CN209109194U - A kind of two-phase laminated flow microdevice based on centrifugation with capillarity - Google Patents

A kind of two-phase laminated flow microdevice based on centrifugation with capillarity Download PDF

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Publication number
CN209109194U
CN209109194U CN201821490617.6U CN201821490617U CN209109194U CN 209109194 U CN209109194 U CN 209109194U CN 201821490617 U CN201821490617 U CN 201821490617U CN 209109194 U CN209109194 U CN 209109194U
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China
Prior art keywords
spiral coil
cylinder
bull
capillarity
outside
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Expired - Fee Related
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CN201821490617.6U
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Chinese (zh)
Inventor
何永清
唐丽莎
刘荣
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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Abstract

The utility model relates to a kind of based on the two-phase laminated flow microdevice being centrifuged with capillarity, belong to microfluidic art.The two-phase laminated flow microdevice based on centrifugation with capillarity, including bull snake bend, undertaking cylinder outside spiral coil and spiral coil, spiral coil outer surface is uniformly provided with several circular holes, bull snake bend one end connects propulsion device, the other end connects spiral coil entrance, each spiral coil is placed in the undertaking cylinder interior outside a spiral coil, and spiral coil access opening top passes through and accepts the undertaking bottom of cylinder of barrel top and spiral coil outlet outside spiral coil outside spiral coil, undertaking barrel top outside spiral coil, which is equipped with, accepts cylinder venthole, undertaking bottom of cylinder side outside spiral coil, which is equipped with, accepts cylinder liquid collection opening.The utility model has at low cost, high-efficient, the advantages of can carrying out multiple block combiners.

Description

A kind of two-phase laminated flow microdevice based on centrifugation with capillarity
Technical field
The utility model relates to a kind of based on the two-phase laminated flow microdevice being centrifuged with capillarity, belong to microflow control technique neck Domain.
Background technique
Microflow control technique refers to the technology that fluid is controlled under microscopic dimensions, comes across earliest 1975, wide at present It is general to be applied to bioanalysis, the fields such as drug conveying.In addition to organic synthesis, outside microreactor and chemical analysis, microflow control technique Increasingly important role is also played in field of biomedicine.The essential characteristic of micro-fluidic chip and maximum advantage are exactly more Kind monotechnics flexible combination and scale in small controllable platform is integrated, droplet coalescence can be divided and be sorted.
In recent years, Crude Oil at Sea incident of leakage constantly occurs, causes serious environmental pollution, biological death, or even thus Cause explosion, leads to casualties.There are many more petroleum to encounter the case where a large amount of water mixing in exploitation, and hardly possible exploitation, hardly possible utilizes. Apparatus of the present invention are to solve the problems, such as the immiscible material mixing difficulty separation of two-phase, using a kind of special micro-fluidic chip, base In the capillary resistance of centrifugal action and drop phase boundary surface pressure institute output, effectively continuous phase is removed from lotion, to adjust Whole droplet size ratio and speed, realize efficiently separating for two-phase fluid.
Summary of the invention
For the above-mentioned problems of the prior art and deficiency, the utility model provides a kind of based on centrifugation and capillarity Two-phase laminated flow microdevice.The utility model has at low cost, high-efficient, the advantages of can carrying out multiple block combiners.This is practical It is novel to be achieved through the following technical solutions.
A kind of two-phase laminated flow microdevice based on centrifugation with capillarity, including bull snake bend 1,2 and of spiral coil Undertaking cylinder 6 outside spiral coil, 2 outer surface of spiral coil are uniformly provided with several circular holes 3,1 one end of bull snake bend Propulsion device is connected, the other end connects 2 entrance of spiral coil, and each spiral coil 2 is placed in the circle of the undertaking outside a spiral coil Inside cylinder 6, and 2 access opening top of spiral coil pass through the top of undertaking cylinder 6 outside spiral coil and the outlet of spiral coil 2 across 6 bottom of undertaking cylinder outside spiral coil is equipped at the top of the undertaking cylinder 6 outside spiral coil and accepts cylinder venthole 7, helical disk 6 bottom side of undertaking cylinder outside pipe, which is equipped with, accepts cylinder liquid collection opening 8.
The bull snake bend 1 is horizontal positioned, and it is straight that 1 pipe diameter of bull snake bend is equal to a discrete phase drop 4 Diameter.
The length a of 1 straight pipe of bull snake bend is greater than 1 elbow diameter b of bull snake bend.
2 pipe diameter of spiral coil is equal to 1 pipe diameter of bull snake bend, and spiral coil 2 is up big and down small spiral shell Shape or the identical helical form of upper and lower size are revolved, 2 outer surface circular hole of spiral coil, 3 diameter is less than 4 diameter of discrete phase drop.
The spiral coil 2 is several, several spiral coils 2 are to be connected in series or be connected in parallel.
When several spiral coils 2 are connected in series, first 2 entrance of spiral coil of the outlet of bull snake bend 1 connection, the One spiral coil 2 outlet connection, second 2 entrance of spiral coil, and so on series connection.
When described several spiral coils 2 are in parallel, the outlet of bull snake bend 1 is equipped with several branches, branch respectively with Each 2 entrance of spiral coil connection is connected in parallel.
The working principle based on centrifugation with the two-phase laminated flow microdevice of capillarity are as follows:
The immiscible substance of the two-phase of emulsion form is injected into 1 inlet of bull snake bend, bull snake with propulsion device The effect of elbow is so that the discrete phase drop 4 reunited together is evenly distributed in continuous phase 5 in shape bend pipe 1, and process is multiple The effect of elbow, the substantially equidistant arrangement of discrete phase drop 4 before entering spiral coil 2;
Into in spiral coil 2, due to centrifugal action and capillarity, the biggish discrete phase drop 4 of density be subject to Mental and physical efforts are greater than centrifugal force close to inner tube wall (as shown in the roundel and Fig. 5 in Fig. 4), and light continuous phase 5 is close to outside Tube wall is evenly distributed with circular hole 3 on the tube wall of outside, and continuous phase 5 is because centrifugal action is thrown away from circular hole 3, by external helical disk Undertaking cylinder 6 outside pipe, which is accepted, to be collected.Discrete phase drop 4 is not easy to be thrown out of close to inside, on the other hand, due to the circle in outside 3 aperture of hole is less than 4 diameter of discrete phase drop, and discrete phase drop 4 needs to overcome caused by biggish surface tension by circular hole 3 Capillarity.Finally, most of lighter continuous phase 5 is separated from spiral coil 2, reaches higher degree, and heavier Discrete phase drop 4 and small part continuous phase 5 are enriched in the exit of spiral coil 2, can be further processed into next stage.
The beneficial effects of the utility model are:
1, utility model device combination centrifugal action, capillarity and microflow control technique manipulate fluid, so that The immiscible substance of two-phase separate ratio more thoroughly.
2, utility model device time-consuming is short, and consumptive material is few, at low cost and high-efficient.
3, utility model device is not limited to oil-water separation, as long as the liquid of two-phase incompatibility is separable, it is past Immiscible substance of three-phase etc. can be even separated afterwards, it can also be used to analyze cell separation, the fields such as chemical pharmacy.
Detailed description of the invention
Fig. 1 is the utility model plane overlooking structure figure;
Fig. 2 is the operation schematic diagram of the utility model snake bend;
Fig. 3 is the utility model spiral coil schematic perspective view A;
Fig. 4 is the utility model spiral coil plane operation schematic diagram;
Fig. 5 is the stress diagram of discrete phase drop in the utility model spiral coil;
Fig. 6 is the utility model spiral coil cascaded structure schematic diagram;
Fig. 7 is the utility model spiral coil parallel-connection structure schematic diagram;
Fig. 8 is the utility model spiral coil schematic perspective view B.
In figure: 1- bull snake bend, 2- spiral coil, 3- circular hole, 4- discrete phase drop, 5- continuous phase, 6- helical disk Undertaking cylinder outside pipe, 7- undertaking cylinder venthole, 8- undertaking cylinder liquid collection opening, the length of a- bull snake bend straight pipe, B- bull snake bend elbow diameter, F1It is the thrust that drop is subject to, F2It is the resistance that drop is subject to, F3Be drop be subject to Mental and physical efforts, F4It is the centrifugal force that drop is subject to.
Specific embodiment
With reference to the accompanying drawings and detailed description, the utility model is described in further detail.
Embodiment 1
As shown in Figures 1 to 4, the two-phase laminated flow microdevice based on centrifugation with capillarity, including bull snake bend 1, Undertaking cylinder 6 outside spiral coil 2 and spiral coil, 2 outer surface of spiral coil are uniformly provided with several circular holes 3, bull snake 1 one end of shape bend pipe connects propulsion device, and the other end connects 2 entrance of spiral coil, and each spiral coil 2 is placed in a spiral coil Inside outer undertaking cylinder 6, and 2 access opening top of spiral coil passes through 6 top of undertaking cylinder and helical disk outside spiral coil Pipe 2 exports 6 bottom of undertaking cylinder outside spiral coil, and it is logical that undertaking cylinder is equipped at the top of the undertaking cylinder 6 outside spiral coil Stomata 7,6 bottom side of undertaking cylinder outside spiral coil, which is equipped with, accepts cylinder liquid collection opening 8.
Wherein bull snake bend 1 is horizontal positioned, and it is straight that 1 pipe diameter of bull snake bend is equal to a discrete phase drop 4 Diameter;The length a of 1 straight pipe of bull snake bend is 20 ~ 40mm, and 1 elbow diameter b of bull snake bend is 1 ~ 2mm;It is described 2 pipe diameter of spiral coil is equal to 1 pipe diameter of bull snake bend, and spiral coil 2 is up big and down small helical form, shares 15 Ring, 2 outer surface circular hole of spiral coil, 3 diameter are that aperture is that 0.5 ~ 1.5mm is less than 4 diameter of discrete phase drop.
Embodiment 2
It, should be snakelike curved based on the two-phase laminated flow microdevice being centrifuged with capillarity, including bull as shown in Fig. 1 to 4 and 6 Undertaking cylinder 6 outside pipe 1, spiral coil 2 and spiral coil, 2 outer surface of spiral coil is uniformly provided with several circular holes 3, more Head 1 one end of snake bend connects propulsion device, and the other end connects 2 entrance of spiral coil, and each spiral coil 2 is placed in a spiral Inside undertaking cylinder 6 outside coil pipe, and 2 access opening top of spiral coil passes through 6 top of undertaking cylinder and spiral shell outside spiral coil Capstan pipe 2 exports 6 bottom of undertaking cylinder outside spiral coil, is equipped at the top of the undertaking cylinder 6 outside spiral coil and accepts circle Cylinder venthole 7,6 bottom side of undertaking cylinder outside spiral coil, which is equipped with, accepts cylinder liquid collection opening 8.
Wherein bull snake bend 1 is horizontal positioned, and it is straight that 1 pipe diameter of bull snake bend is equal to a discrete phase drop 4 Diameter;The length a of 1 straight pipe of bull snake bend is 20 ~ 40mm, and 1 elbow diameter b of bull snake bend is 1 ~ 2mm;It is described 2 pipe diameter of spiral coil is equal to 1 pipe diameter of bull snake bend, and spiral coil 2 is up big and down small helical form, shares 15 Ring, 2 outer surface circular hole of spiral coil, 3 diameter are that aperture is that 0.5 ~ 1.5mm is less than 4 diameter of discrete phase drop;Above-mentioned helical disk Pipe 2 is 3, several spiral coils 2 are to be connected in series, first 2 entrance of spiral coil of the outlet of bull snake bend 1 connection, First spiral coil 2 outlet connection, second 2 entrance of spiral coil, and so on series connection.
Embodiment 3
It, should be snakelike curved based on the two-phase laminated flow microdevice being centrifuged with capillarity, including bull as shown in Fig. 1 to 4 and 7 Undertaking cylinder 6 outside pipe 1, spiral coil 2 and spiral coil, 2 outer surface of spiral coil is uniformly provided with several circular holes 3, more Head 1 one end of snake bend connects propulsion device, and the other end connects 2 entrance of spiral coil, and each spiral coil 2 is placed in a spiral Inside undertaking cylinder 6 outside coil pipe, and 2 access opening top of spiral coil passes through 6 top of undertaking cylinder and spiral shell outside spiral coil Capstan pipe 2 exports 6 bottom of undertaking cylinder outside spiral coil, is equipped at the top of the undertaking cylinder 6 outside spiral coil and accepts circle Cylinder venthole 7,6 bottom side of undertaking cylinder outside spiral coil, which is equipped with, accepts cylinder liquid collection opening 8.
Wherein bull snake bend 1 is horizontal positioned, and it is straight that 1 pipe diameter of bull snake bend is equal to a discrete phase drop 4 Diameter;The length a of 1 straight pipe of bull snake bend is 20 ~ 40mm, and 1 elbow diameter b of bull snake bend is 1 ~ 2mm;It is described 2 pipe diameter of spiral coil is equal to 1 pipe diameter of bull snake bend, and spiral coil 2 is up big and down small helical form, shares 15 Ring, 2 outer surface circular hole of spiral coil, 3 diameter are that aperture is that 0.5 ~ 1.5mm is less than 4 diameter of discrete phase drop;Above-mentioned helical disk Pipe 2 is 3, several spiral coils 2 are to be connected in parallel, first 2 entrance of spiral coil of the outlet of bull snake bend 1 connection, The outlet of bull snake bend 1 is equipped with several branches, and branch connect with each 2 entrance of spiral coil be connected in parallel respectively.
Embodiment 4
As shown in figure 8, should be based on the two-phase laminated flow microdevice being centrifuged with capillarity, including bull snake bend 1, spiral Undertaking cylinder 6 outside coil pipe 2 and spiral coil, 2 outer surface of spiral coil are uniformly provided with several circular holes 3, and bull is snakelike curved 1 one end of pipe connects propulsion device, and the other end connects 2 entrance of spiral coil, and each spiral coil 2 is placed in outside a spiral coil It accepts inside cylinder 6, and 2 access opening top of spiral coil passes through at the top of the undertaking cylinder 6 outside spiral coil and spiral coil 2 goes out Mouth passes through 6 bottom of undertaking cylinder outside spiral coil, is equipped at the top of the undertaking cylinder 6 outside spiral coil and accepts cylinder venthole 7, 6 bottom side of undertaking cylinder outside spiral coil, which is equipped with, accepts cylinder liquid collection opening 8.
Wherein bull snake bend 1 is horizontal positioned, and it is straight that 1 pipe diameter of bull snake bend is equal to a discrete phase drop 4 Diameter;The length a of 1 straight pipe of bull snake bend is 20 ~ 40mm, and 1 elbow diameter b of bull snake bend is 1 ~ 2mm;It is described 2 pipe diameter of spiral coil is equal to 1 pipe diameter of bull snake bend, and spiral coil 2 is the identical helical form of upper and lower size, altogether There are 15 rings, 2 outer surface circular hole of spiral coil, 3 diameter is that aperture is that 0.5 ~ 1.5mm is less than 4 diameter of discrete phase drop.
In conjunction with attached drawing, the specific embodiments of the present invention are described in detail above, but the utility model is not Be limited to above embodiment, within the knowledge of a person skilled in the art, can also do not depart from it is practical Various changes can be made under the premise of novel objective.

Claims (7)

1. a kind of based on centrifugation and the two-phase laminated flow microdevice of capillarity, it is characterised in that: including bull snake bend (1), Undertaking cylinder (6) outside spiral coil (2) and spiral coil, spiral coil (2) outer surface are uniformly provided with several circular holes (3), bull snake bend (1) one end connects propulsion device, and the other end connects spiral coil (2) entrance, each spiral coil (2) The undertaking cylinder (6) being placed in outside a spiral coil is internal, and spiral coil (2) access opening top passes through the undertaking outside spiral coil At the top of cylinder (6) and spiral coil (2) exports undertaking cylinder (6) bottom outside spiral coil, holding outside spiral coil It connects to be equipped at the top of cylinder (6) and accepts cylinder venthole (7), undertaking cylinder (6) bottom side outside spiral coil, which is equipped with, accepts circle Cylinder liquid collection opening (8).
2. the two-phase laminated flow microdevice according to claim 1 based on centrifugation with capillarity, it is characterised in that: described more Head snake bend (1) is horizontal positioned, and bull snake bend (1) pipe diameter is equal to discrete phase drop (4) diameter.
3. the two-phase laminated flow microdevice according to claim 1 based on centrifugation with capillarity, it is characterised in that: described more The length a of head snake bend (1) straight pipe is greater than bull snake bend (1) elbow diameter b.
4. the two-phase laminated flow microdevice according to claim 1 based on centrifugation with capillarity, it is characterised in that: the spiral shell Capstan pipe (2) pipe diameter be equal to bull snake bend (1) pipe diameter, spiral coil (2) be up big and down small helical form or The identical helical form of upper and lower size, spiral coil (2) outer surface circular hole (3) diameter are less than discrete phase drop (4) diameter.
5. the two-phase laminated flow microdevice according to any one of claims 1 to 4 based on centrifugation with capillarity, feature Be: the spiral coil (2) is several, several spiral coils (2) are to be connected in series or be connected in parallel.
6. the two-phase laminated flow microdevice according to claim 5 based on centrifugation with capillarity, it is characterised in that: several When spiral coil (2) is connected in series, first spiral coil (2) entrance of bull snake bend (1) outlet connection, first spiral Coil pipe (2) outlet connection second spiral coil (2) entrance, and so on series connection.
7. the two-phase laminated flow microdevice according to claim 5 based on centrifugation with capillarity, it is characterised in that: if described When dry spiral coil (2) is in parallel, bull snake bend (1) outlet is equipped with several branches, branch respectively with each helical disk Pipe (2) entrance connection is connected in parallel.
CN201821490617.6U 2018-09-12 2018-09-12 A kind of two-phase laminated flow microdevice based on centrifugation with capillarity Expired - Fee Related CN209109194U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078662A (en) * 2018-09-12 2018-12-25 昆明理工大学 A kind of two-phase laminated flow microdevice based on centrifugation with capillarity

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078662A (en) * 2018-09-12 2018-12-25 昆明理工大学 A kind of two-phase laminated flow microdevice based on centrifugation with capillarity
CN109078662B (en) * 2018-09-12 2024-06-21 昆明理工大学 Two-phase separation micro device based on centrifugal and capillary action

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