CN208607172U - Determination of moisture device in a kind of liquid - Google Patents

Determination of moisture device in a kind of liquid Download PDF

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Publication number
CN208607172U
CN208607172U CN201821221342.6U CN201821221342U CN208607172U CN 208607172 U CN208607172 U CN 208607172U CN 201821221342 U CN201821221342 U CN 201821221342U CN 208607172 U CN208607172 U CN 208607172U
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liquid
determination
connect
unit
tube
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CN201821221342.6U
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Inventor
尹荣林
刘汗青
武梦琦
李秀林
肖荣海
滕亚君
陆颖
白明懂
邢翠敏
杨富权
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Ruili Entry-Exit Inspection And Quarantine Bureau Inspection And Quarantine Comprehensive Technical Center (yunnan International Travel Health Center Ruili Branch Center)
Ruili Inspection And Certification Co Ltd
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Ruili Entry-Exit Inspection And Quarantine Bureau Inspection And Quarantine Comprehensive Technical Center (yunnan International Travel Health Center Ruili Branch Center)
Ruili Inspection And Certification Co Ltd
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Abstract

The utility model relates to determination of moisture devices in a kind of liquid, belong to Water content determination engineering device technique field in crude oil, determination of moisture device includes atomization unit, gasification unit, condenser pipe, receiver in the liquid, the atomization unit is connect with gasification unit, gasification unit is connect with condenser pipe, and receiver is connect with atomization unit, condenser pipe respectively.After the utility model is atomized liquid using electrospray device, the droplet that ring shaped heating mechanism rises atomization is vaporized, and solvent and moisture continuously separate in the receiver and achievees the purpose that measure moisture after condensation.Improve working efficiency, reduction working time;Save organic reagent;It thoroughly solves the problems, such as bumping, improves laboratory safety;Unattended, reduction manual labor's cost is realized simultaneously.

Description

Determination of moisture device in a kind of liquid
Technical field
The utility model belongs to Water content determination engineering device technique field in crude oil, specific land tax, is related to water in a kind of liquid Divide content testing device.
Background technique
Moisture teller is widely used in the numerous areas such as pharmacy, daily-use chemical industry, food, agricultural, laboratory, in answering for petroleum It needs to be measured the moisture in petroleum with middle, whether the quality to determine petroleum is qualified, and moisture teller belongs to close instrument Device, in actual operation, it is sometimes desirable to move instrument to scene and operate, in actual operation, it is sometimes desirable to remove instrument It is operated to scene, it is very careful during carrying because there is movable part in instrument, it also inevitably will cause component Between displacement, cause measurement data inaccuracy.
Also, conventional moisture content determining device is directly added to the round bottom beaker for filling sample and solvent using heating cap Heat, heating condition is not easy to control, and easy bumping needs Attended mode.
Utility model content
In order to solve the problems, such as background technique, the utility model provides determination of moisture dress in a kind of liquid It sets, after being atomized using electrospray device to liquid, then electricity consumption vapourizing unit is vaporized collection to atomized drop again, thus Bumping problem is thoroughly solved, laboratory safety is improved, while realizing unattended, raising working efficiency.
To achieve the above object, the utility model is achieved by the following technical solution:
Determination of moisture device includes atomization unit 1, gasification unit 2, condenser pipe 3, receiver 4 in the liquid, The atomization unit 1 is connect with gasification unit 2, and gasification unit 2 is connect with condenser pipe 3, receiver 4 respectively with atomization unit 1, condenser pipe 3 connects, and atomization unit 1 is attached by the way of being threadedly coupled with gasification unit 2.
Further, the atomization unit 1 includes spray chamber 5, hollow metal tube 6, ultrasonic atomizer 7, spray chamber upper cover 8, return pipe 9, spray chamber upper cover 8 is provided at the top of the spray chamber 5, and ultrasonic atomizer 7 is arranged in spray chamber 5, is used for The lower end of hollow metal tube 6 for placing 7 power supply line of ultrasonic atomizer is connect with ultrasonic atomizer 7, the upper end of hollow metal tube 6 from The upper end of spray chamber upper cover 8 is pierced by and is fixed in spray chamber upper cover 8, is provided in spray chamber upper cover 8 and connect with receiver 4 Return pipe 9.
Further, the gasification unit 2 includes vaporizer 10, heating coil 11, heater 12, vaporizer 10 and atomization Room 5 is connected to, and helically wound heating coil 11 on it is arranged in the outer wall of vaporizer 10, and heating coil 11 and heater 12 connect It connects.
Further, the condenser pipe 3 includes outer tube 13 and the inner tube 14 being applied in outer tube 13, outer tube 13 and inner tube The accommodating chamber for containing recirculated cooling water is reserved between 14,13 lower end of outer tube is provided with cooling water inlet 15, and upper end is set It is equipped with cooling water liquid outlet 16, the bottom end of inner tube 14 is connect with vaporizer 10, and the lower end of inner tube 14 is provided with to be connect with receiver 4 Manifold 17.
Further, the receiver 4 includes upper inlet tube 18, lower inlet tube 19, cushion chamber 20, liquid storage pipe 21, described The top of cushion chamber 20 be provided with the upper inlet tube 18 connecting with condenser pipe 3, the side of cushion chamber 20 is provided with single with atomization The lower inlet tube 19 of 1 connection of member, cushion chamber 20 are provided with liquid storage pipe 21.
Further, it is provided on the liquid storage pipe 21 convenient for reading the graduation mark of liquid storage amount.
The utility model has the beneficial effects that
After the utility model is atomized liquid using electrospray device, then electricity consumption vapourizing unit again to atomized drop into Row vaporization is collected, and is improved working efficiency, is reduced the working time significantly;Organic reagent dosage is small, saves 90% organic reagent;Thoroughly It solves the problems, such as bumping, improves laboratory safety;Unattended, reduction manual labor's cost is realized simultaneously.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the structural schematic diagram of the utility model atomization unit;
Fig. 3 is the structural schematic diagram of the utility model gasification unit;
Fig. 4 is the structural schematic diagram of the utility model condenser pipe;
Fig. 5 is the structural schematic diagram of the utility model receiver.
In figure, 1- atomization unit, 2- gasification unit, 3- condenser pipe, 4- receiver, 5- spray chamber, 6- hollow metal tube, 7- Ultrasonic atomizer, 8- spray chamber upper cover, 9- return pipe, 10- vaporizer, 11- heating coil, 12- heater, 13- outer tube, 14- Outlet tube, 20- buffering under inner tube, 15- cooling water inlet, 16- cooling water liquid outlet, 17- manifold, the upper inlet tube of 18-, 19- Chamber, 21- liquid storage pipe.
Specific embodiment
Below in conjunction with the utility model embodiment and attached drawing, the technical scheme in the embodiment of the utility model is carried out clear Chu is fully described by, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole realities Apply example.Based on the embodiments of the present invention, those of ordinary skill in the art institute without making creative work The every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Figure 1, determination of moisture device includes atomization unit 1, gasification unit 2, condenser pipe in the liquid 3, receiver 4, the atomization unit 1 are connect with gasification unit 2, and gasification unit 2 is connect with condenser pipe 3, and receiver 4 is distinguished It is connect with atomization unit 1, condenser pipe 3, atomization unit 1 is attached by the way of being threadedly coupled with gasification unit 2.
As shown in Fig. 2, the atomization unit 1 is including on spray chamber 5, hollow metal tube 6, ultrasonic atomizer 7, spray chamber Lid 8, return pipe 9 are provided with spray chamber upper cover 8, spray chamber 5 and spray chamber upper cover 8 at the top of the spray chamber 5 and are connected using screw thread The mode connect connects, easy to disassemble.Ultrasonic atomizer 7 is arranged in spray chamber 5, for placing 7 power supply line of ultrasonic atomizer The lower end of hollow metal tube 6 is connect with ultrasonic atomizer 7, and the upper end of hollow metal tube 6 is pierced by simultaneously from the upper end of spray chamber upper cover 8 It is fixed in spray chamber upper cover 8, the return pipe 9 connecting with receiver 4 is provided in spray chamber upper cover 8.Using ultrasonic atomizer 7 By the sample liquids atomization in spray chamber 5, the fog formed after sample liquids atomization is discharged by 8 return pipe 9 of spray chamber upper cover It is collected by receiver 4, gasification unit 2 can also be imported by top port and is vaporized processing again.Sample liquids and sample Moisture in liquid carries out atomization process at room temperature (i.e. the temperature of sample), and the moisture in sample and sample is temperature-resistant, this Sample can both eliminate the phenomenon that directly heating sample easy bumping.
As shown in figure 3, the gasification unit 2 include vaporizer 10, heating coil 11, heater 12, vaporizer 10 with Spray chamber 5 is connected to, and helically wound heating coil 11 on it, heating coil 11 and heater is arranged in the outer wall of vaporizer 10 12 connections.Liquid is entered after being atomized in atomization unit 1 in gasification unit 2, under the heat effect of heating coil 11, The fog of vaporizer 10 is vaporized under high temperature action, and gas is entered in condenser pipe 3 and condensed after overflash.Pass through mist Change the atomization droplet risen after unit 1 is atomized to enter in gasification unit 2, under the effect of heater 12, passes through annular-heating Coil 11 rapidly will atomization droplet gasification.
As shown in figure 4, the condenser pipe 3 stated includes outer tube 13 and the inner tube 14 that is applied in outer tube 13, outer tube 13 with it is interior The accommodating chamber for containing recirculated cooling water is reserved between pipe 14,13 lower end of outer tube is provided with cooling water inlet 15, upper end It is provided with cooling water liquid outlet 16, the bottom end of inner tube 14 is connect with vaporizer 10, and the lower end of inner tube 14 is provided with to be connected with receiver 4 The manifold 17 connect.Gas after being gasified by gasification unit 2 enters in the inner tube 14 of condenser pipe 3, from the cooling water of outer tube 13 Inlet 15 constantly guides the coolant into coolant liquid accommodating chamber, after liquid to be cooled fills coolant liquid accommodating chamber, then passes through Coolant liquid is discharged manifold 17, is cooled down by the way of being constantly passed through coolant liquid to the gas in inner tube 14, in inner tube 14 Gas be cooled after liquefaction and fall along 14 tube wall of inner tube, then imported into receiver 4 and be collected by manifold 17.
As shown in figure 5, the receiver 4 includes upper inlet tube 18, lower inlet tube 19, cushion chamber 20, liquid storage pipe 21, institute The top for the cushion chamber 20 stated is provided with the upper inlet tube 18 connecting with condenser pipe 3, and the side of cushion chamber 20 is provided with and is atomized The lower inlet tube 19 that unit 1 connects, cushion chamber 20 are provided with liquid storage pipe 21, are provided on the liquid storage pipe 21 convenient for reading storage The graduation mark of liquid measure.Be atomized droplet gasification after enter condenser pipe 3 be condensed back after, receiver 4 20 moisture of cushion chamber with Organic reagent separation, moisture are sunk in liquid storage pipe 21, and extra organic reagent flows back into spray chamber 5 by lower inlet tube 19, To realize the continuous separation of moisture in liquid, moisture is sunk in liquid storage pipe 21 with a scale, reaches moisture in measurement liquid The purpose of content.
The present apparatus uses atomization unit, makes to fill the spray chamber 5 of sample and solvent under the conditions of room temperature (i.e. sample temperature) It carries out, thoroughly solves bumping problem, improve laboratory safety, while realizing unattended, improve work efficiency, it is organic Reagent dosage is small, saves organic reagent.
After the utility model is atomized liquid using electrospray device, then electricity consumption vapourizing unit again to atomized drop into Row vaporization is collected, and is improved working efficiency, is reduced the working time significantly;Organic reagent dosage is small, saves 90% organic reagent;Thoroughly It solves the problems, such as bumping, improves laboratory safety;Unattended, reduction manual labor's cost is realized simultaneously.
Finally, it is stated that above embodiments are merely intended for describing the technical solutions of the present application, but not for limiting the present application, although logical It crosses above preferred embodiment the utility model is described in detail, however, those skilled in the art should understand that, can To make various changes to it in the form and details, without departing from defined by the utility model claims book Range.

Claims (6)

1. determination of moisture device in a kind of liquid, it is characterised in that: determination of moisture device includes in the liquid Atomization unit (1), gasification unit (2), condenser pipe (3), receiver (4), the atomization unit (1) with gasification unit (2) Connection, gasification unit (2) are connect with condenser pipe (3), and receiver (4) is connect with atomization unit (1), condenser pipe (3) respectively, atomization Unit (1) is attached by the way of being threadedly coupled with gasification unit (2).
2. determination of moisture device in a kind of liquid according to claim 1, it is characterised in that: the atomization unit It (1) include spray chamber (5), hollow metal tube (6), ultrasonic atomizer (7), spray chamber upper cover (8), return pipe (9), the mist Change and be provided with spray chamber upper cover (8) at the top of room (5), ultrasonic atomizer (7) setting is in spray chamber (5), for placing ultrasonic mist The lower end of hollow metal tube (6) for changing device (7) power supply line is connect with ultrasonic atomizer (7), and the upper end of hollow metal tube (6) is from mist The upper end for changing room upper cover (8) is pierced by and is fixed on spray chamber upper cover (8), is provided in spray chamber upper cover (8) and receiver (4) The return pipe (9) of connection.
3. determination of moisture device in a kind of liquid described in -2 any one according to claim 1, it is characterised in that: described Gasification unit (2) include vaporizer (10), heating coil (11), heater (12), vaporizer (10) and spray chamber (5) are even Logical, helically wound heating coil (11) on it, heating coil (11) and heater is arranged in the outer wall of vaporizer (10) (12) it connects.
4. determination of moisture device in a kind of liquid according to claim 1, it is characterised in that: the condenser pipe (3) include outer tube (13) and the inner tube (14) being applied in outer tube (13), reserved between outer tube (13) and inner tube (14) useful In the accommodating chamber for containing recirculated cooling water, outer tube (13) lower end is provided with cooling water inlet (15), and upper end is provided with cooling water The bottom end of liquid outlet (16), inner tube (14) is connect with vaporizer (10), and the lower end of inner tube (14) is provided with to be connect with receiver (4) Manifold (17).
5. determination of moisture device in a kind of liquid according to claim 1,2 or 4, it is characterised in that: described connects Receiving device (4) includes upper inlet tube (18), lower inlet tube (19), cushion chamber (20), liquid storage pipe (21), the cushion chamber (20) Top is provided with the upper inlet tube (18) connecting with condenser pipe (3), and the side of cushion chamber (20) is provided with atomization unit (1) even The lower inlet tube (19) connect, cushion chamber (20) are provided with liquid storage pipe (21).
6. determination of moisture device in a kind of liquid according to claim 5, it is characterised in that: the liquid storage pipe (21) it is provided on convenient for reading the graduation mark of liquid storage amount.
CN201821221342.6U 2018-07-31 2018-07-31 Determination of moisture device in a kind of liquid Active CN208607172U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821221342.6U CN208607172U (en) 2018-07-31 2018-07-31 Determination of moisture device in a kind of liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821221342.6U CN208607172U (en) 2018-07-31 2018-07-31 Determination of moisture device in a kind of liquid

Publications (1)

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CN208607172U true CN208607172U (en) 2019-03-15

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108614002A (en) * 2018-07-31 2018-10-02 瑞丽中检检验认证有限公司 Determination of moisture device in a kind of liquid

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108614002A (en) * 2018-07-31 2018-10-02 瑞丽中检检验认证有限公司 Determination of moisture device in a kind of liquid
CN108614002B (en) * 2018-07-31 2024-08-30 瑞丽中检检验认证有限公司 Device for measuring moisture content in liquid

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