CN208678420U - A kind of rapid equipment of crystallisation by cooling of chemical solution - Google Patents
A kind of rapid equipment of crystallisation by cooling of chemical solution Download PDFInfo
- Publication number
- CN208678420U CN208678420U CN201821101933.XU CN201821101933U CN208678420U CN 208678420 U CN208678420 U CN 208678420U CN 201821101933 U CN201821101933 U CN 201821101933U CN 208678420 U CN208678420 U CN 208678420U
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- China
- Prior art keywords
- cooler bin
- cooling
- bottom plate
- crystallisation
- solution
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Abstract
The utility model discloses a kind of rapid equipment of crystallisation by cooling of chemical solution; including bottom plate; side at the top of the bottom plate is provided with cooler bin; the other side at the top of the bottom plate is provided with storage bin; air pump is installed at the top of the storage bin; the outlet side of the air pump is provided with the second gas-guide tube for being through to cooler bin interior side, and the pumping end of the air pump is provided with the first gas-guide tube for being through to storage bin inner tip, is provided with protective cover at the top of the cooler bin.The utility model is small by the density of the density ratio cold air with hot gas, hot gas be discharged will from escape pipe, it crystallizes solution rapidly, and shaft rotation is driven by motor, so that stirring blade be driven to rotate, solution is stirred, keep solution cooling uniformly, keeps the effect of solution crystallisation by cooling more preferable, improve work efficiency, and by filter screen and collecting box to after crystallization solution and crystallization separate, preferably collect crystallization.
Description
Technical field
The utility model relates to chemical experiment technique field, specially a kind of rapid equipment of crystallisation by cooling of chemical solution.
Background technique
Crystallisation by cooling is a kind of method crystallized to saturated solution, is substantially exactly to make solute by the method for reducing temperature
(substance significantly increased suitable for solubility with the raising of temperature) is separated out in the form of crystal from solution.
Some solution can generate a large amount of heat in reaction in chemical experiment, will in order to preferably save solution
Solution carries out decrease temperature crystalline, however that there are cooling effects is poor for existing crystallization apparatus, it is difficult to crystallize, and when solution crystallizes is cooling not
Uniformly, make the effect of crystallization bad, cannot achieve the effect that crystallize rapidly, reduce working efficiency, existing solution is in cooling
After crystallization, the separating effect of solution and crystallization is bad, cannot be collected well to crystallization.
Utility model content
The purpose of this utility model is to provide a kind of rapid equipment of crystallisation by cooling of chemical solution, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the utility model provides the following technical solutions: a kind of rapid crystallisation by cooling dress of chemical solution
It sets, including bottom plate, the side at the top of the bottom plate is provided with cooler bin, and the other side at the top of the bottom plate is provided with storage bin,
Air pump is installed, the outlet side of the air pump, which is provided with, to be through to the second of cooler bin interior side and lead at the top of the storage bin
The pumping end of tracheae, the air pump is provided with the first gas-guide tube for being through to storage bin inner tip, the top of the cooler bin
It is provided with protective cover, the inside of the protective cover is equipped with motor, and the output end of the motor is provided with inside cooler bin
The shaft on top is evenly arranged with multiple groups stirring blade on the outside of the shaft, and the number of stirring blade is three groups, described cold
But case is provided with feed pipe close to the top of air pump side, and the cooler bin is provided with escape pipe far from the top of air pump side,
The bottom of the cooler bin is provided with the discharge nozzle being through to below bottom plate, and collecting box is provided with below the bottom plate, described
The four corners of bottom base plate are all provided with supporting leg.
Preferably, the bottom of the bottom plate is provided with two groups of card slots, and the two sides at the top of the collecting box are all provided with and block
The fixture block that slot matches, and collecting box is detachably connected by fixture block and card slot with bottom plate, the collecting box is located at discharge nozzle
Underface.
Preferably, the top inside the collecting box is provided with filter screen, and the both ends at the top of the filter screen are all provided with
Deck, and filter screen is detachably connected by deck and collecting box.
Preferably, the bottom of the cooler bin is provided with two groups of support rods, and cooler bin is fixed by support rod and bottom plate
It connects, is provided with insulating layer on the inner wall of the cooler bin.
Preferably, valve is all provided on first gas-guide tube, escape pipe, feed pipe and discharge nozzle.
Preferably, the storage bin is internally provided with ice cube, and the bottom end of the cooler bin is funnel-shaped, and cooler bin is
Transparent glass material.
Compared with prior art, the utility model has the beneficial effects that the rapid equipment of crystallisation by cooling of this kind of chemical solution is logical
It crosses the cold air that air pump volatilizees ice cube in storage bin to extract out, cold air is inputted by cooler bin by the first gas-guide tube and the second gas-guide tube
It is interior, crystallisation by cooling is carried out to solution, the density with the density ratio cold air of hot gas is small, and hot gas rises, and the principle of cold air decline makes
Hot gas will be discharged from escape pipe, crystallize solution rapidly, and drive shaft rotation by motor, so that stirring blade be driven to turn
It is dynamic, solution is stirred, makes solution is cooling uniformly to keep the effect of solution crystallisation by cooling more preferable, improve work efficiency, and logical
Cross filter screen and collecting box to after crystallization solution and crystallization separate, preferably collect crystallization.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the main view of the utility model；
Fig. 3 is the partial structural diagram of the utility model.
In figure: 1, bottom plate；2, motor；3, shaft；4, stirring blade；5, cooler bin；6, storage bin；7, air pump；8, first
Gas-guide tube；9, the second gas-guide tube；10, escape pipe；11, filter screen；12, collecting box；13, feed pipe；14, support rod；15, go out
Expects pipe；16, protective cover；17, supporting leg.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of rapid equipment of crystallisation by cooling of chemical solution,
Including bottom plate 1, the side at 1 top of bottom plate is provided with cooler bin 5, and the other side at 1 top of bottom plate is provided with storage bin
6, the top of the storage bin 6 is equipped with 7 model FAA8006 of air pump), the outlet side of the air pump 7 be provided be through to it is cold
But the second gas-guide tube 9 of 5 interior side of case, the pumping end of the air pump 7, which is provided with, is through to the first of 6 inner tip of storage bin
Gas-guide tube 8, the top of the cooler bin 5 are provided with protective cover 16, and the inside of the protective cover 16 is equipped with 2 (model of motor
OT-RK-775PH-8512), the output end of the motor 2 is provided with the shaft 3 through 5 inner tip of cooler bin, the shaft 3
Outside be evenly arranged with multiple groups stirring blade 4, and the number of stirring blade 4 is three groups, and the cooler bin 5 is close to air pump 7 one
The top of side is provided with feed pipe 13, and the cooler bin 5 is provided with escape pipe 10, the cooling far from the top of 7 side of air pump
The bottom of case 5 is provided with the discharge nozzle 15 for being through to 1 lower section of bottom plate, and the lower section of the bottom plate 1 is provided with collecting box 12, the bottom
The four corners of 1 bottom of plate are all provided with supporting leg 17.
For the utility model by the air pump 7 and storage bin 6 of setting, air pump 7 will be in storage bin 6 by the first gas-guide tube 8
Cold air, is discharged into cooler bin 5 by cold air extraction by the second gas-guide tube 9, is carried out crystallisation by cooling to the solution in cooler bin 5, is led to
Crossing motor 2 drives shaft 3 to rotate, so that stirring blade 4 be driven to rotate, is stirred to the solution in cooler bin 5, keeps solution cold
But uniformly, keep solution crystallization effect more preferable, and the hot gas in cooler bin 5 is discharged by the escape pipe 10 of setting, make cooler bin 5
Inside reach the cold exchange of heat rapidly, make the rapid crystallisation by cooling of solution.
Attached drawing 1,2 and 3 please be considered and examined emphatically, and the bottom of bottom plate 1 is provided with two groups of card slots, and the two sides at 12 top of collecting box are all set
It is equipped with the fixture block to match with card slot, and collecting box 12 is detachably connected by fixture block and card slot with bottom plate 1, collecting box 12 is located at
The underface of discharge nozzle 15.
The rapid equipment of crystallisation by cooling of this kind of chemical solution by the way that card slot is arranged on bottom plate 1, on collecting box 12 setting with
The fixture block that card slot matches makes collecting box 12 be mounted on the bottom of bottom plate 1 by the mutual cooperation of card slot and fixture block, makes to collect
Case 12 disassembles and installs more convenient, and collecting box 12 is located at the underface of discharge nozzle 15, makes collecting box 12 preferably to solution
It is collected.
Attached drawing 1,2 and 3 please be considered and examined emphatically, and the top inside collecting box 12 is provided with filter screen 11,11 top of filter screen
Both ends are all provided with deck, and filter screen 11 is detachably connected by deck with collecting box 12.
The rapid equipment of crystallisation by cooling of this kind of chemical solution passes through filter screen by installing filter screen 11 in collecting box 12
11, by solution and Crystallization Separation, collect solution and crystallization respectively, and by the way that deck is arranged on filter screen 11, make filter screen 11
Just it is stuck in the top of collecting box 12, filter screen 11 easy to disassemble and install.
Attached Fig. 1 and 2 please be considered and examined emphatically, the two sides of 5 bottom of cooler bin are all provided with support rod 14, and cooler bin 5 passes through branch
Strut 14 is fixedly connected with bottom plate 1, is provided with insulating layer on the inner wall of cooler bin 5.
The rapid equipment of crystallisation by cooling of this kind of chemistry passes through support rod by the way that support rod 14 is arranged in the bottom of cooler bin 5
14 are fixedly connected with bottom plate, keep the fixed effect of cooler bin 15 more preferable, and do not influence to switch the valve on discharge nozzle 15, and pass through
Insulating layer is set on the inner wall of cooler bin 5, keeps solution crystallisation by cooling effect more preferable.
Attached Fig. 1 and 2 please be considered and examined emphatically, be all provided on the first gas-guide tube 8, escape pipe 10, feed pipe 13 and discharge nozzle 15
Valve, storage bin 6 are internally provided with ice cube, and the bottom end of cooler bin 5 is funnel-shaped, and cooler bin 5 is transparent glass material.
The rapid equipment of crystallisation by cooling of this kind of chemistry passes through in the first gas-guide tube 8, escape pipe 10, feed pipe 13 and discharge nozzle 15
Upper setting valve makes to form a closed space in cooler bin 5, keeps solution cooling effect more preferable, and is used to adjust by valve
The speed of charging, the discharging of the discharge capacity and solution of section cold air and hot gas passes through ice cube by placing ice cube in storage bin 6
The cold air of volatilization carries out crystallisation by cooling to solution, keeps cooling effect more preferable, by the way that funnel is arranged in the bottom of cooler bin 5
, flow out solution preferably from discharge nozzle 15, and cooler bin 5 uses transparent glass material, convenient for molten in observation cooler bin 5
Liquid crystallizes situation.
Shaft 3: before use, first motor 2 is mounted in protective cover 16, being mounted on the output end of motor 2 by working principle,
Then stirring blade 4 is mounted on to the outside of shaft 3, so that shaft 3 and stirring blade 4 is located at the inside of cooler bin 5, by ice cube
It is placed on the inside of storage bin 5, then air pump 7 is mounted in storage bin 6, the first gas-guide tube 8 is mounted on to the pumping of air pump 7
The end of first gas-guide tube 8, is through to the inside of storage bin 6, then the second gas-guide tube 9 is mounted on to the output of air pump 7 by end
End, is through to cooler bin 5 for the end of the second gas-guide tube 9, is mounted on the bottom end of 5 side of cooler bin, then leads to filter screen 11
The top that deck is placed on collecting box 12 is crossed, collecting box is mounted on to the bottom of bottom plate 1 by the mutual cooperation of card slot and fixture block
Solution is entered in cooler bin 5 from feed pipe 13, is closed on feed pipe 13 in use, opening the valve on feed pipe 13 by portion
Valve is opened the valve on the first gas-guide tube 8, is powered on, and air pump 7 volatilizees ice cube in storage bin 6 from the first gas-guide tube 8
Cold air extraction, is passed through in cooler bin 5 by the second gas-guide tube 9, opens the valve on escape pipe 10, cold by the density ratio of hot gas
The density of gas is small, and hot gas is raised above, and exchanges hot gas and cold air in cooler bin 5 rapidly, improves work efficiency, hot gas and
When cold air is exchanged to a certain extent, the valve on escape pipe 10 is closed, crystallisation by cooling, electricity are carried out to the solution inside cooler bin 5
Machine 2 drives shaft 3 to rotate, so that stirring blade 4 be driven to rotate, is stirred to the solution in cooler bin 5, keeps solution cooling
Uniformly, keep crystallization effect more preferable, after the completion of solution crystallisation by cooling, open the valve on discharge nozzle 15, the solution after crystallisation by cooling
From discharge nozzle 15 outflow enter collecting box 12 in, solution and crystallization are separated by filter screen 11, to solution and crystallize into
Row is collected.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
Claims (6)
1. a kind of rapid equipment of crystallisation by cooling of chemical solution, including bottom plate (1), it is characterised in that: one at the top of the bottom plate (1)
Side is provided with cooler bin (5), and the other side at the top of the bottom plate (1) is provided with storage bin (6), the top of the storage bin (6)
It is equipped with air pump (7), the outlet side of the air pump (7) is provided with the second gas-guide tube for being through to cooler bin (5) interior side
(9), the pumping end of the air pump (7) is provided with the first gas-guide tube (8) for being through to storage bin (6) inner tip, the cooling
Be provided at the top of case (5) protective cover (16), the inside of the protective cover (16) is equipped with motor (2), the motor (2) it is defeated
Outlet is provided with the shaft (3) through cooler bin (5) inner tip, and multiple groups stirring is evenly arranged on the outside of the shaft (3)
Blade (4), and the number of stirring blade (4) be three groups, the cooler bin (5) close to air pump (7) side top be provided with into
Expects pipe (13), the cooler bin (5) are provided with escape pipe (10) far from the top of air pump (7) side, the bottom of the cooler bin (5)
Portion is provided with the discharge nozzle (15) being through to below bottom plate (1), is provided with collecting box (12) below the bottom plate (1), described
The four corners of bottom plate (1) bottom are all provided with supporting leg (17).
2. the rapid equipment of crystallisation by cooling of a kind of chemical solution according to claim 1, it is characterised in that: the bottom plate (1)
Bottom be provided with two groups of card slots, the two sides at the top of the collecting box (12) are all provided with the fixture block to match with card slot, and receive
Header (12) is detachably connected by fixture block and card slot with bottom plate (1), the collecting box (12) be located at discharge nozzle (15) just under
Side.
3. the rapid equipment of crystallisation by cooling of a kind of chemical solution according to claim 1, it is characterised in that: the collecting box
(12) internal top is provided with filter screen (11), and the both ends at the top of the filter screen (11) are all provided with deck, and filter screen
(11) it is detachably connected by deck with collecting box (12).
4. the rapid equipment of crystallisation by cooling of a kind of chemical solution according to claim 1, it is characterised in that: the cooler bin
(5) two sides of bottom are all provided with support rod (14), and cooler bin (5) is fixedly connected by support rod (14) with bottom plate (1), institute
It states and is provided with insulating layer on the inner wall of cooler bin (5).
5. the rapid equipment of crystallisation by cooling of a kind of chemical solution according to claim 1, it is characterised in that: first air guide
Valve is all provided on pipe (8), escape pipe (10), feed pipe (13) and discharge nozzle (15).
6. the rapid equipment of crystallisation by cooling of a kind of chemical solution according to claim 1, it is characterised in that: the storage bin
(6) be internally provided with ice cube, the bottom end of the cooler bin (5) is funnel-shaped, and cooler bin (5) be transparent glass material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821101933.XU CN208678420U (en) | 2018-07-12 | 2018-07-12 | A kind of rapid equipment of crystallisation by cooling of chemical solution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821101933.XU CN208678420U (en) | 2018-07-12 | 2018-07-12 | A kind of rapid equipment of crystallisation by cooling of chemical solution |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208678420U true CN208678420U (en) | 2019-04-02 |
Family
ID=65880377
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821101933.XU Expired - Fee Related CN208678420U (en) | 2018-07-12 | 2018-07-12 | A kind of rapid equipment of crystallisation by cooling of chemical solution |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208678420U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112485165A (en) * | 2020-11-18 | 2021-03-12 | 青岛科技大学 | Online measurement device for size and shape of crystal in high solid content crystallization process |
| CN113877236A (en) * | 2021-12-09 | 2022-01-04 | 东营威联化学有限公司 | Auxiliary device for producing paraxylene |
-
2018
- 2018-07-12 CN CN201821101933.XU patent/CN208678420U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112485165A (en) * | 2020-11-18 | 2021-03-12 | 青岛科技大学 | Online measurement device for size and shape of crystal in high solid content crystallization process |
| CN113877236A (en) * | 2021-12-09 | 2022-01-04 | 东营威联化学有限公司 | Auxiliary device for producing paraxylene |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190402 Termination date: 20200712 |