CN208975193U - A kind of efficient distilling apparatus - Google Patents
A kind of efficient distilling apparatus Download PDFInfo
- Publication number
- CN208975193U CN208975193U CN201821120292.2U CN201821120292U CN208975193U CN 208975193 U CN208975193 U CN 208975193U CN 201821120292 U CN201821120292 U CN 201821120292U CN 208975193 U CN208975193 U CN 208975193U
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- CN
- China
- Prior art keywords
- distillation still
- distillation
- conduit
- distilling apparatus
- still ontology
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
A kind of efficient distilling apparatus, including distillation unit and the condensing unit being attached thereto by conduit, distillation unit includes distillation still ontology, and distillation still body interior is provided with rabbling mechanism, rabbling mechanism includes rotary shaft and several main blades connected thereon, if being hinged with dry plate metaplasm leaf between main blade；Distillation still ontology upper end is provided with liquidometer, pressure gauge and autoclave body thermometer, and liquidometer, pressure gauge and autoclave body thermometer are electrically connected with PLC controller, distillation still ontology and conduit joining place are formed as the frustum type from distillation still ontology to the progressive undergauge of conduit, and distillation still ontology is sequentially connected surge tank and inert gas tank.The distilling apparatus of the utility model improves distilling effect, shortens distillation process.
Description
Technical field
The utility model belongs to chemical production equipment field, and in particular to a kind of efficient distilling apparatus of oil product.
Background technique
Distillation is a kind of thermodynamic (al) separating technology, it is different using each component boiling point in mixing liquid or liquid-solid system,
Low boiling component is evaporated, then is condensed to separate the unit process of entire component, is two kinds of unit operations of evaporation and condensation
Joint.
In simple distillation system, the boiling point of oil product is higher, generally true for distilling the distilling apparatus of oil product in the market
Sky distillation when distilling inflammable low ignition point material, because of emptying suddenly, can generate large quantity of air, therefore meeting under the high temperature conditions
Cause a series of accident；Further, in distillation process, kettle internal pressure is controlled by blow valve for oxidizable substance
Power accelerates the oxidation rate of substance；Efficiently stirring is conducive to the separation of substance in distillation process, and commonly uses steam in the market
It is not satisfactory to evaporate kettle agitating device.
Summary of the invention
To solve the deficiencies in the prior art, the purpose of the present invention is to provide a kind of efficient distilling apparatus, simple steaming is provided
Evaporate system working efficiency.
In order to achieve the above objectives, the present invention adopts the following technical scheme that: a kind of efficient distilling apparatus, including distillation is single
Member and the condensing unit being attached thereto by conduit, it is characterised in that: the distillation unit includes distillation still ontology, the distillation
Kettle body interior is provided with rabbling mechanism, and the rabbling mechanism includes rotary shaft and several main blades connected thereon, the master
If being hinged with dry plate metaplasm leaf between blade；Distillation still ontology upper end is provided with liquidometer, pressure gauge and autoclave body thermometer,
And the liquidometer, pressure gauge and autoclave body thermometer are electrically connected with PLC controller, the distillation still ontology is connected with conduit
Place is formed as the frustum type from distillation still ontology to the progressive undergauge of conduit, and the distillation still ontology is sequentially connected surge tank and inertia
Gas tank.
Preferably, the condenser pipe of the condensing unit is formed as " S " type structure that head and the tail successively connect, with enhancing condensation effect
Fruit.
It is further preferred that being covered with the first insulation jacket on the outer wall of the distillation still ontology, and in the first insulation jacket
It is provided with heating tube, the heating tube and PLC are electrically connected.
It is preferred again, the second insulation jacket is covered on the outer wall of the conduit, and be provided with and add in the second insulation jacket
Heated filament, the heater strip and PLC are electrically connected.
Still further preferably, the seam of the conduit and distillation still ontology is equipped with kettle mouth thermometer, and kettle mouth temperature
Degree meter is electrically connected with PLC.
It is furthermore preferred that being formed with several through-holes on the metaplasm leaf.
Still more preferably, the metaplasm Ye Yuzhu blade is vertical, and the cross section direction of metaplasm leaf and main paddle
The angle that leaf length direction is constituted is 30-60 degree.
The utility model has the beneficial effect that the metaplasm leaf connected between 1) the main blade of the utility model increases stirring
Paddle amount of turbulence in whipping process, further, enhancing metaplasm leaf treat the shearing force of distillating liquid, improve stirring effect
Fruit accelerates distillation process；2) PLC precisely monitors liquid level and temperature in autoclave body, and passes through detected temperature and Liquid level
Heating, is conducive to temperature control, prevents temperature is excessively high from bringing impurity into condensing unit, improve purification effect；3) inert gas generation is used
It is put into air control vacuum degree for blow valve, and is filled with inert gas emptying under the high temperature conditions, to protect oxidizable combustibles
Matter avoids unexpected generation.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is partial enlarged view shown in Fig. 1.
The meaning of appended drawing reference in figure:
1- distillation still ontology, the first insulation jacket of 1-1-, 2- conduit, the second insulation jacket of 2-1-, 3- rotary shaft, the main paddle of 4-
Leaf, 5- metaplasm leaf, 5-1- through-hole, 6- pressure gauge, 7- liquidometer, 8- autoclave body thermometer, 9- kettle mouth thermometer, 10-PLC control
Device, 11- inert gas tank, 12- surge tank, 13- condenser pipe.
Specific embodiment
Specific introduce is made to the present invention below in conjunction with the drawings and specific embodiments.
As shown in Figure 1, the utility model includes distillation unit and the condensing unit that is attached thereto by conduit.
Specifically, distillation unit includes distillation still ontology 1, and distillation still ontology 1 is internally provided with rabbling mechanism, in order to improve
Mixing effect accelerates distillation process, and rabbling mechanism includes rotary shaft 3 and several main blades 4 connected thereon, between main blade 4
If being hinged with dry plate metaplasm leaf 5；Further enhancing mixing effect, as shown in Figure 2: several through-holes are formed on metaplasm leaf 5
5-1, metaplasm leaf 5 is vertical with main blade 5, and the angle that the cross section direction of metaplasm leaf 5 and main 4 length direction of blade are constituted
For 30-60 degree, through-hole 5-1 increases the amount of turbulence in whipping process, and α is that acute angle further enhances metaplasm leaf 5 to be distilled
The shearing force of liquid, so as to improve distillation efficiency.
1 upper end of distillation still ontology is provided with liquidometer 7, pressure gauge 6 and autoclave body thermometer 8, and liquidometer 7, pressure gauge 6 and
Autoclave body thermometer 8 is electrically connected with PLC controller 10, is covered with the first insulation jacket 1-1 on the outer wall of distillation still ontology 1, and
Heating tube is provided in first insulation jacket 1-1, and heating tube and PLC are electrically connected, further, in order to avoid steam is steaming
It evaporates and forms condensation between kettle ontology 1 and conduit 2, be covered with the second insulation jacket 2-1, and the second insulation jacket on the outer wall of conduit 2
Heater strip is provided in 2-1, and heater strip and PLC are electrically connected.PLC precisely monitors liquid level and temperature in autoclave body, and passes through inspection
Temperature and the Liquid level heating measured, is conducive to temperature control, prevents temperature is excessively high from bringing impurity into condensing unit, improve purifying
Effect.
Enter conduit 2 for the ease of steam, distillation still ontology 1 and 2 joining place of conduit are formed as from distillation still ontology 1 to leading
The frustum type of the progressive undergauge of pipe 2, distillation still ontology 1 are sequentially connected surge tank 12 and inert gas tank 11, are replaced with inert gas
Blow valve is put into pressure in air control kettle, and is filled with inert gas emptying under the high temperature conditions, to protect oxidizable combustibles
Matter avoids unexpected generation.
Again specifically, the condenser pipe 13 of condensing unit is formed as " S " type structure that head and the tail successively connect, to enhance condensation
Effect.
In conclusion the utility model has the advantage that the metaplasm leaf connected between 1) the main blade of the utility model increases
Agitating paddle amount of turbulence in whipping process is added, further, enhancing metaplasm leaf treats the shearing force of distillating liquid, improves
Mixing effect accelerates distillation process；2) PLC precisely monitors liquid level and temperature in autoclave body, and passes through detected temperature and liquid
Position control heating, is conducive to temperature control, prevents temperature is excessively high from bringing impurity into condensing unit, improve purification effect；3) inertia is used
Gas replaces blow valve to be put into air control vacuum degree, and is filled with inert gas emptying under the high temperature conditions, oxidizable to protect
Combustible material avoids unexpected generation.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the above embodiments do not limit the invention in any form, all obtained by the way of equivalent substitution or equivalent transformation
Technical solution is fallen within the scope of protection of the present invention.
Claims (7)
1. a kind of efficient distilling apparatus, including distillation unit and the condensing unit being attached thereto by conduit, it is characterised in that: institute
Stating distillation unit includes distillation still ontology, and the distillation still body interior is provided with rabbling mechanism, and the rabbling mechanism includes rotation
Shaft and several main blades connected thereon, if being hinged with dry plate metaplasm leaf between the main blade；On the distillation still ontology
End is provided with liquidometer, pressure gauge and autoclave body thermometer, and the liquidometer, pressure gauge and autoclave body thermometer are controlled with PLC
Device is electrically connected, and the distillation still ontology and conduit joining place are formed as the frustum from distillation still ontology to the progressive undergauge of conduit
Type, the distillation still ontology are sequentially connected surge tank and inert gas tank.
2. efficient distilling apparatus according to claim 1, it is characterised in that: headed by the condenser pipe of the condensing unit is formed
" S " type structure that tail successively connects.
3. efficient distilling apparatus according to claim 1, it is characterised in that: be covered on the outer wall of the distillation still ontology
One insulation jacket, and heating tube is provided in the first insulation jacket, the heating tube and PLC are electrically connected.
4. efficient distilling apparatus according to claim 1, it is characterised in that: be covered with the second heat preservation on the outer wall of the conduit
Collet, and heater strip is provided in the second insulation jacket, the heater strip and PLC are electrically connected.
5. efficient distilling apparatus according to claim 1 or 4, it is characterised in that: the rank of the conduit and distillation still ontology
Interface is equipped with kettle mouth thermometer, and kettle mouth thermometer and PLC are electrically connected.
6. efficient distilling apparatus according to claim 1, it is characterised in that: be formed with several through-holes on the metaplasm leaf.
7. efficient distilling apparatus according to claim 1, it is characterised in that: the metaplasm Ye Yuzhu blade is vertical, and secondary
The angle that the cross section direction of blade and main blade length direction are constituted is 30-60 degree.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821120292.2U CN208975193U (en) | 2018-07-16 | 2018-07-16 | A kind of efficient distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821120292.2U CN208975193U (en) | 2018-07-16 | 2018-07-16 | A kind of efficient distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208975193U true CN208975193U (en) | 2019-06-14 |
Family
ID=66779847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821120292.2U Expired - Fee Related CN208975193U (en) | 2018-07-16 | 2018-07-16 | A kind of efficient distilling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208975193U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111204777A (en) * | 2020-01-17 | 2020-05-29 | 中国航空工业集团公司济南特种结构研究所 | Cyanogen bromide industrialized purification process and equipment |
| CN116459540A (en) * | 2023-05-15 | 2023-07-21 | 安徽亚格盛电子新材料有限公司 | Preparation method and device of [3- (dimethylamino) propyl ] dimethyl indium |
-
2018
- 2018-07-16 CN CN201821120292.2U patent/CN208975193U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111204777A (en) * | 2020-01-17 | 2020-05-29 | 中国航空工业集团公司济南特种结构研究所 | Cyanogen bromide industrialized purification process and equipment |
| CN111204777B (en) * | 2020-01-17 | 2021-05-07 | 中国航空工业集团公司济南特种结构研究所 | Cyanogen bromide industrialized purification process and equipment |
| CN116459540A (en) * | 2023-05-15 | 2023-07-21 | 安徽亚格盛电子新材料有限公司 | Preparation method and device of [3- (dimethylamino) propyl ] dimethyl indium |
| CN116459540B (en) * | 2023-05-15 | 2023-12-22 | 安徽亚格盛电子新材料有限公司 | Preparation method and device of [3- (dimethylamino) propyl ] dimethyl indium |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190614 Termination date: 20210716 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |