CN206645813U - A kind of bromine distilling apparatus - Google Patents
A kind of bromine distilling apparatus Download PDFInfo
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- CN206645813U CN206645813U CN201720224041.8U CN201720224041U CN206645813U CN 206645813 U CN206645813 U CN 206645813U CN 201720224041 U CN201720224041 U CN 201720224041U CN 206645813 U CN206645813 U CN 206645813U
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- bromine
- water
- kettle
- distilling apparatus
- condenser
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
A kind of bromine distilling apparatus, including bromine distillation still, condenser and bromine water -separating bottle, the bromine distillation still includes kettle, the axial location of the kettle is rotatablely equipped with rotating shaft, the upper end power connector of the rotating shaft has motor, lower end is provided with stirring vane, and the top of the kettle is provided with jet chimney；The inlet tube of the condenser is connected with the jet chimney, and outlet is connected with the bromine water -separating bottle；The upper portion side wall of the bromine water -separating bottle is connected with condensed water outlet pipe, and lower sides are connected with bromine discharge nozzle, the condensed water outlet pipe tieback to the top of the kettle.The utility model is adapted to the technique needs for steaming the bromine for making solvent content with bromine after product bromination, and can save process water.
Description
Technical field
It the utility model is related to technical field of chemical, more particularly to a kind of bromine distilling apparatus.
Background technology
Bromine is the volatile liquid for having intense irritation stink of brownish red, and its steam is in brownish red, and solid is in yellow green,
There is metallic luster, be important industrial chemicals, be especially widely used in industries such as medicine, chemical industry, agricultural chemicals, oil fields, mainly
For preparing bromide, medicine, fumigant, fire retardant, extinguishing chemical, fuel intermediate, chemicals, refrigerant, photosensitive material
Deng being additionally operable to bleach and sterilize.
The natural resources of bromine are primarily present in seawater, underground concentrated brine and salt lake saline, generally using concentrated seawater or
It is bittern extraction bromine, needs addition diluted acid to be acidified in the preparation process of bromine, so that pH value reaches the scope of requirement.
The Chinese patent of Application No. 201320377378.4, disclose a kind of bromine destilling tower, the outlet of heat exchanger and the heat
Exchange bittern inlet communication, the bottoms of the heat exchange layers is provided with slops outlet, the import of the heat exchanger and described
Raw brine import connects with raw brine feeding pipe.The utility model bromine destilling tower is using raw brine to being discharged
The distillation heat fallen is reclaimed, and greatly reduces the dosage of steam and chlorine, reduces production cost, and improve bromine
Yield, reduce gas discharge.
But apparatus above is not suitable for the technique rank for steaming the bromine for making solvent content with bromine after product bromination
Section, because this operation stage needs to add water, solvent is made instead of bromine with water, heats and steams bromine, distills the mistake of bromine
Journey can take part water out of.If using apparatus above, after bromine distills out part water, remaining liquid viscosity becomes big, can incite somebody to action
Deposited in destilling tower, until packing layer blocks.
Therefore, a kind of new bromine distilling apparatus is developed, not only with urgent researching value, it may have good economy
Benefit and commercial application potentiality, this is exactly where the power that the utility model is accomplished and basis.
Utility model content
The defects of in order to overcome prior art as indicated above, the present inventor has made intensive studies to this, is paying
After a large amount of creative works, so as to completing the utility model.
Specifically, technical problem to be solved in the utility model is：A kind of bromine distilling apparatus is provided, to meet to produce
The technique needs for steaming the bromine for making solvent content with bromine after product bromination.
In order to solve the above technical problems, the technical solution of the utility model is：
A kind of bromine distilling apparatus, including bromine distillation still, condenser and bromine water -separating bottle,
The bromine distillation still includes kettle, and the axial location of the kettle is rotatablely equipped with rotating shaft, the rotating shaft it is upper
End power connector has motor, and lower end is provided with stirring vane, and the top of the kettle is provided with jet chimney；
The inlet tube of the condenser is connected with the jet chimney, and outlet is connected with the bromine water -separating bottle；
The upper portion side wall of the bromine water -separating bottle is connected with condensed water outlet pipe, and lower sides are connected with bromine discharge nozzle,
The condensed water outlet pipe tieback is to the top of the kettle.
In the utility model, as a kind of perferred technical scheme, the side wall of the kettle is provided with heating oil lagging.
In the utility model, as a kind of perferred technical scheme, the condenser includes the glass tubulation of two series connection
Condenser.
In the utility model, as a kind of perferred technical scheme, the condensed water outlet pipe is provided with opening up
First U-shaped portion.
In the utility model, as a kind of perferred technical scheme, lowest part and the bromine water point of first U-shaped portion
Lowest part from bottle flushes.
In the utility model, as a kind of perferred technical scheme, the bromine discharge nozzle is provided with downward opening
Two U-shaped portions.
In the utility model, as a kind of perferred technical scheme, the bromine discharge nozzle and the bromine water -separating bottle
Junction is flush to the highest point of second U-shaped portion.
In the utility model, as a kind of perferred technical scheme, the bromine discharging pipe end is connected to bromine drying
Device.
After employing above-mentioned technical proposal, the beneficial effects of the utility model are：
The utility model includes bromine distillation still, condenser and bromine water -separating bottle, and the bromine distillation still includes kettle, institute
The axial location for stating kettle is rotatablely equipped with rotating shaft, and the upper end power connector of the rotating shaft has motor, and lower end, which is provided with, to be stirred
Blade is mixed, the top of the kettle is provided with jet chimney；The inlet tube of the condenser is connected with the jet chimney, outlet
Pipe is connected with the bromine water -separating bottle；The upper portion side wall of the bromine water -separating bottle is connected with condensed water outlet pipe, and lower sides connect
It is connected to bromine discharge nozzle, the condensed water outlet pipe tieback to the top of the kettle., will after product bromination based on this structure
When making solvent content bromine with bromine and steaming, solvent is made instead of bromine with water, it is different from the boiling point of water using bromine, in kettle
Interior heating steams bromine, distills the process of bromine and can take part water out of, using bromine water -separating bottle, the bromine steamed is cooled down and passed through
Bromine water -separating bottle is crossed, bromine and water are immiscible, can be layered, so as the process bromine of distillation steams and collects, the water taken out of
Can be more and more in bromine water shunts bottle, this part water is slowly backed into distillation still with distillation, so operation will not be because of water
Reduction influence distillation carry out, the problems such as causing solid knot wall or be fixed up；The benefit of fresh moisture content can also be reduced simultaneously
Fill, so as to save process water.
The utility model condensed water outlet pipe is provided with the first opening up U-shaped portion, the lowest part of first U-shaped portion
Flushed with the lowest part of the bromine water -separating bottle, the bromine discharge nozzle is provided with downward opening second U-shaped portion, the bromine
The junction of discharge nozzle and the bromine water -separating bottle is flush to the highest point of second U-shaped portion.Based on this structure, bromine and
The mixed liquor of condensed water can be layered in bromine water -separating bottle, and bromine can be realized using the first U-shaped portion and the second U-shaped portion
Overflow layering more preferable with condensed water, it is ensured that both separation.
In summary, the technique that the utility model is adapted to steam the bromine for making solvent content with bromine after product bromination needs
Will, and process water can be saved.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is Fig. 1 part A mplifying structure schematic diagram.
Embodiment
The utility model is further illustrated with reference to specific embodiment.But the purposes of these exemplary embodiments
Only it is used for enumerating the utility model with purpose, any type of any limit not is formed to real protection scope of the present utility model
It is fixed, it is more non-that the scope of protection of the utility model is confined to this.
As shown in figure 1, a kind of bromine distilling apparatus, including bromine distillation still, condenser 2 and bromine water -separating bottle 3, the bromine
Plain distillation still includes kettle 1, and the side wall of kettle 1 is provided with heating oil lagging 11, naturally it is also possible to electric heating chuck is provided with, it is described
The axial location of kettle 1 is rotatablely equipped with rotating shaft 12, and the upper end power connector of the rotating shaft has motor 13, and lower end is provided with
Stirring vane 14, the top of the kettle 1 are provided with jet chimney 4；The inlet tube of the condenser 2 and the jet chimney 4
Connection, outlet is connected with the bromine water -separating bottle 3, and in the present embodiment, the condenser 2 includes the glass tubulation of two series connection
Condenser, glass pipe bundle condenser can more intuitively observe water entrainment when distilling bromine than chip type condenser efficiency high
With the situation of material, the upper portion side wall of the bromine water -separating bottle 3 is connected with condensed water outlet pipe 5, and lower sides are connected with bromine
Discharge nozzle 6, the end of bromine discharge nozzle 6 are connected to bromine drier 7 and bromine are dried, the condensed water outlet pipe 5
Tieback is to the top of the kettle.When will make solvent content bromine with bromine after product bromination and steam, made of water instead of bromine
Solvent, it is different from the boiling point of water using bromine, heated in kettle and steam bromine, part can be taken out of by distilling the process of bromine
Water, using bromine water -separating bottle, bromine water -separating bottle is passed through into the bromine steamed cooling, bromine and water are immiscible, can be layered, so with
The process bromine for distillation is steamed and collected, and the water taken out of can be more and more in bromine water shunts bottle, by this part water with distillation
Slowly back into distillation still, so operation will not influence distillation progress because of the reduction of water, cause solid knot wall or stir not
The problems such as dynamic；The supplement of fresh moisture content can also be reduced simultaneously, so as to save process water, while the later stage can also be avoided to dry
Accident occurs for substantial amounts of water and sulfuric acid.
As shown in Fig. 2 bromine water -separating bottle is different from the proportion of condensed water using bromine, layering, the distilled water on upper strata are realized
Discharged by condensed water outlet pipe 5, the condensed water outlet pipe 5 is provided with the first opening up U-shaped portion 51, the first U
The lowest part in type portion 51 flushes with the lowest part of the bromine water -separating bottle, and the bromine discharge nozzle 6 is provided with downward opening
The junction of two U-shaped portions 61, the bromine discharge nozzle 6 and the bromine water -separating bottle 3 is flush to the highest of second U-shaped portion 61
Place.
It should be appreciated that the purposes of these embodiments is merely to illustrate the utility model and is not intended to limit of the present utility model
Protection domain.In addition, it should also be understood that, after technology contents of the present utility model have been read, those skilled in the art can be right
The utility model makees various change, modification and/or variation, and all these equivalent form of values equally fall within right appended by the application will
Ask within the protection domain that book limited.
Claims (8)
- A kind of 1. bromine distilling apparatus, it is characterised in that：Including bromine distillation still, condenser and bromine water -separating bottle,The bromine distillation still includes kettle, and the axial location of the kettle is rotatablely equipped with rotating shaft, and the upper end of the rotating shaft is moved Power is connected with motor, and lower end is provided with stirring vane, and the top of the kettle is provided with jet chimney；The inlet tube of the condenser is connected with the jet chimney, and outlet is connected with the bromine water -separating bottle；The upper portion side wall of the bromine water -separating bottle is connected with condensed water outlet pipe, and lower sides are connected with bromine discharge nozzle, described Condensed water outlet pipe tieback is to the top of the kettle.
- A kind of 2. bromine distilling apparatus as claimed in claim 1, it is characterised in that：The side wall of the kettle is provided with heating oil Chuck.
- A kind of 3. bromine distilling apparatus as claimed in claim 1, it is characterised in that：The condenser includes the glass of two series connection Glass pipe bundle condenser.
- A kind of 4. bromine distilling apparatus as claimed in claim 1, it is characterised in that：The condensed water outlet pipe is provided with opening The first U-shaped portion upward.
- A kind of 5. bromine distilling apparatus as claimed in claim 4, it is characterised in that：The lowest part of first U-shaped portion and institute The lowest part for stating bromine water -separating bottle flushes.
- A kind of 6. bromine distilling apparatus as claimed in claim 1, it is characterised in that：The bromine discharge nozzle is provided with opening court Under the second U-shaped portion.
- A kind of 7. bromine distilling apparatus as claimed in claim 6, it is characterised in that：The bromine discharge nozzle and the bromine water point Junction from bottle is flush to the highest point of second U-shaped portion.
- A kind of 8. bromine distilling apparatus as claimed in claim 1, it is characterised in that：The bromine discharging pipe end is connected to bromine Plain drier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720224041.8U CN206645813U (en) | 2017-03-08 | 2017-03-08 | A kind of bromine distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720224041.8U CN206645813U (en) | 2017-03-08 | 2017-03-08 | A kind of bromine distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206645813U true CN206645813U (en) | 2017-11-17 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720224041.8U Active CN206645813U (en) | 2017-03-08 | 2017-03-08 | A kind of bromine distilling apparatus |
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| CN (1) | CN206645813U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112386939A (en) * | 2021-01-20 | 2021-02-23 | 潍坊惠米农业科技发展有限公司 | Rectifying still for bromine production |
-
2017
- 2017-03-08 CN CN201720224041.8U patent/CN206645813U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112386939A (en) * | 2021-01-20 | 2021-02-23 | 潍坊惠米农业科技发展有限公司 | Rectifying still for bromine production |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220126 Address after: 261000 No. 08778, Lingang Road, Binhai District, Weifang City, Shandong Province Patentee after: WEIFANG TIANFU CHEMICAL TECHNOLOGY Co.,Ltd. Address before: 262724 Chengxin Road South First Road East, Houzhen project area, Shouguang City, Weifang City, Shandong Province Patentee before: SHOUGUANG TAIYUAN CHEMICAL Co.,Ltd. |