CN208857170U - A kind of production line of isoesdragol - Google Patents
A kind of production line of isoesdragol Download PDFInfo
- Publication number
- CN208857170U CN208857170U CN201821152882.3U CN201821152882U CN208857170U CN 208857170 U CN208857170 U CN 208857170U CN 201821152882 U CN201821152882 U CN 201821152882U CN 208857170 U CN208857170 U CN 208857170U
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- China
- Prior art keywords
- tank
- entrance
- connect
- tower
- isoesdragol
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of production lines of isoesdragol, including material storaging tank and finished pot, refrigerator, pulverizer, centrifuge, heating tank, rectifying column, agitator tank and filtering tank are also disposed between material storaging tank and finished pot, wherein, the outlet of heating tank and the entrance of rectifying column connect, the tower top discharge port of rectifying column and the entrance of agitator tank connect, and the outlet of agitator tank and the entrance of filtering tank connect, and the outlet of filtering tank and the entrance of finished pot connect.The utility model passes through addition pulverizer and centrifuge, the solid intracorporal liquid impurity formed after crystallisation by cooling can be will be present in remove, rectifying column and filtering tank are utilized simultaneously, improve the purity of product, so that its purity is may be up to 99.9% or more, while utilizing agitator tank, the product uniform stirring that different time sections rectifying can be made to go out, so that the purity of product is consistent in final tinning, avoid the product purity of top and the bottom inconsistent.
Description
Technical field
The utility model relates to the production line of natural perfume material, especially a kind of production line of isoesdragol.
Background technique
Trans-anethole is a kind of chemicals, is the main component of fennel oil.Trans-anethole is in addition to can be used for
Other than cosmetics, food flavor and medicine, it can also be used to synthesize a series of flavorants.With the rush of demand in market, pass
The purity of the resulting trans-anethole of production line of uniting and production efficiency can not meet the demand in market, therefore be badly in need of research and development one
The production line of the purity of trans-anethole can be improved.
Summary of the invention
In order to solve the above technical problems, the utility model provides a kind of production line of isoesdragol, using the life
Producing line can reach 99.9% or more with the purity for preparing natural trans-anethole.
The technical scheme adopted by the utility model to solve the technical problem is as follows: a kind of production line of isoesdragol, including
Material storaging tank and finished pot are also disposed with refrigerator, pulverizer, centrifugation between the material storaging tank and the finished pot
Machine, heating tank, rectifying column, agitator tank and filtering tank, the discharge port of the material storaging tank and the entrance of refrigerator connect, described
The ice mouth of refrigerator and the entrance of pulverizer connect, and the outlet of pulverizer and the entrance of centrifuge connect, the solid of centrifuge
The connection of the entrance of discharge port and heating tank, the outlet of heating tank and the entrance of rectifying column connect, the tower top discharging of the rectifying column
Mouthful connect with the entrance of agitator tank, the outlet of the agitator tank and the entrance connection of filtering tank, the outlet of the filtering tank and at
The entrance of product tank connects.
Further, the entrance of the liquid outlet opening of the centrifuge and refrigerator connects.
Further, tower is evaporated before further including, the liquid outlet opening of the centrifuge is also connect with the entrance for preceding evaporating tower, before described
The entrance of the tower bottom discharge port and refrigerator that evaporate tower connects.
Further, the tower top discharge port that tower is evaporated before described is connect with the first recycling can.
Further, the filtering tank is internally provided with accurate filter cloth.
Further, the rectifying column uses material filling type.
Further, the tower bottom discharge port of the rectifying column is connect with the second recycling can.
The beneficial effects of the utility model are: by addition pulverizer and centrifuge, after crystallisation by cooling being will be present in
The solid intracorporal liquid impurity formed removes, while utilizing rectifying column and filtering tank, improves the purity of product, makes its purity can
Up to 99.9% or more, while agitator tank is utilized, the product uniform stirring that different time sections rectifying can be made to go out, so that final tinning
The purity of interior product is consistent, and avoids the product purity of top and the bottom inconsistent；Furthermore by the liquid outlet opening of centrifuge point
Not with refrigerator and before evaporate tower and connect, raw material can further be extracted, so that the yield of product can further improve, while also be dropped
Low production cost.
Detailed description of the invention
The present invention will be further described with reference to the accompanying drawings and examples.
Fig. 1 is a kind of flow diagram of embodiment of the utility model.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below with reference to embodiment and
The technical effect of the design of the utility model, specific structure and generation is clearly and completely described in attached drawing, with sufficiently geographical
Solve the purpose of this utility model, feature and effect.Obviously, described embodiment is that a part of the utility model is implemented
Example, rather than whole embodiments, those skilled in the art's other realities obtained without creative efforts
Example is applied, the range of the utility model protection is belonged to.
It referring to Fig.1, is a kind of preferably embodiment, a kind of production line of isoesdragol, including material storaging tank 1 and finished product
Tank 9 is also disposed with refrigerator 2, pulverizer 3, centrifuge 4, heating tank between the material storaging tank 1 and the finished pot 9
5, the discharge port of rectifying column 6, agitator tank 7 and filtering tank 8, the material storaging tank 1 is connect with the entrance of refrigerator 2, described cold
The ice mouth of jelly machine 2 is connect with the entrance of pulverizer 3, and the outlet of pulverizer 3 is connect with the entrance of centrifuge 4, and centrifuge 4 is consolidated
Body discharge port is connect with the entrance of heating tank 5, and the outlet of heating tank 5 is connect with the entrance of rectifying column 6, the tower of the rectifying column 6
Ejection material mouth is connect with the entrance of agitator tank 7, and the outlet of the agitator tank 7 is connect with the entrance of filtering tank 8, the filtering tank 8
Outlet connect with the entrance of finished pot 9.
Raw material is deposited in material storaging tank 1.When specific production, from taking-up is placed in refrigerator 2 in material storaging tank 1
It is freezed, through or so 8 hours, raw material is frozen into solid ice cube, and ice cube is put into pulverizer 3 and carries out extruding crushing, crushes
Afterwards particle investment centrifuge 4 in be centrifuged, out of centrifuge 4 take out solid material be put into heating tank 5 heat it is molten
Solution dissolves in resulting intermediate products investment rectifying column 6 and carries out rectifying, extracts product from the tower top of rectifying column 6, and product is filled
Enter in agitator tank 7, product is stirred, the product entirety purity made is consistent, and after having stirred, then product is packed into and is filtered
It being filtered in tank 8, further impurity screening improves the purity of product, and finally product is inputted in finished pot 9 and is saved,
When finished pot 9 is filled, then the finished pot 9 for replacing sky continues to filtered product, and the finished pot 9 for installing product is packed
Storage.
In the present embodiment, the liquid outlet opening of the centrifuge 4 is connect with the entrance of refrigerator 2, by cold for the first time
Freeze and the raw material mother liquor after a separation also maintains the isoesdragol of higher degree, therefore resulting liquid after separating for the first time
Freezing in refrigerator 2 is put into, the solid material of higher degree can be obtained again.
In the present embodiment, tower 10 is evaporated before further including, the liquid outlet opening of the centrifuge 4 also connects with the entrance for preceding evaporating tower 10
It connects, the tower bottom discharge port that tower 10 is evaporated before described is connect with the entrance of refrigerator 2, the institute after freezing and separation once or twice
Isoesdragol in the liquid of acquisition, which obtains purity, not to be able to satisfy the demand of production lower than 40%, therefore institute after needing to separate
It is evaporated in tower 10 before the liquid input obtained, the purity of product in its liquid is increased to 60% or more, to meet subsequent production
Requirement, and the liquid that purity improves is put into production and is extracted in line again.
In the present embodiment, for the impurity in withdrawal liquid, the tower top discharge port and the first recycling can of tower 10 are evaporated before described
11 connections, so as to recycle the overhead product for preceding evaporating tower 10.
In the present embodiment, in order to further increase the concentration of product, the filtering tank 8 is internally provided with accurate filter cloth, can
Further filter out impurity.
In the present embodiment, in order to which the effect of the purifying of product is more preferable, the rectifying column 6 uses material filling type.
In the present embodiment, for the impurity in withdrawal liquid, in order to avoid product is polluted, the tower bottom of the rectifying column 6
Discharge port is connect with the second recycling can 12, and the tower bottom product after rectifying is recycled.
The above, the only better embodiment of the utility model, but the utility model is not limited to above-mentioned reality
Example is applied, as long as its technical effect for reaching the utility model with any same or similar means, all should belong to the utility model
Protection scope.
Claims (7)
1. a kind of production line of isoesdragol, including material storaging tank (1) and finished pot (9), it is characterised in that: the material storaging tank
(1) refrigerator (2), pulverizer (3), centrifuge (4), heating tank (5), essence are also disposed between the finished pot (9)
Tower (6), agitator tank (7) and filtering tank (8) are evaporated, the discharge port of the material storaging tank (1) is connect with the entrance of refrigerator (2),
The ice mouth of the refrigerator (2) is connect with the entrance of pulverizer (3), and the outlet of pulverizer (3) and the entrance of centrifuge (4) connect
It connects, the solid outlet of centrifuge (4) is connect with the entrance of heating tank (5), the outlet of heating tank (5) and entering for rectifying column (6)
Mouth connection, the tower top discharge port of the rectifying column (6) are connect with the entrance of agitator tank (7), the outlet and mistake of the agitator tank (7)
The entrance of filter tank (8) connects, and the outlet of the filtering tank (8) is connect with the entrance of finished pot (9).
2. the production line of isoesdragol according to claim 1, it is characterised in that: the liquid of the centrifuge (4) discharges
Mouth is connect with the entrance of refrigerator (2).
3. the production line of isoesdragol according to claim 1 or 2, it is characterised in that: it is evaporated before further including tower (10), it is described
The liquid outlet opening of centrifuge (4) is also connect with the entrance for preceding evaporating tower (10), evaporated before described the tower bottom discharge port of tower (10) with it is cold
The entrance of jelly machine (2) connects.
4. the production line of isoesdragol according to claim 3, it is characterised in that: evaporate the tower top discharging of tower (10) before described
Mouth is connect with the first recycling can (11).
5. the production line of isoesdragol according to claim 1, it is characterised in that: the filtering tank (8) is internally provided with
Accurate filter cloth.
6. the production line of isoesdragol according to claim 1, it is characterised in that: the rectifying column (6) uses material filling type.
7. the production line of isoesdragol according to claim 1 or 6, it is characterised in that: the tower bottom of the rectifying column (6) goes out
Material mouth is connect with the second recycling can (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821152882.3U CN208857170U (en) | 2018-07-19 | 2018-07-19 | A kind of production line of isoesdragol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821152882.3U CN208857170U (en) | 2018-07-19 | 2018-07-19 | A kind of production line of isoesdragol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208857170U true CN208857170U (en) | 2019-05-14 |
Family
ID=66412887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821152882.3U Expired - Fee Related CN208857170U (en) | 2018-07-19 | 2018-07-19 | A kind of production line of isoesdragol |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208857170U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114644959A (en) * | 2020-12-21 | 2022-06-21 | 大连理工江苏研究院有限公司 | Purification system and method of trans-anethole |
-
2018
- 2018-07-19 CN CN201821152882.3U patent/CN208857170U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114644959A (en) * | 2020-12-21 | 2022-06-21 | 大连理工江苏研究院有限公司 | Purification system and method of trans-anethole |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190514 Termination date: 20200719 |