butterfly valve 8 and cleaning pipe on control jet chimney 6 close to crystallizing tank 19 Butterfly valve 8 on road 5 is used cooperatively to control input and its input port of steam, when whole device is in crystallization work, clearly The butterfly valve 8 for washing pipeline 5 is in close state, and the butterfly valve 8 on jet chimney 6 is in the open state, and steam enters from jet chimney 6 Crystallizing tank 19 completes the heating to pharmaceutic adjuvant and realizes the circulation of whole device;After one time of crystallization, when to knot When brilliant tank 19 is cleaned, the butterfly valve 8 on jet chimney 6 is in close state, and the butterfly valve for cleaning pipeline 5 is in the open state, Steam enters crystallizing tank 19 from jet chimney 6, and 19 inner wall of crystallizing tank is cleaned in completion, by opening setting after the completion of cleaning Steam is discharged in butterfly valve 8 on the steam (vapor) outlet 15 of crystallization pot bottom.
Preferably, the circulating line 2, input duct 16, jet chimney 6, cleaning pipeline 5 pass through the connection crystallization of flange 9 Tank 19, structure is simple, easy to disassemble, easy for installation.
Preferably, it is provided with peep hole 4, maintenance window 18, pressure gauge 7 and sampler 10 on the crystallizing tank 19, sees Examining hole 4 can be in order to intuitively see the crystallization situation in crystallizing tank 19, and setting maintenance window 18 is to be able in crystallizing tank 19 go wrong after can directly by open maintenance window 18 place under repair, more convenient, pressure gauge 7 and sampler 10 can Guarantee to complete sampling flowsheet while the safety in crystallizing tank 19 and its normal operation, guarantee the crystalline quality of pharmaceutic adjuvant, It is high-efficient.
Using the above scheme, a kind of crystallizing tank automatic circulation device structure for pharmaceutic adjuvant provided by the utility model It is unusual, it is easy to operate, the solution in crystallizing tank is heated by resistive heating device, while passing through the steam pipe Road is passed through high-temperature steam to crystallizing tank, completes reheating by heat transfer, observes the steam in crystallizing tank by peep hole and reaches When to a certain amount and the pressure value of pressure gauge is met the requirements, and opens vacuum pump, and high-temperature steam is pumped to liquid glucose and stored up by vacuum pump In tank, since temperature is lower in liquid glucose storage tank, the dissolved drip that flash distillation generates occurs for high-temperature steam, in the dissolved drip and liquid glucose storage tank Solution mixing, when in crystallizing tank being in certain negative pressure, is opened and is arranged in input duct to reduce the air pressure in crystallizing tank Butterfly valve, the solution in liquid glucose storage tank will be entered continuously in crystallizing tank by input duct, and be arranged in feed liquor Circulating pump on pipeline can according to need the process for accelerating feed liquor, and this structure setting solves the problems, such as automatic feed liquor, realize In crystallizing tank once can the more crystal of output, more saving cost, more efficiently, the use in the work of satisfaction is wanted It asks.
The foregoing description of the disclosed embodiments makes those skilled in the art can be realized or use the utility model. Various modifications to these embodiments will be apparent for a person skilled in the art, general original as defined herein Reason can be realized in other embodiments without departing from the spirit or scope of the present utility model.Therefore, this is practical new Type is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase Consistent widest scope.

Claims (8)

1. a kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant characterized by comprising crystallizing tank (19), circulation pipe Road (2), input duct (16), liquid glucose storage tank (1), heating device (12) and jet chimney (6);
The liquid glucose storage tank (1) is located at the side of the crystallizing tank (19), the liquid glucose storage tank (1) by circulating line (2) and Input duct (16) connects the crystallizing tank (19), and the both ends of the circulating line (2) are separately connected the top of liquid glucose storage tank (1) Lower part and the crystallizing tank of liquid glucose storage tank (1) are separately connected with the both ends on the top of crystallizing tank (19), the input duct (16) (19) lower part is provided with vacuum pump (3) on the circulating line (2), is provided with circulating pump on the input duct (16) (17), the heating device (12) is mounted on the lower section of crystallizing tank (19), and the jet chimney (6) connects under crystallizing tank (19) Portion, the lower part of the crystallizing tank (19) are provided with seed entrance (11) and crystal outlet (14).
2. the crystallizing tank automatic circulation device according to claim 1 for pharmaceutic adjuvant, which is characterized in that the heating Device (12) is any one of resistive heating device and electromagnetic heater.
3. the crystallizing tank automatic circulation device according to claim 1 for pharmaceutic adjuvant, which is characterized in that the steam Vapor (steam) temperature in pipeline (6) is greater than the boiling point of the interior solution of the liquid glucose storage tank (1).
4. the crystallizing tank automatic circulation device according to claim 1 for pharmaceutic adjuvant, which is characterized in that the crystallization Cleaning pipeline (5), sampler (10) and steam (vapor) outlet (15) are additionally provided on tank (19), the cleaning pipeline (5) passes through three Lead to and connect the jet chimney (6), the steam (vapor) outlet (15) and sampler (10) are separately positioned under crystallizing tank (19) Portion.
5. the crystallizing tank automatic circulation device according to claim 4 for pharmaceutic adjuvant, which is characterized in that the cleaning Butterfly valve is respectively arranged on pipeline (5), input duct (16), seed entrance (11), steam (vapor) outlet (15) and jet chimney (6) (8), the butterfly valve (8) on the jet chimney (6) is close to crystallizing tank (19).
6. the crystallizing tank automatic circulation device according to claim 1 or 4 for pharmaceutic adjuvant, which is characterized in that described Input duct (16), jet chimney (6), steam (vapor) outlet (15) and cleaning pipeline (5) pass through flange (9) and crystallizing tank (19) respectively Connection.
7. the crystallizing tank automatic circulation device according to claim 1 for pharmaceutic adjuvant, which is characterized in that the crystallization Peep hole (4), maintenance window (18), pressure gauge (7) and sampler (10) are additionally provided on tank (19).
8. the crystallizing tank automatic circulation device according to claim 1 for pharmaceutic adjuvant, which is characterized in that further include branch Frame (13), the bracket (13) are mounted on the bottom of crystallizing tank (19).
CN201821363916.3U 2018-08-22 2018-08-22 A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant Active CN209123386U (en)

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CN201821363916.3U CN209123386U (en) 2018-08-22 2018-08-22 A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant

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Application Number Priority Date Filing Date Title
CN201821363916.3U CN209123386U (en) 2018-08-22 2018-08-22 A kind of crystallizing tank automatic circulation device for pharmaceutic adjuvant

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111003371A (en) * 2019-12-16 2020-04-14 沈阳化工大学 Process for preventing storage tank material from crystallizing by utilizing thermosiphon principle
CN111283839A (en) * 2019-12-11 2020-06-16 河南省科学院化学研究所有限公司 Device for straw plaiting bleaching and dyeing
CN112044102A (en) * 2020-08-31 2020-12-08 江苏康祥实业集团有限公司 A multistage evaporation plant for evaporation of sodium hypophosphite aqueous solution
CN115364735A (en) * 2022-06-20 2022-11-22 岳阳耀宁新能源科技有限公司 Paddle-free stirring system and negative electrode slurry paddle-free stirring method

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111283839A (en) * 2019-12-11 2020-06-16 河南省科学院化学研究所有限公司 Device for straw plaiting bleaching and dyeing
CN111003371A (en) * 2019-12-16 2020-04-14 沈阳化工大学 Process for preventing storage tank material from crystallizing by utilizing thermosiphon principle
CN111003371B (en) * 2019-12-16 2024-05-10 沈阳化工大学 Technology for preventing storage tank material from crystallizing by utilizing thermosiphon principle
CN112044102A (en) * 2020-08-31 2020-12-08 江苏康祥实业集团有限公司 A multistage evaporation plant for evaporation of sodium hypophosphite aqueous solution
CN112044102B (en) * 2020-08-31 2022-02-08 江苏康祥实业集团有限公司 A multistage evaporation plant for evaporation of sodium hypophosphite aqueous solution
CN115364735A (en) * 2022-06-20 2022-11-22 岳阳耀宁新能源科技有限公司 Paddle-free stirring system and negative electrode slurry paddle-free stirring method

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Address after: 456150, Henan, Anyang province Tangyin county east of the south end of the road

Patentee after: Henan Zhenghong pharmaceutical Accessories Co., Ltd

Address before: 456150, Henan, Anyang province Tangyin county east of the south end of the road

Patentee before: HENAN ZHENGHONG PHARMACEUTICAL ADJUVANT CO., LTD.

CP01 Change in the name or title of a patent holder