CN212051287U - Volatile oil separation equipment - Google Patents
Volatile oil separation equipment Download PDFInfo
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- CN212051287U CN212051287U CN202020287056.0U CN202020287056U CN212051287U CN 212051287 U CN212051287 U CN 212051287U CN 202020287056 U CN202020287056 U CN 202020287056U CN 212051287 U CN212051287 U CN 212051287U
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- oil
- condenser
- circulation pipeline
- water separator
- separator
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 32
- 238000000926 separation method Methods 0.000 title claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 70
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 239000011521 glass Substances 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 11
- 238000004891 communication Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 5
- 238000004945 emulsification Methods 0.000 abstract description 3
- 230000006872 improvement Effects 0.000 description 8
- 235000019198 oils Nutrition 0.000 description 7
- 238000010586 diagram Methods 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 230000008676 import Effects 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000019476 oil-water mixture Nutrition 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
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Abstract
The utility model relates to a volatile oil splitter, it includes: the device comprises a reaction kettle interface, a condenser, a first circulation pipeline, an oil-water separator, a second circulation pipeline, a discharge hole and a return pipe; the reaction kettle interface is communicated with a condenser through a first tee joint, the lower part of the condenser is connected with an oil-water separator through a first circulating pipeline, the lower part of the oil-water separator is connected with a second circulating pipeline, the bottom of the second circulating pipeline is connected with a discharge hole, a stop valve is arranged on the second circulating pipeline, one end of a return pipe is connected with the oil-water separator, and the other end of the return pipe is communicated with the condenser through a tee joint; the oil-water separator comprises a separator main body and a shell, and the shell is sleeved outside the separator main body. The utility model discloses simple structure, reasonable in design, convenient operation can retrieve the water through oil water separator separation, also can solve profit emulsification problem when the separation, has improved separation efficiency greatly, is fit for using widely in the chemical industry workshop.
Description
Technical Field
The utility model relates to a chemical industry instrument and equipment technical field especially relates to a volatile oil splitter.
Background
The volatile oil is also called essential oil, and is volatile aromatic substance extracted from flower, leaf, stem, root or fruit of plant by steam distillation, extrusion, cold soaking or solvent extraction. The volatile oil has antibacterial, antiinflammatory, healing, respiratory tract immunity enhancing, sweating or fever relieving, phlegm eliminating, pathogenic wind dispelling, and stomach invigorating effects, and can be widely used in food and medicine technical field.
In the prior art, by utilizing the characteristic that volatile oil can be distilled out along with steam but is incompatible with water, oil-water mixed liquid in a reaction kettle is generally heated into steam, and the steam is introduced into a condenser for condensation and then is separated by an oil-water separator to obtain the volatile oil. However, volatile oil is separated in an actual chemical workshop, and firstly, when the oil-water mixture in the reaction kettle is heated, water needs to be added into the reaction kettle when necessary, and the water separated by the oil-water separator is wasted and cannot be recycled; secondly, the condensed volatile oil and water are easy to emulsify, so that the water and the volatile oil are not easy to separate, and the production efficiency is reduced.
SUMMERY OF THE UTILITY MODEL
The utility model aims to solve the technical problem that a volatile oil separation equipment that can retrieve the water after oil water separator separates, can solve the profit emulsification problem when separating moreover is provided.
In order to solve the above problems, the utility model adopts the following technical proposal:
a volatile oil separation apparatus, comprising: the device comprises a reaction kettle interface, a condenser, a first circulation pipeline, an oil-water separator, a second circulation pipeline, a discharge hole and a return pipe; the reaction kettle interface is communicated with the condenser through a first tee joint, the lower part of the condenser is connected with the oil-water separator through the first circulation pipeline, the lower part of the oil-water separator is connected with the second circulation pipeline, the bottom of the second circulation pipeline is connected with a discharge hole, a stop valve is arranged on the second circulation pipeline, one end of the return pipe is connected with the oil-water separator, and the other end of the return pipe is communicated with the condenser through the first tee joint;
the oil-water separator comprises a separator main body and a shell, the shell is sleeved outside the separator main body, and a cavity is formed between the shell and the separator main body; a plurality of spoilers are fixedly arranged in the cavity;
the lower part of the shell is provided with a hot liquid inlet, and the upper part of the shell is provided with a hot liquid outlet; one side of the lower part of the separator main body is communicated with the return pipe, the outer wall of the other side of the lower part of the separator main body is provided with an ultrasonic transducer, and the inner wall of the separator is provided with a horn corresponding to the ultrasonic transducer.
As a further improvement, the first circulation pipeline is communicated with the oil-water separator through a three-way joint II, the three-way joint I sequentially passes through the connecting pipe, the three-way joint II and the first circulation pipeline are communicated with the condenser.
As a further improvement of the utility model, the top of the condenser is provided with an emptying valve.
As a further improvement of the utility model, a third sight glass is arranged on the connecting pipe.
As a further improvement, the first tee joint is communicated with the top of the condenser through an air duct, and the air duct is used for introducing oil-water mixed gas into the condenser.
As a further improvement of the utility model, the outer wall of the air duct is wrapped with a heat preservation layer.
As a further improvement, the first circulation pipeline upper portion is the U type, the one end of U type pipe with the condenser intercommunication, the other end are provided with the atmospheric valve.
As a further improvement of the present invention, a first sight glass is arranged at the lower part of the first circulation pipeline, and the height of the first tee joint corresponds to the first sight glass; and a second sight glass is arranged on the second circulation pipeline and is arranged above the stop valve.
As a further improvement of the utility model, the first import of tee joint one with the back flow is connected, the second import with the reation kettle interface intercommunication, the third import with the condenser intercommunication.
Adopt the produced beneficial effect of above-mentioned technical scheme to lie in:
the utility model provides a volatile oil separation device, wherein a tee joint I is arranged at the position of a reaction kettle interface and is connected with a liquid outlet of an oil-water separator through a return pipe, and water separated by the oil-water separator is collected into the reaction kettle for recycling, so that the volatile oil separation device is energy-saving and environment-friendly; the oil-water separator is externally provided with a shell, the shell is provided with a hydrothermal solution inlet and a hydrothermal solution outlet, an ultrasonic transducer and a horn, emulsion breaking can be carried out through two modes of heating and vibrating, and the emulsified volatile oil and water are separated into layers.
The utility model can conveniently observe the state of the material in the pipeline by arranging the sight glass; the height of the first inlet of the first tee joint corresponds to the height of the sight glass on the first circulation pipeline, and the oil storage capacity of the separator is increased.
The utility model discloses simple structure, reasonable in design, convenient operation can retrieve the water through oil water separator separation, also can solve profit emulsification problem when the separation, has improved separation efficiency greatly, is fit for using widely in the chemical industry workshop.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the embodiments or the technical solutions in the prior art will be briefly described below, and it is obvious that the drawings in the following description are some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
Fig. 1 is a schematic structural diagram of embodiment 1 of the present invention.
Fig. 2 is a schematic structural diagram of embodiment 2 of the present invention.
Fig. 3 is a schematic structural diagram of the separator of the present invention.
Wherein: the system comprises a reaction kettle interface 1, a condenser 2, a condenser inlet 201, a condenser outlet 202, a first circulation pipeline 3, an oil-water separator 4, a separator main body 401, a shell 402, a hydrothermal inlet 403, a hydrothermal outlet 404, a spoiler 405, an ultrasonic transducer 406, a horn 407, a second circulation pipeline 5, a stop valve 501, a discharge port 6, a return pipe 7, a tee joint I8, a first inlet 801, a second inlet 802, a third inlet 803, a connecting pipe 9, a tee joint II 10, a third sight glass 11, a gas guide pipe 12, a vent valve 13, a first sight glass 14 and a second sight glass 15.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, the following description of the present invention with reference to the accompanying drawings and specific embodiments is provided for clarity and completeness.
Example 1
An apparatus for separating volatile oil as shown in fig. 1 and 3, comprising: the device comprises a reaction kettle interface 1, a condenser 2, a first circulation pipeline 3, an oil-water separator 4, a second circulation pipeline 5, a discharge hole 6 and a return pipe 7; the reaction kettle interface 1 is communicated with the condenser 2 through a tee joint 8, the lower part of the condenser 2 is communicated with the first circulation pipeline 3 and the oil-water separator 4, the lower part of the oil-water separator 4 is connected with the second circulation pipeline 5, the bottom of the second circulation pipeline 5 is connected with the discharge port 6, the second circulation pipeline 5 is provided with a stop valve 501, one end of a return pipe 7 is connected with the oil-water separator 4, and the other end of the return pipe is communicated with the condenser 2 through the tee joint 8. Further, a first inlet 801 of the first tee joint 8 is connected with the return pipe 7, a second inlet 802 is communicated with the reaction kettle interface 1, and a third inlet 803 is communicated with the condenser 2.
Wherein, the reaction kettle interface 1, the first circulation pipeline 3, the oil-water separator 4, the second circulation pipeline 5 and the discharge port 6 form a volatile oil separation and extraction system, and the oil-water mixed gas is condensed by the condenser 2 to become liquid which enters the oil-water separator 4 for separating and extracting volatile oil and water; the return pipe 7 and the first tee joint 8 form a recovery system, water is collected into the reaction kettle after being separated by the oil-water separator 4, and the water is continuously heated into steam which enters the volatile oil separation and extraction system for further extraction, so that energy conservation and emission reduction are facilitated.
Further, a first sight glass 14 is arranged at the lower part of the first circulation pipeline 3, and the height of the first tee joint 8 corresponds to that of the first sight glass 14, that is, the height of the first inlet 801 corresponds to that of the first sight glass 14; a second sight glass 15 is provided on the second flow channel 5, and the second sight glass 15 is provided above the shutoff valve.
As shown in fig. 3, the oil-water separator 4 includes a separator main body 401 and a housing 402, the housing 402 is sleeved outside the separator main body 401, and a cavity is formed between the housing 402 and the separator main body 401; a plurality of flow blocking plates 405 are fixedly arranged in the cavity, and further, the flow blocking plates 405 are horizontally arranged on the inner wall of the shell 402; the lower part of the shell 402 is provided with a hot liquid inlet 403, and the upper part is provided with a hot liquid outlet 404; one side of the lower part of the separator main body 401 is communicated with the return pipe 7, the outer wall of the other side is provided with an ultrasonic transducer 406, and the inner wall of the separator is provided with a horn 407 corresponding to the ultrasonic transducer 406. The outer shell 402 is arranged outside the oil-water separator 4, the hot liquid inlet 403 and the hot liquid outlet 404 as well as the ultrasonic transducer 406 and the amplitude transformer 407 are arranged on the outer shell 402, emulsion breaking can be carried out through two modes of heating and vibration, and the emulsified volatile oil and water are separated into layers.
In this embodiment, the first circulation line 3 is communicated with the oil-water separator 4 through a second three-way joint 10, and the first three-way joint 8 is communicated with the condenser 2 through an elbow, a connecting pipe 9, the second three-way joint 10 and the first circulation line 3 in sequence. And a pipeline between the first tee joint 8 and the condenser 2 is short, so that steam is prevented from condensing in the pipeline and flowing back to the reaction kettle. Further, an emptying valve 13 is arranged at the top of the condenser 2. And a third sight glass 11 is arranged on the connecting pipe 9 and used for observing the state of the oil-water mixed gas. As shown in fig. 1.
Example 2
In embodiment 2, the same reference numerals are given to the same structures as those in embodiment 1, and the same descriptions are omitted, and embodiment 2 differs from embodiment 1 only in the communication form of the first three-way joint 8 and the condenser 2.
In this embodiment, the first tee joint 8 is communicated with the top of the condenser 2 through an air duct 12, and the air duct 12 is used for introducing oil-water mixed gas into the condenser 2. Furthermore, the outer wall of the air duct 12 is wrapped with a heat-insulating layer. The heat preservation is used for preventing steam in the air duct 12 from condensing in the process of not reaching the condenser 2 and reflowing to the reaction kettle, so that the production efficiency is reduced. The upper part of the first circulation pipeline 3 is U-shaped, one end of the U-shaped pipe is communicated with the condenser 2, and the other end of the U-shaped pipe is provided with a vent valve 13. As shown in fig. 2.
When in use, the air is exhausted through the emptying valve 13, cold water is introduced into the inlet 201 of the condenser, and the cold water flows out from the outlet 202 of the condenser after being circulated; the stop valve 501 is closed, the ultrasonic transducer 406 and the amplitude transformer 407 in the oil-water separator 4 are opened or hot water is introduced into the hot water inlet 403, then the reaction kettle is heated, the oil-water mixed gas volatilized from the reaction kettle continuously flows to the oil-water separator 4 for separation after being condensed by the condenser 2, and the oil floats above the water because the density of the water is greater than that of the oil. Moreover, the height of the first inlet 801 of the first tee joint 8 corresponds to the height of the first sight glass 14; based on Bernoulli principle, the water separated by the oil-water separator 4 is continuously recycled to the reaction kettle through the return pipe 7. Along with the reaction, the oil quantity in the oil-water separator 4 is increased, and when the oil-water separator 4 is full of oil, the stop valve 501 is opened to extract water and volatile oil.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it should be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the embodiments of the present invention.
Claims (9)
1. An apparatus for separating volatile oil, comprising: the device comprises a reaction kettle interface (1), a condenser (2), a first circulation pipeline (3), an oil-water separator (4), a second circulation pipeline (5), a discharge hole (6) and a return pipe (7);
the reaction kettle connector (1) is communicated with the condenser (2) through a first tee joint (8), the lower portion of the condenser (2) is connected with the oil-water separator (4) through the first circulation pipeline (3), the lower portion of the oil-water separator (4) is connected with the second circulation pipeline (5), the bottom of the second circulation pipeline (5) is connected with a discharge hole (6), a stop valve (501) is arranged on the second circulation pipeline (5), one end of the return pipe (7) is connected with the oil-water separator (4), and the other end of the return pipe is communicated with the condenser (2) through the first tee joint (8);
the oil-water separator (4) comprises a separator main body (401) and a shell (402), wherein the shell (402) is sleeved outside the separator main body (401), and a cavity is formed between the shell (402) and the separator main body (401); a plurality of spoilers (405) are fixedly arranged in the cavity;
the lower part of the shell (402) is provided with a hot liquid inlet (403), and the upper part is provided with a hot liquid outlet (404); one side of the lower part of the separator main body (401) is communicated with the return pipe (7), the outer wall of the other side of the separator main body is provided with an ultrasonic transducer (406), and the inner wall of the separator is provided with a horn (407) corresponding to the ultrasonic transducer (406).
2. The volatile oil separation equipment according to claim 1, characterized in that the first circulation pipeline (3) is communicated with the oil-water separator (4) through a second three-way joint (10), and the first three-way joint (8) is communicated with the condenser (2) sequentially through a connecting pipe (9), the second three-way joint (10) and the first circulation pipeline (3).
3. A volatile oil separating apparatus according to claim 2, wherein the condenser (2) is provided with an air release valve (13) at the top.
4. A volatile oil separating apparatus according to claim 2, wherein a third sight glass (11) is provided on the connecting tube (9).
5. The volatile oil separation equipment according to claim 1, characterized in that the first tee joint (8) is communicated with the top of the condenser (2) through a gas guide pipe (12), and the gas guide pipe (12) is used for introducing oil-water mixed gas into the condenser (2).
6. A volatile oil separation apparatus according to claim 5 wherein the outer wall of the duct (12) is coated with a layer of insulation.
7. A volatile oil separating device according to claim 5, characterized in that the upper part of the first circulating pipeline (3) is U-shaped, one end of the U-shaped pipe is communicated with the condenser (2), and the other end is provided with an air release valve (13).
8. The volatile oil separation device according to claim 1, characterized in that a first sight glass (14) is arranged at the lower part of the first circulation pipeline (3), and the first sight glass (14) corresponds to the height of the first tee joint (8); a second sight glass (15) is arranged on the second circulation pipeline (5), and the second sight glass (15) is arranged above the stop valve (501).
9. A volatile oil separating apparatus according to claim 1, wherein the first inlet (801) of the first three-way joint (8) is connected to the return pipe (7), the second inlet (802) is in communication with the reactor interface (1), and the third inlet (803) is in communication with the condenser (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020287056.0U CN212051287U (en) | 2020-03-10 | 2020-03-10 | Volatile oil separation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020287056.0U CN212051287U (en) | 2020-03-10 | 2020-03-10 | Volatile oil separation equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212051287U true CN212051287U (en) | 2020-12-01 |
Family
ID=73531986
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202020287056.0U Active CN212051287U (en) | 2020-03-10 | 2020-03-10 | Volatile oil separation equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212051287U (en) |
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2020
- 2020-03-10 CN CN202020287056.0U patent/CN212051287U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240906 Address after: Building 4, Courtyard 2, Sihezhuang Road, Fengtai District, Beijing 100071, Floors 1-17, Unit 101, 11th Floor 1112 Patentee after: TUNGHSU TECHNOLOGY GROUP Co.,Ltd. Country or region after: China Address before: 050000 314, 3rd floor, building 10, Fangda Science Park, 266 Tianshan Street, Yuhua District, Shijiazhuang City, Hebei Province Patentee before: Shijiazhuang Ripley Health Technology Co.,Ltd. Country or region before: China |
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| TR01 | Transfer of patent right |