CN208915934U - A kind of higher boiling chemical reagent purification filling apparatus - Google Patents
A kind of higher boiling chemical reagent purification filling apparatus Download PDFInfo
- Publication number
- CN208915934U CN208915934U CN201821778301.7U CN201821778301U CN208915934U CN 208915934 U CN208915934 U CN 208915934U CN 201821778301 U CN201821778301 U CN 201821778301U CN 208915934 U CN208915934 U CN 208915934U
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- Prior art keywords
- chemical reagent
- evaporator
- filling apparatus
- capping
- temperature
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Abstract
The utility model relates to chemical reagent to purify filling apparatus technical field, specifically a kind of higher boiling chemical reagent purifies filling apparatus, including pedestal and evaporator and fluid reservoir, the evaporator and fluid reservoir are fixedly welded respectively at left and right sides of pedestal top, the evaporator top is fixed with capping, the capping upper middle position is equipped with servo motor, the servo motor output end is connected with agitating shaft by shaft joint, the agitating shaft bottom end is also welded with the filtration members of annular setting in pairs up and down, the filtration members include the interior plectane and excircle board of hollow setting, heating efficiency is lower and dust removal rate is higher: heating rod is rotated during heating by the servo motor drive agitating shaft being electrically connected with external city, to drive stirring blade to carry out the rotation of different angle, so that Chemical reagent is uniformly heated, and purification effect is more preferably.
Description
Technical field
The utility model relates to chemical reagent to purify filling apparatus technical field, specifically a kind of higher boiling chemistry examination
Agent purifies filling apparatus.
Background technique
The chemical reagent of domestic liquid type is mainly based on packing, strict demand due to chemical reagent to product index,
The standard of packing is not achieved in many raw materials, it is necessary to be purified.The chemical reagent of common liq class can be by way of distillation
It purifies, can but encounter problems to the purification of high boiling liquid, such as existing heating method is that steam heats, vapor (steam) temperature
It is difficult to reach the evaporating temperature of material at 120-150 DEG C, purchase equipment need to be led using electric heating, and the chemical reagent of liquid type is more
For flammable liquid, equipment safety grade need to be greatly improved；Production batch is small, so laboratory preparation can only be used, but laboratory
Preparation method yield is too low and does not catch up with the needs in market, and chemical reagent is wide in variety, it is impossible to accomplish that a set of equipment only produces a product
Kind, multi-purpose content, an object multipotency are needed, the equipment junction purchased in the market is to be fixedly connected, and dismounting is inconvenient, is not easy clear
It washes, existing production model is that workshop will be packed into big packaging after the purification of high boiling liquid chemical reagent, then send to packaging vehicle
Between carry out filling, since high boiling liquid chemical reagent freezing point is also high, has often just solidified or become when sending to packing shop
It is sticky, can only be heated to certain temperature again makes that it melts or viscosity reduction carries out filling again, reduces efficiency, increases energy
Consumption.
In this regard, number of patent application is that CN201620987087.0 proposes a kind of purification of higher boiling chemical reagent, filling one
Body formula equipment, including bottom plate, the upper surface of the bottom plate are equipped with evaporator, and the bottom of evaporator is equipped with heater strip, heater strip
Top is equipped with heating plate, and the upper end of the evaporator is equipped with evaporation lid, and the lower end for evaporating lid is equipped with temperature sensor, by adding
Heated filament gives chemical reagent heating, more uniform when making heating chemical reagents by heating plate, is provided with temperature in evaporation lid and passes
Sensor and humidity sensor detect temperature when evaporating by temperature sensor, are released the pressure in evaporator by relief tube
It runs out, prevents to explode, liquid is converted into the Gas chemistries flashed to by cooling tube, so that cooling is more square
Just, above scheme structure is simple, easy to clean, and purification is integrated the efficiency for improving work with filling, saves a large amount of energy
Source.
But there is also defects in use for above scheme:
1. heating efficiency is lower and lacks filter mechanism: heater strip, evaporation only is arranged in evaporation pot bottom in above scheme
Lack stirring structure inside tank, it is lower so as to cause internal chemical reagent heat conduction efficiency, and then lead to the purifying of chemical reagent
Efficiency is lower, while lacking the mechanism that can be filtered the solid impurity mixed in liquid in above scheme, thus inconvenient
It is quickly cleaned in by evaporator；
2. cooling effect is less desirable: above scheme exports the reagent after evaporation by U-shaped conduit, but exports
Distance is relatively short, lower so as to cause cooling efficiency.
Utility model content
In order to make up the above deficiency, the utility model provides a kind of higher boiling chemical reagent purification filling apparatus, with solution
The problems in certainly above-mentioned background technique.
The technical solution of the utility model is: a kind of higher boiling chemical reagent purification filling apparatus, including pedestal and evaporation
Tank and fluid reservoir, the evaporator and fluid reservoir are fixedly welded respectively at left and right sides of pedestal top, on the evaporator
Portion is fixed with capping, and the capping upper middle position is equipped with servo motor, and the servo motor output end passes through company
Axis device is connected with agitating shaft, and the agitating shaft bottom end is also welded with the filtration members of annular setting in pairs up and down, and the filtration members are equal
It include the interior plectane and excircle board of hollow setting, by being placed equidistant with CARBURIZING FURNACE FOR STAINLESS FASTENER between the interior plectane and excircle board
Nail is equipped with filter screen, the interior plectane and agitating shaft bottom end outer wall and is installed fixed (not shown) by screw, and the evaporation
Top tank structure, which is offered, slips matched annular opening slot with excircle board side, and agitating shaft outer wall side is equidistantly welded with difference
Upward with the stirring blade of lower section, bottom is equipped with heating rod in the evaporator, and heating rod uses model HY-DT-
10 industry heating stick, the capping top are plugged with conduit, and the conduit and the activity grafting of fluid reservoir upper end, the conduit
Outer wall has also been arranged in pairs cooling tube, and the fluid reservoir bottom right side is communicated with the drain pipe for being equipped with gate valve.
In this setting
1. heating efficiency is lower and dust removal rate is higher: heating rod heating during by being electrically connected with external city
Servo motor drive agitating shaft rotated, thus drive stirring blade carry out different angle rotation so that
Chemical reagent is uniformly heated, and purification effect more preferably, during purifying, is arranged between interior plectane and excircle board by having
Filter screen can be filtered removing to the solid particle in chemical reagent, reduce impurity inside subsequent cleaning evaporator
Time；
2. cooling efficiency is preferable: in flow process, conduit is vertical section and tilting section, is conveyed so as to lengthen
Journey, i.e., cooling distance, cooperates the setting of cold water storage cistern ontology and water pump can in cooling distance by the cooling tube being arranged in pairs
Vapor in acceleration duct is cooled to liquid, to preferably flow to inside fluid reservoir.
Preferably, the pedestal top is also equipped with cold water storage cistern ontology, and the cold water storage cistern body upper part is also equipped with water pump,
The model TS45-01 of water pump, water pump water delivery end are communicated with into water main pipeline, and the water inlet main pipeline is connected by tee tube
It is connected with into water subtube, and two water inlet subtubes are connected on the left of cooling tube, and the cooling pipe outer wall bottom is also
It is communicated with the water return pipeline being connected to cold water storage cistern ontology.
This setting drives the intrinsic cold water of cold water storage cistern to flow on the left of cold water pipe by the water pump being electrically connected with external city
It moves to inside it, then flows diagonally downward, then be back in cold water storage cistern ontology again from water return pipeline.
Preferably, the shape of the conduit is that vertical section and tilting section are staggered, and the vertical section and tilting section it
Between angle be 80 degree, and two cooling tubes are all set on the outside of the tilting section of conduit, and the conduit is also equipped with hand
Dynamic valve.
This setting is staggered by vertical section and tilting section and can lengthen the distance of conduit, to lengthen cooled
Journey.
Preferably, Temperature Humidity Sensor is installed on the left inside wall of capping, the capping upper left end passes through screw
Temperature and humidity controller is installed, the Temperature Humidity Sensor passes through conducting wire respectively and is electrically connected at temperature and humidity controller, temperature and humidity
Controller is electrically connected with the external city 220V, and the temperature and humidity controller is also electrically connected at heating rod, the Temperature and Humidity Control
The multi-way intelligence temperature and humidity controller for the model CD195X-9M7 that device uses, the model that the Temperature Humidity Sensor uses
The Temperature Humidity Sensor of RS-WS-N01-2.
Preferably, the capping upper left-hand is communicated with relief pipeline, is also fixedly installed with valve on the relief pipeline.
Preferably, the capping upper left-hand is also communicated with charging line, and the charging line top is threaded with end
Lid.
Preferably, the liquid storage tank wall is fixedly welded with aluminium base cooling fin, and the fluid reservoir and evaporation tank wall are equal
Embedded with form.
This setting further can carry out cooling and heat dissipation to the liquid inside liquid reserve tank by aluminium base cooling fin, pass through view
The case where setting of window is convenient for observation evaporator and liquid storage pot liquid.
Preferably, the base bottom is fixedly installed with Self-locking universal wheel, and the chassis left side is fixedly installed with and pushes away
?.
This setting is convenient for moving whole device by the setting of Self-locking universal wheel, and convenient transfer is to be made
User offers convenience, and Self-locking universal wheel driving device can be assisted to be moved by the setting of handle.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property
It puts, is also possible to obtain other drawings based on these drawings.
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is partial enlargement structural representation at the A in the utility model Fig. 1；
Fig. 3 is the utility model evaporator external front face structural schematic diagram；
Fig. 4 is the utility model agitating shaft and its component structure diagram；
Fig. 5 is the utility model parts of vessels structural schematic diagram；
Fig. 6 is the electrical connection schematic diagram of the utility model temperature and humidity controller.
Wherein, appended drawing reference is summarized as follows: 1 pedestal, 2 evaporators, 3 fluid reservoirs, 4 cappings, 5 agitating shafts, plectane in 6, outside 7
Plectane, 8 servo motors, 9 filter screens, 10 annular opening slots, 11 stirring blades, 12 heating rods, 13 conduits, 131 vertical sections, 132
Tilting section, 14 cooling tubes, 15 drain pipes, 16 cold water storage cistern ontologies, 17 water pumps, 18 water inlet main pipelines, 19 water inlet subtubes, 20 return water
Pipeline, 21 Temperature Humidity Sensors, 22 temperature and humidity controllers, 23 relief pipelines, 24 charging lines, 25 aluminium base cooling fins, 26 forms,
27 Self-locking universal wheels.
Specific embodiment
The utility model is further illustrated in the following with reference to the drawings and specific embodiments.
With reference to Fig. 1-6 it is found that a kind of higher boiling chemical reagent of the utility model purifies filling apparatus, including pedestal 1 and steaming
Tank 2 and fluid reservoir 3 are sent out, the evaporator 2 and fluid reservoir 3 are fixedly welded respectively at left and right sides of 1 top of pedestal, the steaming
Hair 2 top of tank is fixed with capping 4, and 4 upper middle positions of the capping are equipped with servo motor 8, and the servo motor 8 is defeated
Outlet is connected with agitating shaft 5 by shaft joint, and 5 bottom end of agitating shaft is also welded with the filtration members of annular setting in pairs up and down,
The filtration members include the interior plectane 6 and excircle board 7 of hollow setting, by equidistant between the interior plectane 6 and excircle board 7
It is provided with CARBURIZING FURNACE FOR STAINLESS FASTENER nail and filter screen 9, the interior plectane 6 and interior plectane 6 described in agitating shaft 5 and 5 bottom end of agitating shaft is installed
Outer wall is installed by screw and is fixed, and 2 inner wall of the evaporator offers and slips matched annular opening slot with 7 side of excircle board
10, the 5 outer wall side of agitating shaft is equidistantly welded with the stirring blade 11 above and below being respectively facing, in the evaporator 2
Bottom is equipped with heating rod 12, and 4 tops of the capping are plugged with conduit 13, and the conduit 13 and 3 upper end activity of fluid reservoir are inserted
It connects, 13 outer wall of conduit has also been arranged in pairs cooling tube 14, and 3 bottom right side of fluid reservoir is communicated with the row for being equipped with gate valve
Liquid pipe 15.1 top of pedestal is also equipped with cold water storage cistern ontology 16, and 16 top of cold water storage cistern ontology is also equipped with water pump 17,
The 17 water delivery end of water pump is communicated with into water main pipeline 18, and the water inlet main pipeline 18 is communicated with by tee tube into water subtube
19, and two water inlet subtubes 19 are connected to 14 left side of cooling tube, and 14 outer wall bottom of the cooling tube is also connected to
There is the water return pipeline 20 being connected to cold water storage cistern ontology 16.The shape of the conduit 13 is that vertical section 131 and tilting section 132 are staggeredly set
It sets, and the angle between the vertical section 131 and tilting section 132 is 80 degree, and two cooling tubes 14 are all set in and lead
132 outside of tilting section of pipe 13, the conduit 13 are also equipped with hand-operated valve.Temperature and humidity biography is installed on 4 left inside walls of the capping
Sensor 21,4 upper left ends of the capping are equipped with temperature and humidity controller 22 by screw, and the Temperature Humidity Sensor 21 is distinguished
It is electrically connected at temperature and humidity controller 22 by conducting wire, the temperature and humidity controller 22 is also electrically connected at heating rod 12, described
The multi-way intelligence temperature and humidity controller for the model CD195X-9M7 that temperature and humidity controller 22 uses, the Temperature Humidity Sensor 21
The Temperature Humidity Sensor 21 of the model RS-WS-N01-2 of use.4 upper left-hands of the capping are communicated with relief pipeline 23, institute
It states and is also fixedly installed with valve on relief pipeline 23.4 upper left-hands of the capping are also communicated with charging line 24, the liquid-feeding tube
24 top of road is threaded with end cap.3 outer wall of fluid reservoir is fixedly welded with aluminium base cooling fin 25, and 3 He of the fluid reservoir
2 outer wall of evaporator is embedded with form 26.1 bottom of pedestal is fixedly installed with Self-locking universal wheel 27, and 1 left side of the pedestal
It is fixedly installed with handle.
Chemical reagent to be purified is thrown in evaporator 2 when implementing by charging line 24 by the present embodiment
Portion, 2 inner top of evaporator are equipped with heating rod 12, control heating rod 12 by temperature and humidity controller 22 and add to chemical reagent
Heat during heating, drives agitating shaft 5 to be rotated, to drive by the servo motor 8 being electrically connected with external city
Stirring blade 11 carries out the rotation of different angle so that chemical reagent is uniformly heated, purification effect more preferably,
During purifying, by there is the filter screen 9 being arranged between interior plectane 6 and excircle board 7 can be to the solid in chemical reagent
Grain is filtered removing, reduces the time of subsequent cleaning 2 inside impurity of evaporator, while during heating by temperature and humidity
Sensor 21 incudes the temperature and humidity in evaporator 2, and inductive signal is transmitted to temperature and humidity controller 22, temperature and humidity control
Display screen is come on device 22 processed, so that chemical reagent can be not achieved in temperature according to the data manipulation person of display screen display
Boiling point when, the pressure in evaporator 2 is shed by the valve beaten on relief pipeline 23, when temperature reaches the boiling of chemical reagent
Point and air humidity it is big when, by open conduit 13 on hand-operated valve close relief pipeline 23 on valve so that steam
Flowed in fluid reservoir 3 from conduit 13, in flow process, conduit 13 be vertical section 131 and tilting section 132, so as to
Transmission process is lengthened, i.e., cooling distance cooperates 16 He of cold water storage cistern ontology by the cooling tube 14 being arranged in pairs in cooling distance
The vapor that the setting of water pump 18 can speed up in conduit 13 is cooled to liquid, to preferably flow to inside fluid reservoir 3, passes through
The setting of drain pipe 15 and gate valve is convenient for the liquid in fluid reservoir 3 carrying out discharge use.
The advantages of basic principles and main features and the utility model of the utility model have been shown and described above.Current row
The technical staff of industry is described in above embodiments and description it should be appreciated that the present utility model is not limited to the above embodiments
Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also
It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.The utility model
Claimed range is defined by the appending claims and its equivalent thereof.
Claims (8)
1. a kind of higher boiling chemical reagent purifies filling apparatus, including pedestal (1) and evaporator (2) and fluid reservoir (3), described
Evaporator (2) and fluid reservoir (3) are fixedly welded respectively at left and right sides of pedestal (1) top, it is characterised in that: the evaporator
(2) top is fixed with capping (4), and described capping (4) upper middle position is equipped with servo motor (8), the servo electricity
Machine (8) output end is connected with agitating shaft (5) by shaft joint, and agitating shaft (5) bottom end is also welded with annular in pairs up and down and sets
The filtration members set, the filtration members include the interior plectane (6) and excircle board (7) of hollow setting, the interior plectane (6) and outer
It is equipped with filter screen (9) between plectane (7) by being placed equidistant with CARBURIZING FURNACE FOR STAINLESS FASTENER nail, the interior plectane (6) and agitating shaft (5)
Bottom end outer wall is installed by screw and is fixed, and the evaporator (2) inner wall offers and slips matched ring with excircle board (7) side
Shape open slot (10), agitating shaft (5) the outer wall side are equidistantly welded with the stirring blade above and below being respectively facing (11),
The interior bottom of the evaporator (2) is equipped with heating rod (12), and described capping (4) top is plugged with conduit (13), and the conduit
(13) and fluid reservoir (3) upper end activity grafting, conduit (13) outer wall have also been arranged in pairs cooling tube (14), the fluid reservoir
(3) bottom right side is communicated with the drain pipe (15) for being equipped with gate valve.
2. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the pedestal
(1) top is also equipped with cold water storage cistern ontology (16), and cold water storage cistern ontology (16) top is also equipped with water pump (17), the water pump
(17) water delivery end is communicated with into water main pipeline (18), and the water inlet main pipeline (18) is communicated with by tee tube into water subtube
(19), and two water inlet subtubes (19) are connected on the left of cooling tube (14), and the cooling tube (14) outer wall bottom
Also it is communicated with the water return pipeline (20) being connected to cold water storage cistern ontology (16).
3. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the conduit
(13) shape is that vertical section (131) and tilting section (132) are staggered, and the vertical section (131) and tilting section (132) it
Between angle be 80 degree, and two cooling tubes (14) are all set on the outside of the tilting sections (132) of conduit (13), described to lead
Pipe (13) is also equipped with hand-operated valve.
4. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the capping
(4) it is equipped on left inside wall Temperature Humidity Sensor (21), capping (4) upper left end is equipped with temperature and humidity control by screw
Device (22) processed, the Temperature Humidity Sensor (21) is electrically connected at temperature and humidity controller (22) by conducting wire respectively, described warm and humid
Degree controller (22) is also electrically connected at heating rod (12), the model CD195X-9M7 that the temperature and humidity controller (22) uses
Multi-way intelligence temperature and humidity controller, the temperature and humidity for the model RS-WS-N01-2 that the Temperature Humidity Sensor (21) uses passes
Sensor (21).
5. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the capping
(4) upper left-hand is communicated with relief pipeline (23), is also fixedly installed with valve on the relief pipeline (23).
6. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the capping
(4) upper left-hand is also communicated with charging line (24), and charging line (24) top is threaded with end cap.
7. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the fluid reservoir
(3) outer wall is fixedly welded with aluminium base cooling fin (25), and the fluid reservoir (3) and evaporator (2) outer wall are embedded with form (26).
8. a kind of higher boiling chemical reagent described in accordance with the claim 1 purifies filling apparatus, it is characterised in that: the pedestal
(1) bottom is fixedly installed with Self-locking universal wheel (27), and is fixedly installed with handle on the left of the pedestal (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821778301.7U CN208915934U (en) | 2018-10-31 | 2018-10-31 | A kind of higher boiling chemical reagent purification filling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821778301.7U CN208915934U (en) | 2018-10-31 | 2018-10-31 | A kind of higher boiling chemical reagent purification filling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208915934U true CN208915934U (en) | 2019-05-31 |
Family
ID=66711129
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821778301.7U Expired - Fee Related CN208915934U (en) | 2018-10-31 | 2018-10-31 | A kind of higher boiling chemical reagent purification filling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208915934U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111001365A (en) * | 2019-12-23 | 2020-04-14 | 张小飞 | Fine chemical product purification equipment |
| CN112212616A (en) * | 2020-10-14 | 2021-01-12 | 芜湖森爱驰生物科技有限公司 | Production line and process of blood coagulation reagent production equipment |
-
2018
- 2018-10-31 CN CN201821778301.7U patent/CN208915934U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111001365A (en) * | 2019-12-23 | 2020-04-14 | 张小飞 | Fine chemical product purification equipment |
| CN111001365B (en) * | 2019-12-23 | 2021-08-24 | 甘肃金川恒信高分子科技有限公司 | Fine chemical product purification equipment |
| CN112212616A (en) * | 2020-10-14 | 2021-01-12 | 芜湖森爱驰生物科技有限公司 | Production line and process of blood coagulation reagent production equipment |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190531 Termination date: 20211031 |
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| CF01 | Termination of patent right due to non-payment of annual fee |