CN200949969Y - Device for cooling and crystallizing liquid material - Google Patents
Device for cooling and crystallizing liquid material Download PDFInfo
- Publication number
- CN200949969Y CN200949969Y CN 200620035468 CN200620035468U CN200949969Y CN 200949969 Y CN200949969 Y CN 200949969Y CN 200620035468 CN200620035468 CN 200620035468 CN 200620035468 U CN200620035468 U CN 200620035468U CN 200949969 Y CN200949969 Y CN 200949969Y
- Authority
- CN
- China
- Prior art keywords
- cooling
- liquid material
- charging ladle
- cooler
- agitator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000001816 cooling Methods 0.000 title claims abstract description 20
- 239000011344 liquid material Substances 0.000 title claims abstract description 15
- 238000002425 crystallisation Methods 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052802 copper Inorganic materials 0.000 claims abstract description 5
- 239000010949 copper Substances 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 9
- 239000000498 cooling water Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 3
- 239000004809 Teflon Substances 0.000 claims description 2
- 229920006362 Teflon® Polymers 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 11
- 230000008025 crystallization Effects 0.000 abstract description 7
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 3
- 230000000903 blocking effect Effects 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 230000000087 stabilizing effect Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000011343 solid material Substances 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000009938 salting Methods 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
A liquid material cooling crystallization device comprises a water division cover of a cooler, a cooler core, a material filling barrel, a blending motor and a wave wheel blender. The water division cover is provided with a cooling water-in pipe and a water-out pipe, the cooler core is arranged around a circle in two groups by the copper tube bundles and is sleeved in the material filling barrel which is opened with a material-in pipe and a material-out pipe at the bottom, an upper end of a principal shaft of the blender is connected with the motor, a circle wave wheel is provided in the center of the principal shaft and a stabilizing frame is provided at a lower end of the principal shaft. The device has the advantages of high heat exchanging efficiency and corrosion resistance without blocking the pipeline.
Description
Technical field
The invention belongs to refrigeration technology field, relate to a kind of device that the liquid material cooling is made its crystallization and crystal is therefrom separated, particularly a kind of liquid material equipment of crystallisation by cooling.
Background technology
During the saline solution that in handling vanadium product enterprise or other Production in Chemical Plant process, produces, need crystallizations such as the solid salt that contains in the solution such as sodium sulphate to be separated out with cooling means.Because solution be along with the reduction of temperature can be separated out the salt crystal gradually, so when cooling off such solution with the existing heat exchange type of cooling, the frequent blockage phenomenon of the pipeline that solution passes through, normally the carrying out continuously of influence production; Moreover because of salting liquid has certain corrosivity, the heat exchanger life-span in the cooling heat transferring system is short, causes parts replacement frequent.
The utility model content
In order to overcome the above-mentioned problems in the prior art, the utility model provides a kind of liquid material equipment of crystallisation by cooling.
Technical scheme is, described liquid material equipment of crystallisation by cooling cooler divides water cover, cooler core, charging ladle, stirring motor, ripple-wheel agitator to form, divide water cover to be provided with cooling water inlet pipe and outlet pipe, cooler core becomes two groups and be set in the charging ladle by U type red copper tube bundle by circumferential arrangement, the coating of scribble acid and alkali-resistance, coefficient of overall heat transmission height on the copper tube, not being stained with material.The cooling core retainer plate is contained on the charging ladle, and the charging ladle bottom has a feed pipe and a discharge nozzle, and agitator main shaft upper end is connected with motor, and the main shaft middle part is provided with circular impeller, and the lower end is provided with a steady rest; The surface of charging ladle inner surface, main shaft, circular impeller, steady rest all scribbles coating, prevents the agitator adhered materials.
Because the utility model is with cooling water (temperature can be determined according to manufacturing technique requirent) cooling liquid material, makes its cooling, crystallization, discharge, and because solution is to be contained in the staving, so heat exchange efficiency height, corrosion-resistant the pipeline clogging can not take place.
Description of drawings
Fig. 1 is an A-A view of the present utility model.
Fig. 2 is a front view of the present utility model.
Among the figure, 2 stirring motors; 3 divide water cover for cooler; 4 is cooling water inlet pipe; Be 5 cooler water outlet pipes; 6 is cooler core; 7 is charging ladle; 8 is heat exchanger tube; 9 for stirring impeller; 10 is axle sleeve; 11 is steady rest; 12 is the cooler bottom; 13 is discharging opening; 14 is charging aperture, and 15 are rotating shaft.
The specific embodiment
Illustrate a kind of liquid material equipment of crystallisation by cooling, this device is discontinuous input and output material equipment of crystallisation by cooling, divide water cover 3 by cooler, cooler core 6, charging ladle 7, stirring motor 2, ripple-wheel agitator is formed, divide water cover to be provided with cooling water inlet pipe 4 and outlet pipe 5, cooler core becomes two to consist of cooling core and being set in the charging ladle by U type red copper heat exchanger tube 8 by circumferential arrangement, the charging ladle bottom has a feed pipe 14 and a discharge nozzle 13, agitator is vertically arranged, agitator main shaft 15 upper ends are connected with motor 2, the main shaft middle part is provided with circular impeller 9, and the lower end is provided with a steady rest 11.
Liquid material 14 is input in the charging ladle 7 from entering the mouth, the valve that connect on the discharging opening 13 this moment is in closed condition, when detecting the charging ladle filled with fluid by liquid level sensor, cooling water is from entering the mouth 4 through heat exchanger tube 8 inflows and circulation, through the heat exchange of heat exchanger tube, after water temperature raises, flow out refrigeration machine and lower the temperature again through exporting 5, circulate the heat of taking away material, make material cooling, the salts substances in this moment liquid material begins crystallization and separates out and form solid.In said process, stirring motor is entry into service simultaneously also, and purpose is to make liquid material stir the raising heat exchange efficiency, does not allow heat exchanger tube liquid material temperature on every side low excessively simultaneously, and the solids adhering of avoiding crystallization is on heat exchanger tube.Bottom stirring impeller plays and sinks to the bottom the solid material tipping effect, in order to avoid a large amount of materials sinks to the bottom the discharge difficulty.The temperature of cooling water looks different production requirement and specific liquid material is set.After cooling water temperature drops to design temperature, open the valve on the charging ladle outlet at bottom 13, emit the solid material of liquid and crystallization, pass through isolated by filtration again, and solid material oven dry processing is obtained finished product.
Described charging ladle 7 can be rolled into by steel plate, also can be made such as plastics by other material, and its external form can be columniform, also can be other shape.
Described rotating shaft of stirrer 15 upper ends are connected with motor, and so that portion's agitator power to be provided, rotating shaft 15 lower ends are connected with a steel cross steady rest 11, and uranium cover 10 plays stable agitator effect, prevent to swing the heat exchanger tube of damaging when agitator from rotating.
The inner surface of described charging ladle 7, the outer surface of rotating shaft 15, stirring impeller 9, heat exchanger tube 8, steady rest 11 all scribbles corrosion-resistant teflon coatings, to prevent the material bonding.
Claims (2)
1, a kind of liquid material equipment of crystallisation by cooling, divide water cover (3), cooler core (6), charging ladle (7), stirring motor (2), ripple-wheel agitator to form by cooler, it is characterized in that, divide water cover to be provided with cooling water inlet pipe (4) and outlet pipe (5), cooler core (6) becomes two groups to form and be set in the charging ladle by U type red copper heat exchanger tube (8) by circumferential arrangement; The charging ladle bottom has a feed pipe (14) and a discharge nozzle (13), and agitator arranges that vertically agitator main shaft (15) upper end is connected with motor (2), and the main shaft middle part is provided with circular impeller (9), and the lower end is provided with a steady rest (11).
2, a kind of liquid material equipment of crystallisation by cooling according to claim 1 is characterized in that, the surface of charging ladle (7) inner surface and main shaft (15), circular impeller (9), steady rest (11), heat exchanger tube (8) all scribbles the teflon coatings coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200620035468 CN200949969Y (en) | 2006-08-26 | 2006-08-26 | Device for cooling and crystallizing liquid material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200620035468 CN200949969Y (en) | 2006-08-26 | 2006-08-26 | Device for cooling and crystallizing liquid material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN200949969Y true CN200949969Y (en) | 2007-09-19 |
Family
ID=38892510
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200620035468 Expired - Fee Related CN200949969Y (en) | 2006-08-26 | 2006-08-26 | Device for cooling and crystallizing liquid material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN200949969Y (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104690101A (en) * | 2014-10-09 | 2015-06-10 | 安徽工程大学 | Wire drawing liquid cooling system and controlling method thereof |
| CN104740891A (en) * | 2015-04-16 | 2015-07-01 | 威海沁和实业有限公司 | Air cooling crystallizer for inner fin tubes |
| CN109569012A (en) * | 2018-11-23 | 2019-04-05 | 衡阳市晋宏精细化工有限公司 | It can be quickly cooled to the crystallization making apparatus of type |
| CN110057203A (en) * | 2019-05-14 | 2019-07-26 | 安徽轩鸣新材料有限公司 | The manufacturing smoke processing system of rock wool |
| CN114669079A (en) * | 2022-04-28 | 2022-06-28 | 稀美资源(广东)有限公司 | Dynamic crystallization equipment of potassium fluotantalate |
| CN118079434A (en) * | 2024-02-20 | 2024-05-28 | 江苏联恒电子新材料科技有限公司 | Electronic grade phosphoric acid production equipment and production process thereof |
-
2006
- 2006-08-26 CN CN 200620035468 patent/CN200949969Y/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104690101A (en) * | 2014-10-09 | 2015-06-10 | 安徽工程大学 | Wire drawing liquid cooling system and controlling method thereof |
| CN104740891A (en) * | 2015-04-16 | 2015-07-01 | 威海沁和实业有限公司 | Air cooling crystallizer for inner fin tubes |
| CN109569012A (en) * | 2018-11-23 | 2019-04-05 | 衡阳市晋宏精细化工有限公司 | It can be quickly cooled to the crystallization making apparatus of type |
| CN110057203A (en) * | 2019-05-14 | 2019-07-26 | 安徽轩鸣新材料有限公司 | The manufacturing smoke processing system of rock wool |
| CN114669079A (en) * | 2022-04-28 | 2022-06-28 | 稀美资源(广东)有限公司 | Dynamic crystallization equipment of potassium fluotantalate |
| CN114669079B (en) * | 2022-04-28 | 2023-10-20 | 稀美资源(广东)有限公司 | Dynamic crystallization equipment of potassium fluotantalate |
| CN118079434A (en) * | 2024-02-20 | 2024-05-28 | 江苏联恒电子新材料科技有限公司 | Electronic grade phosphoric acid production equipment and production process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20070919 Termination date: 20130826 |