CN208959864U - A kind of reaction kettle convenient for adjusting temperature - Google Patents

A kind of reaction kettle convenient for adjusting temperature Download PDF

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Publication number
CN208959864U
CN208959864U CN201821478105.8U CN201821478105U CN208959864U CN 208959864 U CN208959864 U CN 208959864U CN 201821478105 U CN201821478105 U CN 201821478105U CN 208959864 U CN208959864 U CN 208959864U
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CN
China
Prior art keywords
autoclave body
heating tube
collet
cold water
reaction kettle
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821478105.8U
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Chinese (zh)
Inventor
田振江
姜国海
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Dajia Chemical Co Ltd
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Tianjin Dajia Chemical Co Ltd
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Priority to CN201821478105.8U priority Critical patent/CN208959864U/en
Application granted granted Critical
Publication of CN208959864U publication Critical patent/CN208959864U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of reaction kettles convenient for adjusting temperature, belong to chemical equipment technical field, its key points of the technical solution are that including autoclave body and top cover, feed inlet is equipped on top cover, agitating device is equipped on top cover, the autoclave body is equipped with collet, collet wraps up autoclave body, heating tube is connected on autoclave body, heating tube is put in collet, and it is fixedly connected with autoclave body, solenoid valve is fixedly connected in heating tube, cold water pipe is also fixedly connected on autoclave body, the cold water pipe being placed in outside autoclave body is equipped with control valve, achieve the effect that convenient for adjusting reactor temperature.

Description

A kind of reaction kettle convenient for adjusting temperature
Technical field
The utility model relates to a kind of field of chemical equipment, in particular to a kind of reaction kettle convenient for adjusting temperature.
Background technique
Reaction kettle is widely used in petroleum, chemical industry, rubber, pesticide, dyestuff, medicine and food etc., for completing vulcanization, nitre The pressure vessel of the process engineerings such as change, hydrogenation, hydrocarbonylation, polymerization, condensation.Material generally has carbon manganese steel, stainless steel etc., and reaction kettle is The container physically or chemically reacted, by the design of structure to container and parameter configuration, realize heating, evaporation that technique requires, The mixed function of cooling and low high speed.
In process of production, initial reaction is heated in reaction kettle, is usually heated in reaction kettle outer wall, It heats excess or heating time is inadequate, the substance in reaction kettle can be impacted, to reduce production efficiency.
Utility model content
In view of the deficienciess of the prior art, the purpose of the utility model is to provide a kind of reactions convenient for adjusting temperature Kettle achievees the effect that convenient for adjusting reactor temperature.
The above-mentioned technical purpose of the utility model has the technical scheme that
A kind of reaction kettle convenient for adjusting temperature, including autoclave body and top cover, feed inlet is equipped on top cover, is set on top cover There is agitating device, the autoclave body is equipped with collet, and collet wraps up autoclave body, heating tube is connected on autoclave body, heating tube is put in It in collet, and is fixedly connected with autoclave body, solenoid valve is fixedly connected in heating tube, cold water is also fixedly connected on autoclave body Pipe, the cold water pipe being placed in outside autoclave body are equipped with control valve.
Through the above technical solutions, raw material is added by the feed inlet on top cover, solenoid valve is then opened, into heating tube It is passed through steam or hot water, the intracorporal substance of kettle is heated, during being heated to the intracorporal substance of kettle, stirring dress It sets and constantly the intracorporal substance of kettle is stirred, the intracorporal substance of kettle is enable to be heated evenly, when the intracorporal temperature of kettle is relatively high When, solenoid valve can control the flow velocity of steam or hot water in heating tube, and the personnel of working at the same time can open manually cold water pipe, cold water pipe Into can reduce the intracorporal temperature of kettle, the intracorporal temperature of kettle is made to facilitate the heating of kettle substance in vivo, while work as the intracorporal temperature of kettle When spending relatively low, solenoid valve control increases the flow velocity of steam or hot water in heating tube, and whole process is easy to operate, while also facilitating The intracorporal temperature of kettle is adjusted, certain insulation effect is played in the setting of collet to autoclave body, reduces energy consumption.
Preferably, being fixedly connected with one layer of heat preservation layer outside the collet.
Through the above technical solutions, collet itself has certain insulation effect, the setting of insulating layer is played further Insulation effect reduces energy consumption, while certain antisepsis is played in the setting of insulating layer to collet, and that improves collet uses the longevity Life.
Preferably, the heating tube and cold water pipe apart windings are on autoclave body periphery.
Through the above technical solutions, needing to add the intracorporal substance of kettle sufficiently when heating the intracorporal substance of kettle Heat when heating tube is wrapped on autoclave body, can enable the intracorporal substance of kettle sufficiently be heated layer, to enable the intracorporal substance of kettle Enough homogeneous heatings, similarly, when cold water pipe is wrapped on autoclave body, so that the cooling velocity of kettle substance in vivo is consistent, heating tube and cold When water pipe interval is arranged, keeps the speed being heated or cooled consistent, improve the efficiency being heated or cooled.Also facilitate adjusting autoclave body simultaneously Interior temperature.
Preferably, the water outlet of the heating tube and cold water pipe is respectively positioned on the bottom of autoclave body, in heating tube and cold water pipe Water outlet is connected separately with the first outlet pipe and the second outlet pipe, is connected separately on the first outlet pipe and the second outlet pipe First control valve and the second control valve.
Through the above technical solutions, facilitating when the water outlet of heating tube and cold water pipe is located at the bottom of autoclave body by heating tube Water discharge in cold water pipe, is connected separately with the first outlet pipe and the second outlet pipe in the water outlet of heating tube and cold water pipe When, the hot water in heating tube can be passed through in boiler room and be heated again, save the energy, moreover it is possible to it reuses, it similarly, will be cold Water in water pipe is stored, and is recycled, and whole process is easy to operate, while water circulation use, reduces waste, Facilitate and adjusts the intracorporal temperature of kettle.
Preferably, first outlet pipe and the second outlet pipe are fixedly connected with observation tube close to the position of autoclave body bottom end, Observation tube is made of glass material.
Through the above technical solutions, need to drain in the water in heating tube and cold water pipe when autoclave body is not required to heating, it is convenient Next time uses, and the observation tube of the glass material of the first outlet pipe and the second water outlet pipe part facilitates staff to observe the first outlet pipe Work people is given to can determine whether the water in autoclave body in heating tube and cold water pipe drains with the flow velocity of water in the second outlet pipe It is convenient that the operation of member provides.
Preferably, the bottom end of the autoclave body is equipped with discharge nozzle.
Through the above technical solutions, the discharge nozzle of autoclave body bottom end, facilitates and the substance after reaction is discharged by discharge nozzle, together When discharge nozzle connection collet and autoclave body, it is convenient to provide to the connection of staff.
Preferably, packet is equipped with muff made of a circle rubber material on the discharge nozzle.
Through the above technical solutions, autoclave body in reaction after substance be in it is liquid, then transported down by discharge nozzle The position of one processing, since the substance after reaction is in liquid, and some substances crystalline temperature it is relatively low when, transported in discharge nozzle It is possible that crystallization, not only causes to waste, can also result in blockage to discharge nozzle in defeated process, efficiency is influenced, on discharge nozzle The muff of rubber material can effectively reduce the probability of substance crystallization, while rubber is relatively cheap, save cost, improve transmission Efficiency.
In conclusion the utility model has the following beneficial effects:
1, heating tube and solenoid valve, cold water pipe are used cooperatively, and facilitate the flow velocity of steam or hot water in control heating tube, from And facilitate the control intracorporal temperature of kettle;
2, muff and insulating layer are used cooperatively, and are had certain insulation effect to the intracorporal substance of kettle, are reduced energy consumption.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the winding state diagram that heating tube and cold water pipe are aimed to show that after hiding collet;
Fig. 3 is intended to show partial structural diagram when muff on discharge nozzle.
In figure, 1, autoclave body;2, top cover;21, agitating device;22, feed inlet;3, collet;31, insulating layer;4, heating tube; 41, solenoid valve;5, cold water pipe;51, control valve;6, the first outlet pipe;61, the first control valve;7, the second outlet pipe;71, second Control valve;8, observation tube;9, discharge nozzle;91, muff.
Specific embodiment
The utility model is described in further detail below in conjunction with attached drawing.The wherein identical attached drawing of identical components Label indicates.It should be noted that word "front", "rear" used in the following description, "left", "right", "up" and "down" refer to It is the direction in attached drawing, word " bottom surface " and " top surface ", "inner" and "outside" are referred respectively to towards or away from particular elements geometry The direction at center.
A kind of reaction kettle convenient for adjusting temperature, as shown in Figure 1, including autoclave body 1, top cover 2, agitating device 21,3 and of collet Heating tube 4, top cover 2 are fixedly connected with the opening of autoclave body 1, and agitating device 21 is fixedly connected with the top of top cover 2, and are located at top On the center line of lid 2, feed inlet 22 is offered on top cover 2, collet 3 is fixedly connected with autoclave body 1, heating tube 4 be located at collet 3 with Between autoclave body 1, and it is fixedly connected with 1 outer wall of autoclave body.
The shape of collet 3 is consistent with the shape of autoclave body 1 combined with Figure 1 and Figure 2, is wrapped in collet 3 on autoclave body 1, and makes to press from both sides There are cavitys between set 3 and autoclave body 1, and heating tube 4 is wrapped in the outer wall of autoclave body 1 after passing through collet 3, and fixes with 1 outer wall of autoclave body Connection, along the axial direction of autoclave body 1, heating tube 4 is wound with multi-turn, the height and autoclave body of the number of total coils that heating tube 4 is wound on autoclave body 1 1 height is suitable, is fixedly connected with solenoid valve 41 in the heating tube 4 being located at outside autoclave body 1, is connected with cold water pipe on autoclave body 1 5, cold water pipe 5 is wrapped on 1 outer wall of autoclave body after passing through collet 3 and is fixedly connected with 1 outer wall of autoclave body, between cold water pipe 5 and heating tube 4 Every setting, control valve 51 is fixedly connected on the cold water pipe 5 being located at outside autoclave body 1.
Fig. 1 is reviewed, further, is fixedly connected with one layer of heat preservation layer 31 in 3 outer wall of collet.
In use, raw material is added in autoclave body 1 by the feed inlet 22 on top cover 2, then by the lid on feed inlet 22 Close, open solenoid valve 41, steam or hot water are entered in heating tube 4, and enter in the heating tube 4 in collet 3, to autoclave body 1 into Row heating, while starting agitating device 21 and the substance in autoclave body 1 is stirred, make its homogeneous heating, since heating tube 4 is wound In 1 outer wall of autoclave body, the substance in autoclave body 1 can be made to be heated evenly, while the circle number that heating tube 4 is wound is suitable with the height of autoclave body 1 When, more facilitate the heating of substance in autoclave body 1, thus guarantee the efficiency of heating, when the temperature in autoclave body 1 is relatively high, electricity Magnet valve 41 controls the flow of hot water or steam in heating tube 4, while opening the control valve 51 on cold water pipe 5 manually, infuses cold water Enter in the cold water pipe 5 between collet 3 and autoclave body 1, so that the temperature in autoclave body 1 be made to reduce, guarantees the substance energy in autoclave body 1 Enough abundant reactions, while when heating tube 4 and the setting of the interval of cold water pipe 5, the rate that autoclave body 1 can be made to cool down is consistent, thus reduction pair The setting of the influence of substance in autoclave body 1,3 outer wall insulating layer 31 of collet both played a certain protective role collet 3, while also rising To certain insulation effect, heat loss is reduced.
As shown in Figure 1, the water outlet of heating tube 4 and cold water pipe 5 is respectively positioned on the bottom of collet 3, in the water outlet of heating tube 4 Place is fixedly connected with the first outlet pipe 6, is fixedly connected with the second outlet pipe 7, the first outlet pipe 6 in the water outlet of cold water pipe 5 It is pierced by collet 3 with the second outlet pipe 7, the first control valve 61 is fixedly connected on the first outlet pipe 6, in the second outlet pipe 7 On be fixedly connected with the second control valve 71.
Further, observation tube is fixedly connected to close to the position of collet 3 in the first outlet pipe 6 and the second outlet pipe 7 8, observation tube 8 is made of glass material.
After the completion of the substance reaction in autoclave body 1, needs to drain in the water in heating tube 4 and cold water pipe 5, facilitate make next time With opening the first control valve 61 and the second control valve 71 at this time, the water in heating tube 4 and cold water pipe 5 constantly passes through the first water outlet Pipe 6 and the discharge of the second outlet pipe 7, staff can pass through the judgement of observation tube 8 heating on the first outlet pipe 6 and the second outlet pipe 7 Whether the water in water and cold water pipe 5 in pipe 4 drains, and it is convenient to provide to the operation of staff, while also saving the time, the Water in one outlet pipe 6 and the second outlet pipe 7 is Ke Xunhuanliyong, reduces waste.
As shown in figure 3, being fixedly connected with discharge nozzle 9 in 3 bottom end of collet, packet is equipped with the guarantor of rubber material on discharge nozzle 9 Temperature set 91.
Different types of substance can be reacted in autoclave body 1, the substance after reaction is discharged and then is carried out next by discharge port A processing, but the crystalline temperature of some substances is relatively low, crystallization is easy during discharge nozzle 9 transports, to will cause out Expects pipe 9 blocks, so the muff 91 of rubber material can effectively reduce the probability of crystallization on discharge nozzle 9, improves the efficiency of transmission.
The utility model use process is as follows:
Raw material is added by the enterprising material mouth 22 of top cover 2, then starts agitating device 21 and it is stirred, open simultaneously electromagnetism Valve 41, which makes to be passed through steam or hot water in heating tube 4, heats 1 outer wall of autoclave body, when the temperature is excessively high, opening control in autoclave body 1 Valve 51 in the cold water pipe 5 for entering cold water between collet 3 and autoclave body 1, cools down to autoclave body 1, raw material reacts in autoclave body 1 Afterwards, the substance in autoclave body 1 is discharged by discharge nozzle 9, is opening the first control valve 61 and the second control valve 71, is making 3 He of collet The water in heating tube 4 and cold water pipe 5 between autoclave body 1 is discharged by the first outlet pipe 6 and the second outlet pipe 7, whole process behaviour Make simply, the setting of heating tube 4 and cold water pipe 5 facilitates the temperature adjusted in autoclave body 1, and it is convenient to provide to the operation of staff.
This specific embodiment is only the explanation to the utility model, is not limitations of the present invention, ability Field technique personnel can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but As long as all by the protection of Patent Law in the scope of the claims of the utility model.

Claims (7)

1. a kind of reaction kettle convenient for adjusting temperature, including autoclave body (1) and top cover (2), are equipped with feed inlet on top cover (2) (22), agitating device (21) are equipped on top cover (2), it is characterised in that: the autoclave body (1) is equipped with collet (3), collet (3) Autoclave body (1) is wrapped up, is connected on autoclave body (1) heating tube (4), heating tube (4) is put in collet (3), and solid with autoclave body (1) Fixed connection, solenoid valve (41) are fixedly connected on heating tube (4), cold water pipe (5) are also fixedly connected on autoclave body (1), are set Control valve (51) are equipped in the cold water pipe (5) of autoclave body (1) outside.
2. a kind of reaction kettle convenient for adjusting temperature according to claim 1, it is characterised in that: the collet (3) is solid outside Surely one layer of heat preservation layer (31) are connected with.
3. it is according to claim 1 it is a kind of convenient for adjust temperature reaction kettle, it is characterised in that: the heating tube (4) and Cold water pipe (5) apart windings are on autoclave body (1) periphery.
4. it is according to claim 1 it is a kind of convenient for adjust temperature reaction kettle, it is characterised in that: the heating tube (4) and The water outlet of cold water pipe (5) is respectively positioned on the bottom of autoclave body (1), is separately connected in the water outlet of heating tube (4) and cold water pipe (5) There are the first outlet pipe (6) and the second outlet pipe (7), is connected separately with first on the first outlet pipe (6) and the second outlet pipe (7) Control valve (61) and the second control valve (71).
5. a kind of reaction kettle convenient for adjusting temperature according to claim 4, it is characterised in that: first outlet pipe (6) it is fixedly connected with observation tube (8) with the second outlet pipe (7) close to the position of autoclave body (1) bottom end, observation tube (8) is by glass material Matter is made.
6. a kind of reaction kettle convenient for adjusting temperature according to claim 1, it is characterised in that: the bottom of the autoclave body (1) End is equipped with discharge nozzle (9).
7. a kind of reaction kettle convenient for adjusting temperature according to claim 6, it is characterised in that: on the discharge nozzle (9) Packet is equipped with muff (91) made of a circle rubber material.
CN201821478105.8U 2018-09-11 2018-09-11 A kind of reaction kettle convenient for adjusting temperature Expired - Fee Related CN208959864U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821478105.8U CN208959864U (en) 2018-09-11 2018-09-11 A kind of reaction kettle convenient for adjusting temperature

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821478105.8U CN208959864U (en) 2018-09-11 2018-09-11 A kind of reaction kettle convenient for adjusting temperature

Publications (1)

Publication Number Publication Date
CN208959864U true CN208959864U (en) 2019-06-11

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114100555A (en) * 2021-12-02 2022-03-01 扬州金珠树脂有限公司 Resin polymerization temperature control device
CN114315681A (en) * 2021-12-31 2022-04-12 江苏同禾药业有限公司 High-yield preparation method of brivaracetam

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114100555A (en) * 2021-12-02 2022-03-01 扬州金珠树脂有限公司 Resin polymerization temperature control device
CN114315681A (en) * 2021-12-31 2022-04-12 江苏同禾药业有限公司 High-yield preparation method of brivaracetam

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20190611

Termination date: 20210911