CN207786585U - A kind of novel reaction kettle - Google Patents
A kind of novel reaction kettle Download PDFInfo
- Publication number
- CN207786585U CN207786585U CN201721793996.1U CN201721793996U CN207786585U CN 207786585 U CN207786585 U CN 207786585U CN 201721793996 U CN201721793996 U CN 201721793996U CN 207786585 U CN207786585 U CN 207786585U
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- CN
- China
- Prior art keywords
- dryness storehouse
- autoclave body
- valve
- reaction
- container mechanism
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Abstract
The utility model provides a kind of novel reaction kettle, including：First reaction container mechanism, drier, the second reaction container mechanism；The first reaction container mechanism includes the first autoclave body, lid, sieve plate, power motor, planet-gear transmission device, agitating paddle, the first valve；The drier includes dryness storehouse, ultrasonic vibration stick, breather valve, the second valve, moves expects pipe, the ultrasonic vibration stick is mounted in dryness storehouse, the dryness storehouse lower end is equipped with dry bin discharge port external, second valve is connected with dry bin discharge port external, described one end for moving expects pipe is connected with the second valve, it is additionally provided with semiconductor heating plate on the outside of the dryness storehouse, the semiconductor heating plate includes chill surface and heating face, and the heating face of the semiconductor heating plate is bonded with dryness storehouse；The second reaction container mechanism includes the second autoclave body, feed inlet, sealing ring, holder, homogenizer.The solid that the utility model reaction kettle can generate reaction is efficiently removed.
Description
Technical field
The utility model is related to a kind of reaction kettles, more particularly to a kind of novel reaction kettle.
Background technology
Reaction kettle is widely used in the fields such as chemical industry, rubber, oil, dyestuff, medicine, food, for completing production process
In the technical process such as hydrolysis, polymerization, mixture, neutralization, hydrogenation, chlorination.Currently, the reaction kettle that generally uses of enterprise by autoclave body,
Motor, agitating shaft and stirring wheel piece composition, motor are installed on autoclave body top, and agitating shaft is located at autoclave body centre and leads to across autoclave body
It crosses shaft coupling to connect with motor, stirring wheel piece and agitating shaft vertical connection, by motor driving agitating shaft rotation, make on agitating shaft
Stirring wheel piece quickly rotates to carry out material stirring mixing.
But it in process of production, often will produce a large amount of solid precipitations in reaction solution, the normal stirring of reaction kettle influenced, if not
Processing precipitation, then can influence being normally carried out for reaction, if processing precipitation, need to stop reacting, and filtered, and also need to
Cleaning is carried out to reaction kettle to reuse, and influences the reaction efficiency of reaction kettle.
Utility model content
The utility model provides a kind of novel reaction kettle, at least solve existing reaction kettle reaction generate solid when not
The problem of capable of effectively removing.
The utility model provides a kind of novel reaction kettle, including：First reaction container mechanism, drier, the second reaction kettle
Mechanism；It is described first reaction container mechanism include the first autoclave body, lid, sieve plate, power motor, planet-gear transmission device,
Agitating paddle, the first valve, the lid and the first autoclave body lid close, and form the first reaction chamber, and the power motor is mounted on lid
Top, the power motor are connected by planet-gear transmission device with agitating paddle, and it is anti-that the agitating paddle is mounted on first
Intracavitary, first autoclave body lower end is answered to be equipped with discharge port, the sieve plate is mounted on the first reaction chamber bottom close to discharge outlet, institute
The first valve is stated with discharge port to be connected；The drier includes dryness storehouse, ultrasonic vibration stick, breather valve, the second valve, moves material
Pipe, the dryness storehouse are connected with the first valve, and the breather valve is mounted on dryness storehouse upper end, and the ultrasonic vibration stick is mounted on dry
In dry storehouse, the dryness storehouse lower end is equipped with dry bin discharge port external, and second valve is connected with dry bin discharge port external, the shifting material
One end of pipe is connected with the second valve, is additionally provided with semiconductor heating plate on the outside of the dryness storehouse, the semiconductor heating plate includes
Chill surface and heating face, the heating face of the semiconductor heating plate is bonded with dryness storehouse；The second reaction container mechanism includes the
Two autoclave bodies, feed inlet, sealing ring, holder, homogenizer, the feed inlet are mounted on the second autoclave body upper end, the feed inlet
It is connected with the other end for moving expects pipe, second autoclave body is fixed on holder, and heating is additionally provided in the side wall of second autoclave body
Chamber, the homogenizer include pedestal, strut, casing, high-speed electric expreess locomotive, feed belt, shearing paddle, and the pedestal hangs down with strut
Straight to be connected, the casing is mounted on strut, and the high-speed electric expreess locomotive is mounted on the outside of casing, and the feed belt is mounted on casing
Interior, described shearing paddle one end is connected by feed belt with casing, and the other end of the shearing paddle passes through the second autoclave body upper end simultaneously
In the second autoclave body, the shearing paddle is bonded by sealing ring with the second autoclave body upper end.
Further, strainer is additionally provided in the dryness storehouse, the strainer is parallel to horizontal plane in dryness storehouse.
Further, the sealing ring surface also has tetrafluoroethene coating.
Further, it is additionally provided with temperature-detecting device in the dryness storehouse.
Further, the dryness storehouse further includes controller, the controller respectively with temperature-detecting device, semiconductor
Heating plate is connected.
The utility model forms one compared with prior art, by using the first reaction container mechanism, the second reaction container mechanism
Kind novel reaction kettle carries out first segment reaction using the first reaction container mechanism, when having a large amount of solids to generate, then passes through drier
Reaction solution is shifted, effectively except the solid generated in dereaction, remaining reaction solution is allow to react container mechanism second
The middle reaction for carrying out the second half section, makes reaction kettle remain to keep higher reaction efficiency while effectively removing solid.Meanwhile this
Utility model can effectively concentrate reaction solution by using drier, improve the material concentration in reaction solution, and then promote
Into the progress of reaction, reaction yield is improved.
Description of the drawings
Fig. 1 is the utility model embodiment structural schematic diagram.
Specific implementation mode
In order to make those skilled in the art more fully understand the utility model, below in conjunction with the utility model reality
The attached drawing in example is applied, the technical scheme in the utility model embodiment is clearly and completely described, it is clear that described
Embodiment is only the embodiment of the utility model part, instead of all the embodiments.Based on the reality in the utility model
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts is all answered
When the range for belonging to the utility model protection.
It should be noted that term " first " in the specification and claims of the utility model and above-mentioned attached drawing,
" second " etc. is for distinguishing similar object, without being used to describe specific sequence or precedence.
The utility model discloses a kind of novel reaction kettles, as shown in Figure 1, including：First reaction container mechanism, drier,
Second reaction container mechanism；The first reaction container mechanism includes the first autoclave body 11, lid 12, sieve plate 13, power motor 14, few tooth
Difference planet gear driver 15, agitating paddle 16, the first valve 17, the lid 12 and the first autoclave body 11 lid close, and it is anti-to form first
Chamber, the power motor 14 is answered to be mounted on 12 top of lid, the power motor 14 passes through planet-gear transmission device 15
It is connected with agitating paddle 16, the agitating paddle 16 is mounted in the first reaction chamber, and 11 lower end of the first autoclave body is equipped with discharge port, institute
Sieve plate 13 is stated mounted on the first reaction chamber bottom close to discharge outlet, first valve 17 is connected with discharge port；The drying
Device includes dryness storehouse 21, ultrasonic vibration stick 22, breather valve 23, the second valve 24, moves expects pipe 25, the dryness storehouse 21 and the first valve
Door 17 is connected, and the breather valve 23 is mounted on 21 upper end of dryness storehouse, and the ultrasonic vibration stick 22 is mounted in dryness storehouse 21, described
21 lower end of dryness storehouse is equipped with dry bin discharge port external, and second valve 24 is connected with dry bin discharge port external, the shifting expects pipe 25
One end is connected with the second valve 24, and 21 outside of the dryness storehouse is additionally provided with semiconductor heating plate 26, the semiconductor heating plate 26
Including chill surface and heating face, the heating face of the semiconductor heating plate 26 is bonded with dryness storehouse 21；The second reaction kettle machine
Structure includes the second autoclave body 31, feed inlet 33, sealing ring 34, holder 35, homogenizer, and the feed inlet 32 is mounted on the second kettle
31 upper end of body, the feed inlet 32 are connected with the other end for moving expects pipe 25, and second autoclave body 31 is fixed on holder 35, described
Heating chamber 32 is additionally provided in the side wall of second autoclave body 31, the homogenizer includes pedestal 41, strut 43, casing 44, high speed
Motor 45, feed belt 46, shearing paddle 47, the pedestal 41 are vertically connected with strut 43, and the casing 44 is mounted on strut 43
On, the high-speed electric expreess locomotive 45 is mounted on 44 outside of casing, and the feed belt 46 is mounted in casing 44, the shearing paddle 47 1
End is connected by feed belt 46 with casing 44, and the other end for shearing paddle 47 is across 31 upper end of the second autoclave body and is mounted on the
In two autoclave bodies 31, the shearing paddle 47 is bonded by sealing ring 34 with 31 upper end of the second autoclave body.
Wherein, as shown in Figure 1, being additionally provided with inlet tube 321, outlet tube 322, inlet tube 321, outlet tube on the second autoclave body 31
322 are connected with heating chamber 32 respectively.
When being reacted, the first reaction container mechanism is added raw materials into, so that the first autoclave body 11 is closed with the lid of lid 12, by power
Motor 14 drive agitating paddle 16 rotate, so that agitating paddle 16 is ground stirring to raw material, make the granular size in raw material it is uniform, rush
Efficient mixing into raw material and progress first segment reaction, after generating more precipitation, open the first valve 17, make sieve plate 13 to reaction
Particle is precipitated in liquid to be removed, and so that reaction solution is flowed into dryness storehouse 21, is closed the first valve 17, staff can be according to actual
Production needs to choose whether to concentrating in reaction solution, if selection concentration, breather valve 23 is connected with vacuum pump, opens super
Acoustic vibration stick 22 simultaneously opens semiconductor heating plate 26 to the heating of dryness storehouse 21, is dried in vacuo, low-pressure distillation removes excessive
Low-boiling point liquid.After drying after the completion, breather valve 23 is connected with air pump, opens the second valve 24, the gas formed using air pump
Pressure is further reacted material liquid by moving the inflow of expects pipe 25 second reaction container mechanism.
The utility model embodiment forms a kind of novel reaction by using the first reaction container mechanism, the second reaction container mechanism
Kettle carries out first segment reaction using the first reaction container mechanism, when thering are a large amount of solids to generate, then by drier by reaction solution into
Row transfer allows remaining reaction solution to be carried out in the second reaction container mechanism later half effectively except the solid generated in dereaction
The reaction of section, makes reaction kettle remain to keep higher reaction efficiency while effectively removing solid.Meanwhile the utility model is real
Example is applied by using drier, reaction solution can effectively be concentrated, the material concentration in reaction solution is improved, and then is promoted anti-
The progress answered improves reaction yield.
Optionally, strainer is additionally provided in the dryness storehouse 21, the strainer is parallel to horizontal plane and is installed in dryness storehouse 21.
The utility model embodiment is filtered point the larger particles in reaction solution by the way that strainer is arranged, using strainer
From effectively larger particles being avoided to flow out, prevents the blocking of pipette.
Optionally, 34 surface of the sealing ring also has tetrafluoroethene coating.
The utility model embodiment reduces sealing ring 34 and strut by the way that tetrafluoroethene coating is arranged on 34 surface of sealing ring
Friction between 43, it is ensured that strut 43 can normal high speed rotation.
Particularly, it is additionally provided with temperature-detecting device in the dryness storehouse 2.
Particularly, the drier further includes controller, the controller and temperature-detecting device, semiconductor heating plate phase
Even.
Wherein, controller is connected with temperature-detecting device, semiconductor heating plate respectively by conducting wire.
The utility model embodiment is by being arranged controller, using controller come according to the detection data of temperature-detecting device
The working condition of semiconductor heating plate is automatically controlled, when temperature is too low, semiconductor heating plate is started by controller and carries out work
Make, and then makes drier that there is automation function.
Finally it should be noted that above example is only to illustrate the technical solution of the utility model rather than limits it
System, although the utility model is described in detail with reference to above-described embodiment, those of ordinary skill in the art should
Understand, technical staff read present specification after can still modify to specific embodiment of the present utility model or
Equivalent replacement, but these are changed or are changed within all without departing from present utility model application accompanying claims protection domain.
Claims (5)
1. a kind of novel reaction kettle, which is characterized in that including：
First reaction container mechanism, the first reaction container mechanism includes the first autoclave body, lid, sieve plate, power motor, few teeth difference row
Star gear driver, agitating paddle, the first valve, the lid and the first autoclave body lid close, and form the first reaction chamber, the power electric
Machine is mounted on above lid, and the power motor is connected by planet-gear transmission device with agitating paddle, the agitating paddle
In the first reaction chamber, first autoclave body lower end is equipped with discharge port, and the sieve plate is leaned on mounted on the first reaction chamber bottom
Nearly discharge outlet, first valve are connected with discharge port；
Drier, the drier include dryness storehouse, ultrasonic vibration stick, breather valve, the second valve, move expects pipe, the dryness storehouse
It is connected with the first valve, the breather valve is mounted on dryness storehouse upper end, and the ultrasonic vibration stick is mounted in dryness storehouse, described dry
Dry storehouse lower end is equipped with dry bin discharge port external, and second valve is connected with dry bin discharge port external, one end of the shifting expects pipe and the
Two valves are connected, and are additionally provided with semiconductor heating plate on the outside of the dryness storehouse, the semiconductor heating plate includes chill surface and heating
The heating face in face, the semiconductor heating plate is bonded with dryness storehouse；
Second reaction container mechanism, the second reaction container mechanism includes the second autoclave body, feed inlet, sealing ring, holder, high-speed stirred
Machine, the feed inlet are mounted on the second autoclave body upper end, and the feed inlet is connected with the other end for moving expects pipe, and second autoclave body is solid
Be scheduled on holder, be additionally provided with heating chamber in the side wall of second autoclave body, the homogenizer include pedestal, strut, casing,
High-speed electric expreess locomotive, feed belt, shearing paddle, the pedestal are vertically connected with strut, and the casing is mounted on strut, the high speed
Motor is mounted on the outside of casing, and the feed belt is mounted in casing, and described shearing paddle one end passes through feed belt and casing
It is connected, the other end of the shearing paddle passes through the second autoclave body upper end and in the second autoclave body, the shearing paddle passes through sealing
Circle is bonded with the second autoclave body upper end.
2. reaction kettle according to claim 1, which is characterized in that be additionally provided with strainer in the dryness storehouse, the strainer is flat
Row is mounted in horizontal plane in dryness storehouse.
3. reaction kettle according to claim 1, which is characterized in that the sealing ring surface also has tetrafluoroethene coating.
4. reaction kettle according to claim 1, which is characterized in that be additionally provided with temperature-detecting device in the dryness storehouse.
5. reaction kettle according to claim 4, which is characterized in that the dryness storehouse further includes controller, the controller
It is connected respectively with temperature-detecting device, semiconductor heating plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721793996.1U CN207786585U (en) | 2017-12-20 | 2017-12-20 | A kind of novel reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721793996.1U CN207786585U (en) | 2017-12-20 | 2017-12-20 | A kind of novel reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207786585U true CN207786585U (en) | 2018-08-31 |
Family
ID=63281412
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721793996.1U Expired - Fee Related CN207786585U (en) | 2017-12-20 | 2017-12-20 | A kind of novel reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207786585U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113908792A (en) * | 2021-10-25 | 2022-01-11 | 上海丽唯生物科技有限公司 | Equipment and method for preparing nicotinamide ribose |
-
2017
- 2017-12-20 CN CN201721793996.1U patent/CN207786585U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113908792A (en) * | 2021-10-25 | 2022-01-11 | 上海丽唯生物科技有限公司 | Equipment and method for preparing nicotinamide ribose |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180831 Termination date: 20211220 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |