CN208588686U - Online nytron water content of matter and pure oil density analyze skid system - Google Patents
Online nytron water content of matter and pure oil density analyze skid system Download PDFInfo
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Abstract
The utility model belongs to water content in oil detection technique field, is related to online nytron water content of matter and pure oil density analysis skid system.Online nytron water content of matter provided by the utility model and pure oil density analyze skid system, including the sampler being measured on medium pipeline, the bearing analysis being connected with sampler sled main body and data collection system is arranged in；The bearing analysis sled main body includes being sequentially connected the filter device connect, sampling pump, density measuring equipment and analyzer of water content；The density measuring equipment and analyzer of water content are electrically connected the data collection system.The system, which realizes, in real time, efficiently monitors the moisture content of hydrocarbon and the online of quality, the interference for reducing human factor and oil product change of component are to the influence containing water gaging, improve reliability, the accuracy of measurement data, it can obtain high performance measured value, it is easy to accomplish industrial applications.
Description
Technical field
The utility model belongs to water content in oil detection technique field, is related to online nytron water content of matter and pure oil is close
Degree analysis skid system.
Background technique
The moisture content and pure oil density of online hydrocarbon (crude oil and its refining product) analyze demand, are widely present in
The storage and transportation of the crude oil production process and finished product crude oil of oil-gas mining, handover, petrochemical industry/oil refining enterprise feedstock oil, such as crude oil and again
(slag) oil and downstream refining product such as petrol and diesel oil and other light components refine the transmission & distribution handover, life of product, heavy oil, fuel oil etc.
In the quality control of production and the process control of oil refining production.Since the component fluctuation of the different crude oil of the place of production, batch is very big, and
Refining product, there is also the fluctuations of purity, density, and especially these oil products are all to be transported by way of sea-freight from the seller mostly
To buyer, especially international oil product trade, and inevitably water ballast is mixed into shipment so that influencing magnitude
Join or directly influence the quality of oil product.
In in the past few decades, the component and product due to oil product are monitored to the online moisture content of crude oil and its refining product
Matter fluctuates and one as industry denounces greatly.Fluctuation of many online bearing analysis products applied in the market due to this component
And it can not accurately measure the moisture content of oil product and finally end in failure.Due to the sensing of online bearing analysis product utilization
Device is different and unified technique standard and criterion in none whole world up to now.Finally have to using on-line period+experiment
The mode of room analysis carries out aqueous and oil density analysis, but whether this method is again equal by oil mixing with water in pipeline
The problem of whether sample that is even and obtaining can really represent the truth of oil mixing with water inside pipeline, there are also take automatically
Whether sample device uses enclosed sampling bottle also to influence whether finally to analyze quality；In addition a whole set of sampling system return line size compared with
Small, impurity, wax deposition and the wall built-up being highly prone in crude oil product influence and cause pipeline blockage.Therefore, on-line period+reality of oil product
It tests room analysis method in the actual operation process or there is very big uncertainty and noncontinuity operation, it is likely that because of people
The result of final moisture content and density analysis is influenced for enchancement factors such as, equipment.
Therefore, online moisture content and pure oil density a kind of reliable, continuous, that be preferably minimized random error are found
(quality) analytical equipment just becomes particularly important.
For a long time, each petrochemical industry, Petrochemical Enterprises used the online water cut monitor instrument of a large amount of imports, domestic crude oil,
But effective, successfully application is never obtained, what this also became in industry one denounces greatly.The online water-containing machine of crude oil at present
Microwave method is in the majority, and main representative producer has: mutually moving (the microwave absorption method of Phase-Dynamics and Agar company, the U.S. in the U.S.
Microwave method (plug-in type representative) and U.S. Ai Mosheng under Roxar company microwave resonance principle based on full-bore
(duct type) deisgn product；The online water content in oil analyzer of the condenser type principle of Canadian Delta C；There are also domestic with Jinzhou
Brocade grinds the product of the radio frequency principle for representative.Several products in addition to the raw Roxar of Ai Mo are refined oil at home and production of hydrocarbons field
There is extensive practice, but finally cannot all meet the needs of production.Thus, crude oil water containing analysis means use at most at present
Or lab analysis is carried out with the way of distillation after automatic or manual sampling.But sampling+lab analysis is still difficult to accomplish reality
When, accurately carry out Water in oil amount analysis, error is larger, this is because sampling when it is difficult to ensure that the sample got is exactly to manage
The sample of practical aqueous distribution in road because mixing is critically important, no matter the aqueous situation of height all.Also, bring back to experiment
Room carries out moisture content analysis, and the chemical examination time is long, and labor intensity, manpower and material resources consume more, dangerous environmental protection.And since crude oil produces
Ground, component, quality is different, also results in online analyzer of water content and is difficult meet the needs of existing frequent switching.
Present bearing analysis instrument online on the market no matter import or homemade goods, do not have the automatic component of oil product and repair
Orthofunction.When oil product change of component, that is, when density changes, the method required manually is sampled through testing
The moisture content that room analysis obtains manually is returned to zero with instrument detection moisture content, to eliminate change of component to the shadow containing water gaging
It rings.It carries out above and it is assumed that oil mixing with water condition is highly desirable.But in fact, oil mixing with water is difficult to protect
Card is uniform.For so, if the oil product of oil refining enterprise very diversity, such as with regard to same root crude oil pipeline, by Zhenghai
Refinery participates in the crude oil pipeline that pipeline reconciles and is tested, it was concluded that almost will more change oil every 1-2 days kind.This
If sample, it is meant that will resample analysis and zeroing when changing oil product, just can guarantee the elimination of oil product components influence, this
In do not consider that just same 100,000 cubes of petroleum tank abhiseca and bottom component change influence to measurement also.But practical this oil
The variation of product component is difficult to track, and the way of this frequent adjustment meter parameter is that oil refining enterprise is unacceptable.
In consideration of it, special propose the utility model.
Utility model content
The first of the utility model is designed to provide a kind of online nytron water content of matter and pure oil density analysis sled
Base system, which, which realizes, in real time, efficiently monitors the moisture content of hydrocarbon and the online of quality, reduces artificial
The interference of factor and oil product change of component improve reliability, the accuracy of measurement data, can obtain to the influence containing water gaging
To high performance measured value, it is easy to accomplish industrial applications.
To achieve the above object, the technical solution adopted in the utility model are as follows:
One aspect according to the present utility model, the utility model provide a kind of online nytron water content of matter and pure oil
Density analysis skid system, it is aqueous including the sampler being measured on medium pipeline is arranged in, is connected with the sampler
Analysis sled main body and data collection system；
Bearing analysis sled main body includes being sequentially connected the filter device connect, sampling pump, density measuring equipment and aqueous
Analyzer；
The density measuring equipment and analyzer of water content are electrically connected the data collection system.
As further preferred technical solution, the analyzer of water content includes the online analyzer of water content of microwave type and/or penetrates
The online analyzer of water content of frequency formula；
Preferably, the online analyzer of water content of the microwave type includes the online analyzer of water content based on microwave resonance principle
And/or the online analyzer of water content of microwave absorption principle；
Preferably, the analyzer of water content is the online analyzer of water content of Roxar microwave resonance.
As further preferred technical solution, the density measuring equipment is intelligent online densitometer；
Preferably, the density measuring equipment is online coriolis force densitometer or the coriolis force flowmeter with density output；
Preferably, the mounting means of the density measuring equipment is vertically-mounted.
As further preferred technical solution, the filter device includes y-type filter and/or magnetic filter；
Preferably, the filter device is y-type filter；
Preferably, differential pressure transmitter, the differential pressure transmitter and the number are connect by the inlet and outlet both ends of the filter device
It is electrically connected according to acquisition system.
As further preferred technical solution, the sampling pump is booster pump；
Preferably, the input end of the sampling pump is provided with threeway before pump；
Preferably, the outlet end of the sampling pump is provided with threeway after pump.
As further preferred technical solution, the bearing analysis sled main body further includes sampling valve and artificial sample mouth, is used
In artificial sample；The sampling valve and artificial sample mouth are connect with the outlet of the analyzer of water content；
Preferably, the bearing analysis sled main body further includes the sampling valve with contact output, the adopting with contact output
Sample valve is connect with the outlet of the analyzer of water content, and the sampling valve with contact output is also electrically connected with the data collection system
It connects.
As further preferred technical solution, the sampler is hub spoke multiple spot oil sampling device；
Preferably, the sampler includes installation pipe fitting, hub spoke multiple spot oil sampling pipe fitting and return pipe；The installation
The outer wall of pipe fitting is equipped with the connector for connecting with measured medium pipeline, and the return pipe and the installation pipe fitting connect
It is logical；
Preferably, the sampler is prized the filter device in main body with bearing analysis by sampling valve and is connect；
Preferably, the sampler is prized the analyzer of water content in main body with bearing analysis by return valve and is connect；
Preferably, connecting tube is provided between the sampler and filter device and/or analyzer of water content.
As further preferred technical solution, the data collection system include for acquire or receiving sensor and/or
The data acquisition unit of the data information of analysis instrument, for carrying out data acquisition unit data information obtained at analysis
The data analysis and processing unit of reason for storing the data information after the data analysis and processing unit, and is the data
Analysis and processing unit provides the data storage cell of data information, and the output list for exporting above-mentioned data to user terminal
Member；
Preferably, output end with wireless remote the transmission receiving unit of the data collection system are connect；
Preferably, the data collection system and cloud server are wirelessly connected.
As further preferred technical solution, the density measuring equipment and analyzer of water content transmit electricity by signal respectively
Cable connects data collection system；
Preferably, the data acquisition unit acquires density signal, the flow/flow velocity letter that the density measuring equipment measures
Number and the amplitude signal that issues of driving coil, and send a signal to data analysis and processing unit and be analyzed and processed；
Preferably, the data acquisition unit acquires the moisture content signal and temperature signal that the analyzer of water content measures,
And it sends a signal to data analysis and processing unit and is analyzed and processed；
Density signal, flow/flow velocity signal, temperature signal and moisture content signal are preferably based on, at the data analysis
Reason unit is modified moisture content signal by temperature, is modified to moisture content signal by density, further to moisture content
Signal by density be segmented in the way of be modified；Correcting mode is segmented by using density to eliminate oil and water zonation form or oil
Product viscosity height is different to be influenced caused by measurement result, to obtain accurately aqueous rate score.
It further include alarm as further preferred technical solution, the alarm is connect with the data collection system.
Compared with prior art, the utility model has the beneficial effects that:
1, skid system provided by the utility model, be provided with sampler, filter device, sampling pump, density measuring equipment,
Analyzer of water content and data collection system, by connecting data collection system with density measuring equipment and analyzer of water content respectively
It connects, realizes the influence by oil product change of component to measurement of water ratio and carry out systematic amendment, to eliminate change of component
Influence to measurement of water ratio.The utility model can eliminate change of component and oil and water zonation form or oil viscosity height is different
The influence that result is caused to measurement, obtains high performance measured value, it is ensured that the wide model of hydrocarbon density under ultralow moisture content
The high-performance for enclosing online analyzer of water content when fluctuation advances the industrial applications of online analyzer of water content, can alleviate existing skill
Art needs the problems such as frequently adjustment meter parameter, cumbersome, large labor intensity.Meanwhile the system can also export and represent oil product
The pure oil density of the standard state of quality provides further theoretical foundation for the quality analysis of oil product.
2, the utility model, which realizes, in real time, efficiently monitors the moisture content of hydrocarbon and the online of quality, subtracts
The interference for having lacked human factor and oil product change of component can guarantee online analyzer of water content ultralow the influence containing water gaging
The high-performance of instrument under moisture content, random error is dropped to it is extremely low, have real time and reliability is high, popularization is strong, continuity is good,
The advantage that measurement is accurate, accuracy is high.
Detailed description of the invention
It, below will be right in order to illustrate more clearly of specific embodiment of the present invention or technical solution in the prior art
Specific embodiment or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, it is described below
In attached drawing be that some embodiments of the utility model are not paying creativeness for those of ordinary skill in the art
Under the premise of labour, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is that line nytron water content of matter provided by the embodiment of the utility model and pure oil density analyze skid system knot
Structure schematic diagram；
Fig. 2 is that bearing analysis provided by the embodiment of the utility model prizes main body schematic front view；
Fig. 3 is that bearing analysis provided by the embodiment of the utility model prizes main body schematic top plan view；
Fig. 4 is that bearing analysis provided by the embodiment of the utility model prizes main body schematic side view.
Icon: 1- is measured medium pipeline；2- sampler；3- bearing analysis prizes main body；4- data collection system；
301- filter device；302- sampling pump；303- density measuring equipment；304- analyzer of water content；305- sampling valve；306-
Differential pressure transmitter；Threeway before 307- is pumped；Threeway after 308- pump；309- sampling valve；310- return valve；311- inlet bend；
312- outlet elbow.
Specific embodiment
The embodiments of the present invention are described in detail below in conjunction with embodiments and examples, but ability
Field technique personnel will be understood that following embodiments and embodiment are merely to illustrate the utility model, and be not construed as limitation originally
The range of utility model.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative labor
Every other embodiment obtained under the premise of dynamic, fall within the protection scope of the utility model.The person that is not specified actual conditions, presses
The condition that more solito condition or manufacturer suggest carries out.
In a first aspect, providing a kind of online nytron water content of matter and the analysis of pure oil density at least one embodiment
Skid system, including the sampler being measured on medium pipeline, the bearing analysis being connected with sampler sled master is arranged in
Body and data collection system；
Bearing analysis sled main body includes being sequentially connected the filter device connect, sampling pump, density measuring equipment and aqueous
Analyzer；
The density measuring equipment and analyzer of water content are electrically connected the data collection system.
It should be understood that above-mentioned " hydrocarbon " includes crude oil and its refining product, for specific crude oil and its
Concrete type the utility model of refining product is not particularly limited.
It should be noted that above-mentioned " data collection system " is data acquisition, analysis and output system, the acquisition of abbreviation data
System.
Since in June, 2015, utility model people has found that the Roxar under U.S. Ai Mosheng house flag has a microwave resonance
The online analyzer of water content of the duct type design with heavy wool product density of fraction zero offset capability of principle, it is online close in conjunction with one
Degree meter can be realized as oil product change of component and realize automatic compensating approach to density.But as previously mentioned, in practical applications, encountering
When frequent oil product change of component, which needs frequently adjustment meter parameter, this is that oil refining enterprise is unacceptable.Therefore exist
Almost online bearing analysis is at the state of stopping before Roxar popularization microwave resonance technology+auto zero function.Further
It says:
It will be appreciated by persons skilled in the art that in current online analyzer of water content, it is no matter former using which kind of physics
Reason, being provided to find different moments flows through the oil mixing with water permittivity ε of pipelinemix.And it can be seen using Brueggemann equation
Out, moisture content β not only with oil mixing with water permittivity εmixIt is related, it goes back and pure oily permittivity εoilWith the dielectric constant of water
εwaterIt is related.Brueggemann equation is as follows:
In formula, β is moisture content, εmixTo mix dielectric constant, εwaterFor the dielectric constant of water, εoilIt is normal for pure oily dielectric
Number.
It is (i.e. close to carry out component to oil product by the method for manual sampling when driving to come into operation for analyzer under normal circumstances
Degree) and instantaneous crude oil water content analysis, remember the original moisture content detected value of lower sampling moment instrument, will analyze get it is close
Angle value configuration inputs water-containing machine electronic unit and is set by the deviation between manual analysis water cut value and the original reading value of instrument
Set zero shift value；This is carried out under the premise of current oil product component.Due to the dielectric constant of oil product and the correspondence of density
Relationship can be easily found by being implanted into the database of electronic unit, the dielectric constant including water.Thus, it is supposed that oil product component is not
In the case where change namely density and pure oily dielectric constant it is constant in the case where, then being by the moisture content that instrument detected
It will not be influenced by change of component.And moisture content output accuracy just only has relationship with oil mixing with water degree.But with regard to one 10
For ten thousand cubes of petroleum tank, after cutting water by the standing of a period of time, actually the top and bottom density components of tank are not yet
It can be identical.Therefore, the accuracy of reading of actual instrument will lead to the variation of pure oily dielectric constant because of oil product component difference, that
In this case, the precision of the original reading value of the moisture content of output is difficult to that the number aqueous due to oil water mixture be ensured of
Cause mix change in dielectric constant still as it is pure oil change in dielectric constant caused by oil mixing with water dielectric constant variation? here
It is assumed that oil mixing with water is uniform.But in fact especially in ultralow moisture content (when moisture content is lower than ± 0.2%),
Grease is it is difficult to ensure that being mixed thoroughly.
And the online water-containing machine of Roxar microwave resonance has oil product component zero offset capability auto zero skill in other words
Art.It is combined by the on-line densimeter being mounted near analyzer of water content upstream or downstream with one, passes through oil mixing with water
The real-time measurement of density, to obtain pure oil density, Jie of pure oil is obtained by pure oil density under the premise of known aqueous rate
Electric constant, to obtain moisture content further through Brueggemann equation, moisture content is used as again to be calculated with real-time oil mixing with water density
Pure oil density out just exports measurement of water ratio value in this way by former and later two moisture content fiducial values < 0.001, namely by with
Calculating between lower two formula formulas (1) and formula (2) can be achieved with auto zero technology, to guarantee measurement of water ratio not by oil
The influence of product change of component.
In formula, β is moisture content, εmixTo mix dielectric constant, εwaterFor the dielectric constant of water, εoilIt is normal for pure oily dielectric
Number, ρoilTPFor the initial value of the density of pure oil, ρmixFor hybrid density, ρwaterFor the density of water.
Specific steps can parse are as follows:
Initialization:
Frequency (T, P, the ρ of mixture temperature, pressure, density and mixture are obtained from different sensorsmix, fmix)；
Calculate mixing dielectric constant (εmix)；
Calculate the density being lauched in working condition pressure and temperature and dielectric constant (ρwater, εwater)；
Assuming that under working temperature and pressure condition moisture content and oil density initial value (β, ρoilTP)；
Iteration:
β value before storage；
Calculate εoil=f (ρoilTP)；
Calculate β=f (εmix, εoil, εwater)
Calculate ρoilTP=f (ρmix, β, ρwater)
Above step is repeated until the difference < 0.001 of the β value of previous and new calculating.
In brief, bearing analysis product of the Roxar with Autozero function be by (2) two formula of formula (1) and formula,
Ensure that analyzer of water content is able to achieve to heavy wool during constantly initializing, be iteratively repeated under " ultrahigh speed " operation state
Highly reliable, high-precision measurement when product component changes.Above is exactly Roxar auto zero technology and we are entire
The basis of crude oil water containing analysis performance guarantee.
However, the online analyzer of water content of Roxar is lower to oil mixing with water requirement, the water body diameter in general recommendations oil is less than
Instrument latus rectum 1/10 is the lowest performance marked in the data that can guarantee.Especially when ultralow aqueous, due to weight viscosity of crude
Difference, in identical ultralow moisture content (assuming that water cut value is 0.065%), due to the difference of oil viscosity height, in vacation
If oil and water zonation form and different under moisture content, it is different that this will lead to water-containing machine original output.So in very wide original
Oil density range, such as Zhenghai refinery, pure oil density is from 720kg/m3To 930kg/m3, on the one hand pass through above-mentioned auto zero
Influence when technology is able to solve change of component to measurement, on the other hand it still will receive oil property i.e. oil and water zonation form
Different influence still needs to calibrate instrument fan-out capability when density fluctuation range is larger, that is, re-scales zero,
This just gives the practical application in industry of analyzer of water content to be provided with a big obstacle.Ultralow moisture content especially within ± 0.2%
In the case of, the variation of instrument original output can be fluctuated between 0.9% to 0.2%, but practical moisture content is not so high, can
Can also there was only 0.05% or 0.025%, because the resolution ratio of the way of distillation is just 0.025%.Which increases instrument to contain ultralow
Measurement error under water rate.
Based on this, utility model people develops a set of data acquisition software, i.e., is segmented correcting mode using density to eliminate
Oil and water zonation form is influenced caused by measurement result, and a point density section used by this sets of data acquisition system software is repaired
Positive method enables to the performance of the online bearing analysis of crude oil when the oil density wide swings under ultralow moisture content to obtain
To guarantee.It enables to using Roxar band using this sets of data acquisition system software and modification method of the utility model
Heavy wool product density of fraction zero offset capability (Autozero component debugging functions) realizes more have after line analyzer of water content
Effect ultralow containing underwater industrial application.
Therefore, the utility model, which is provided with, includes sampler, filter device, sampling pump, density measuring equipment, bearing analysis
The line nytron water content of matter and pure oil density of instrument and data collection system analyze skid system, are by acquiring data
System is connect with density measuring equipment and analyzer of water content respectively, realize influence by oil product change of component to measurement of water ratio into
The systematic amendment of row has obtained reliable, accurately data to eliminate influence of the change of component to measurement of water ratio, into
And it realizes and the moisture content of oil product and the online of quality in real time, is efficiently monitored.
In a preferred embodiment, the analyzer of water content includes the online analyzer of water content of microwave type and/or penetrates
The online analyzer of water content of frequency formula；
Preferably, the online analyzer of water content of the microwave type includes the online analyzer of water content based on microwave resonance principle
And/or the online analyzer of water content of microwave absorption principle；
Preferably, the analyzer of water content is the online analyzer of water content of Roxar microwave resonance.
The analyzer of water content of the utility model is preferably using the Roxar under U.S. Ai Mosheng (Emerson) house flag
The online analyzer of water content with heavy wool product density of fraction zero offset capability of microwave resonance principle.I.e. the utility model is with Ai Mo
The microwave resonance technology HighCut type (abbreviation with automatic component debugging functions (Autozero) of Roxar company under raw house flag
0~50% moisture content range of HC type) online bearing analysis product prizes the core sensor of main body as bearing analysis.The product is logical
Crossing can be by commercially available acquisition.But it is not limited to this, those skilled in the art it should be appreciated that, can also select similar
Analyzer or analyzer of water content with similar performance and demand.
In a preferred embodiment, the density measuring equipment is intelligent online densitometer；
Preferably, the density measuring equipment is online coriolis force densitometer or the coriolis force flowmeter with density output.
The density measuring equipment of the utility model preferably section using online coriolis force densitometer or with density output
Family name's force flow meter, measuring device feature with high performance can be shown excellent under severe working environment
Performance has strong antijamming capability, and the pressure loss is small, easy cleaning, high reliablity, and measurement accuracy is high, and installation is simple, the scope of application
The advantages that wide.The density measuring equipment can pass through commercially available acquisition.
Preferably, the mounting means of the density measuring equipment is vertically-mounted.By above-mentioned density measuring equipment it is vertical or
Vertical installation in systems, and fluid bottom in and top out, it is ensured that not entrained gas in densitometer, it is hydraulically full in densitometer,
And then ensure the accuracy of oil density measurement data, the accuracy of the water content in oil data further ensured that.
In a preferred embodiment, the filter device includes y-type filter and/or magnetic filter；
Preferably, the filter device is y-type filter.
The utility model installs filter before sampling pump, can effectively remove the impurity in hydrocarbon
Fall, is conducive to the measurement of subsequent density and moisture content.It is preferred that simple using structure, easy for installation, high treating effect Y
Type filter.
In a preferred embodiment, the sampling pump is booster pump；
Preferably, differential pressure transmitter, the differential pressure transmitter and the number are connect by the inlet and outlet both ends of the filter device
It is electrically connected according to acquisition system.
Booster pump is installed between filter device and density measuring equipment, for guaranteeing that samples taken can reach instrument measurement
Flow velocity required by precision, and guarantee that the measured medium of different viscositys reaches its oil mixing with water under the action of pump and compares
Ideal state (uniform).Differential pressure transmitter is connect by the inlet and outlet both ends of filter device, can be filtered by differential pressure value inspection
Whether device has blocking and issues the prompt of " cleaning filter " by system.
Preferably, the input end of the sampling pump is provided with threeway before pump；The outlet of threeway and filter before pumping；
Preferably, the outlet end of the sampling pump is provided with threeway after pump；The import of threeway and density measuring equipment after pump
Connection.
In a preferred embodiment, the bearing analysis sled main body further includes sampling valve and artificial sample mouth, is used
In artificial sample；The sampling valve and artificial sample mouth are connect with the outlet of the analyzer of water content；
Preferably, the bearing analysis sled main body further includes the sampling valve with contact output, the adopting with contact output
Sample valve is connect with the outlet of the analyzer of water content, and the sampling valve with contact output is also electrically connected with the data collection system
It connects.
Sampling valve and artificial sample mouth are set on the downstream or outlet connecting pipe road of analyzer of water content, using manually adopting
Sample is compared and calibrates to the reliability of the data of systematic survey.
In a preferred embodiment, the sampler is hub spoke multiple spot oil sampling device；
Preferably, the sampler includes installation pipe fitting, hub spoke multiple spot oil sampling pipe fitting and return pipe；The installation
The outer wall of pipe fitting is equipped with the connector for connecting with measured medium pipeline, and the return pipe and the installation pipe fitting connect
It is logical；
Above-mentioned hub spoke multiple spot oil sampling device is preferably using Publication No. CN205958295U, entitled " hub spoke
The hub spoke multiple spot oil sampling device mentioned in the patent of formula multiple spot oil sampling tube assembly and sampler ", the sampler (sampling
Device) by a kind of sampler (sampler) for being researched and developed before utility model people.
Preferably, hub spoke multiple spot oil sampling device, comprising: the outer wall of installation pipe fitting, the installation pipe fitting is equipped with
Connector for being connect with pipeline road (measured medium pipeline)；
Hub spoke multiple spot oil sampling tube assembly, wherein the first subsegment of gathering tube is located at the axis of installation pipe fitting, converges
The second subsegment of general pipeline is drawn from the outer wall of installation pipe fitting；
Return pipe, the return pipe flow back again for fluid sample after will test, the return pipe and installation pipe fitting
Connection.
Wherein, hub spoke multiple spot oil sampling tube assembly, comprising: the side of more sampling single tubes, the sampling single tube is set
There is thieff hatch；Gathering tube, the gathering tube include sampling the first subsegment of single tube and for that will sample single tube acquisition for connecting
Fluid draw pipeline road the second subsegment；More sampling single tubes are installed radially in the first subsegment, and sample single tube
First end be connected to the first subsegment, sample single tube second end closing.
Preferably, the quantity of the thieff hatch is unique, which arranges along the axial of sampling single tube；Preferably, institute
The width for stating thieff hatch is gradually increased in the first end to the second extreme direction of sampling single tube；Preferably, all sampling single tubes
Tilted to the opening direction of thieff hatch；Preferably, the thieff hatch is equipped with multiple, and multiple thieff hatch are along the axis for sampling single tube
It is sampled on single tube to being distributed in；Preferably, the outer wall of the gathering tube is equipped with one week equally distributed multiple threaded hole, described
Threaded hole connects plugging block or sampling single tube.
Preferably, the second subsegment of the gathering tube is equipped with purging valve port, is connected on the purging valve port and reversely blows
Sweeping device；Preferably, the second subsegment of the gathering tube is connect by sampling valve with sample analysis system, and the return pipe passes through
Return valve is connected to installation pipe fitting；It preferably, further include a triple valve, the first end of the triple valve and the second son of gathering tube
Section connection, second end are connect with return pipe, and third end connects a sampling valve.
Preferably, the sampler is prized the filter device in main body with bearing analysis by sampling valve and is connect；
Preferably, the sampler is prized the analyzer of water content in main body with bearing analysis by return valve and is connect；
Preferably, connecting tube is provided between the sampler and filter device and/or analyzer of water content；Further,
It is equipped with inlet bend between the sampler and filter device, it is curved that outlet is equipped between the sampler and the analyzer of water content
Pipe.
In a preferred embodiment, the data collection system include for acquire or receiving sensor and/or
The data acquisition unit of the data information of analysis instrument, for carrying out data acquisition unit data information obtained at analysis
The data analysis and processing unit of reason for storing the data information after the data analysis and processing unit, and is the data
Analysis and processing unit provides the data storage cell of data information, and the output list for exporting above-mentioned data to user terminal
Member；
Preferably, output end with wireless remote the transmission receiving unit of the data collection system are connect；
Preferably, the data collection system and cloud server are wirelessly connected.
Further, the density measuring equipment pass through respectively with analyzer of water content signal-transmitting cable connect data acquisition
System；
Preferably, the data acquisition unit acquires density signal, the flow/flow velocity letter that the density measuring equipment measures
Number and the amplitude signal that issues of driving coil, and send a signal to data analysis and processing unit and be analyzed and processed；It is therein
Amplitude signal can be used for whether display instrument breaks down, i.e., within the scope of certain amplitude signal, densimeter is operated normally, vibration
Width abnormal signal, then it represents that failure occurs in densimeter.
Preferably, the data acquisition unit acquires the moisture content signal and temperature signal that the analyzer of water content measures,
And it sends a signal to data analysis and processing unit and is analyzed and processed.
It should be understood that density sensor, flow/flow sensor, driving coil are equipped in density measuring equipment,
Moisture sensor, temperature sensor are equipped in analyzer of water content, above-mentioned data acquisition unit is adopted respectively by the sensor
Collect the data such as density, flow/flow velocity, moisture content, temperature, acquisition or acquisition modes of the utility model for data, sensor
Concrete form etc. be not described in detail, be that those skilled in the art can learn.
Density signal, flow/flow velocity signal, temperature signal and moisture content signal are preferably based on, at the data analysis
Reason unit is modified moisture content signal by temperature, and because temperature change can cause variable density, and oil density variation is made
Error is generated at the moisture content gone out by Brueggemann equation calculation, so, this detecting device for moisture content is devised according to temperature in real time
It spends to correct the function of this error.The pure oil density that will change under real-time working condition with measured medium temperature change, conversion
For the pure oil density of (15 DEG C) fixations under standard state, and moisture content is calculated by this standard state density；
Moisture content signal is modified by density.Due to the variation of oil product, component also accordingly changes；And oil product
The variation of component can reflect in the variation of oil density, so learning its component by the variable density for detecting oil product
Variation；Oil density variation causes to generate error by the moisture content that Brueggemann equation calculation goes out again, so, the detection of this moisture content
Device devises according to real-time density the function of correcting this error；
Further moisture content signal is modified in the way of being segmented using density；Although temperature and close has been pressed in front
Degree is corrected moisture content, but is unevenly distributed due to aqueous, also can in the density that each moment flows through the oil product of instrument
It has differences, in order to further improve output accuracy, the density of oil product in entire measurement process is segmented into much by system
A minizone, and further corrected for moisture content corresponding between each cell.It is repaired by using density segmentation
Positive way eliminates oil and water zonation form or the different influences caused by measurement result of oil viscosity height, accurately to be contained
Water rate score.
The utility model is the Autozero function based on the configuration of Roxar microwave resonance analyzer of water content and realize will be oily
Influence of the product change of component to measurement of water ratio carries out systematic amendment, to eliminate change of component to measurement of water ratio
It influences.It is incorporated in oil mixing with water density under the operation operating condition that line density measures and utilizes analyzer of water content Autozero software meter
Calculation obtains pure oil density under operating condition, and the online temperature signal calculating measured is being obtained by the temperature sensor on analyzer of water content
Obtain the pure oil density under standard state.So that whole system realizes the detection of the online moisture content of oil product and pure oil density, crude oil is realized
And its in the Quality Detection of refining product important two indices on-line checking.Further, system can be sent by GPRS
To cloud big data server progress remote data management, analysis is carried out to instrument operation data and equipment state is carried out long-range
Diagnosis, configuration and guarantor's fortune service.
Above-mentioned density segmentation revised law includes: to be segmented correcting mode using density to eliminate oil and water zonation form or oil product and glue
Degree height is different to be influenced caused by measurement result, to obtain accurately aqueous rate score.It further include that (its basis is) passes through certainly
Dynamic return zero technique eliminates influence of the oil product change of component to measurement of water ratio.
It further, include: that the oil density of wide swings is divided into several using density segmentation correcting mode
Sub- density section, each sub- density section are corresponding with respective drift correction coefficient；
Sub- density section by oil density value come Automatic-searching corresponding to it, according to density value it is different call it is different
The amendment deviation factor in sub- density section, to eliminate, oil and water zonation form or oil viscosity are just different to cause measurement result
Influence.
Wherein, the density increment value in sub- density section is 2~6kg/m3, preferably 3~5kg/m3；More preferably 3kg/m3
Or 5kg/m3。
It should be noted that the oil density of the wide swings can be understood as oil density in more wide model
Interior fluctuation is enclosed, which may be greater than any range of the incremental value in sub- density section, for example, the original of the wide swings
Oil density can be 720~930kg/m3, 720~900kg/m3, 750~800kg/m3, 750~850kg/m3, 800~
900kg/m3Etc., the utility model does not do excessive limitation to this, can according to the oil types that each oil refining enterprise is included or
The difference of oil density and set.
It is understood that the density increment value in the sub- density section indicate be each sub- density section maximum value
Difference between minimum value, such as oil density range are 850~880kg/m3When, then it can be divided into multiple sons
Density section, comprising: 850~853kg/m3, 853~886kg/m3, 856~860kg/m3, 860~865kg/m3, 865~
868kg/m3, 868~872kg/m3, 872~875kg/m3With 875~880kg/m3。
Further, the mode of drift correction coefficient corresponding to each sub- density section of acquisition includes:
It will first be run 20~40 days after the debugging of crude oil water content monitoring instrument, pass through the change to this 20~40 days oil product kinds
Change the amendment deviation factor obtained between every sub- density region, then by the amendment deviation factor configuration between every sub- density region to data
In the software of acquisition system, to realize subsequent applications in the process for the calling for correcting deviation factor in different sub- density sections.
The data collection system of the utility model, which is able to achieve, is divided into density increment in wider oil density fluctuation range
Value is+3~+5kg/m3Different sub- density sections is corresponding with different drift correction coefficients in different sub- density sections, leads to
It crosses pure oil density and comes Automatic-searching oil property section, the drift correction in different sub- density sections is called according to the difference of density value
Coefficient, to eliminate the influence caused by measurement of oil and water zonation form, this influence is more prominent when ultralow aqueous.
Further speaking, the drift correction coefficient value between every sub- density region can drive first to run after debugging by instrument
One month or so, the drift correction system obtaining every sub- density region by the variation between this month or so crude oil quality kind
Number, it is online aqueous to guarantee by software of the drift correction coefficient configuration between every sub- density region to data collection system
The high-performance of analyzer instrument under ultralow moisture content.
Meanwhile the drift correction coefficient between every sub- density region will receive the influence of the flow velocity of oil water mixture in pipeline,
Within the scope of wide density fluctuation, if flow velocity is higher and stablizes, the original moisture content wave that instrument exports in different density sections
It moves smaller, that is to say, that the drift correction coefficient fluctuation in each sub- density section is also just smaller.Under normal circumstances, recommend in big pipeline
Flow velocity >=1m/s.
The method that point density section is modified used by the software of above-mentioned data collection system is efficiently solved super
The high-performance of the online analyzer of water content of crude oil guarantees when oil density wide swings under low-water-content.It is repaired using density segmentation
Correction method is able to solve online analyzer of water content of the Roxar with Autozero component debugging functions and answers ultralow containing underwater industry
With.
It in a preferred embodiment, further include alarm, the alarm is connect with the data acquisition unit；
Preferably, the alarm is combined aural and visual alarm.It, can when instrument, which breaks down or measures, the abnormal conditions such as goes wrong
Operator is prompted by alarm, and is adjusted, overhauls in real time.
It should be noted that it further includes the accessories such as connecting flange, valve that the skid system of the utility model, which further includes,
The utility model such as its specific structure type, connection type are not particularly limited, and those skilled in the art can be according to reality
Situation carries out configuration appropriate.
The online nytron water content of matter of the utility model and pure oil density analysis skid system can be applied in crude oil
In the fields such as refinery, oil product transaction, oil product clearing.In crude oil refinery, for the safety for guaranteeing refinery device, strict control is needed
The moisture content of crude oil；It is fair to guarantee, it is also desirable to the water content in precise measurement oil product in oil product transaction, clearing.
It should be understood that the content being not described in detail in the utility model specification belongs to this field professional technique people
The prior art well known to member.
Combined with specific embodiments below and attached drawing, the utility model is described in further detail.
Embodiment
As shown in Figures 1 to 4, the present embodiment provides a kind of online nytron water content of matter and pure oil density to analyze skid
System, including the sampler 2 being measured on medium pipeline 1 is arranged in, the bearing analysis being connected with sampler 2 prizes main body 3, with
And data collection system 4；
Bearing analysis sled main body 3 includes being sequentially connected the filter device 301, sampling pump 302, density measuring equipment 303 connect
With analyzer of water content 304, and sampling valve of the setting in 304 downstream of analyzer of water content, with the outlet connection of analyzer of water content 304
305 or artificial sample mouth；
Density measuring equipment 303, analyzer of water content 304 and sampling valve 305 are electrically connected data collection system 4.
Wherein, analyzer of water content 304 is the online analyzer of water content (HC type) of Roxar microwave resonance；Density measuring equipment
303 be online coriolis force densitometer；The mounting means of density measuring equipment 303 is vertically-mounted.
Filter device 301 is y-type filter；Differential pressure transmitter 306, differential pressure are connect by the inlet and outlet both ends of filter device 301
Transmitter 306 is electrically connected with data collection system 4.
Sampling pump 302 is booster pump；The input end of sampling pump 302 is provided with threeway 307 before pump；The outlet of sampling pump 302
End is provided with threeway 308 after pump.
Sampler 2 is hub spoke multiple spot oil sampling device；Sampler 2 includes installation pipe fitting, hub spoke multiple spot oil sampling
Pipe fitting and return pipe；The outer wall of pipe fitting is installed equipped with the connector for connecting with measured medium pipeline, return pipe and peace
The connection of tubulature part.
Sampler 2 is prized the filter device 301 in main body 3 with bearing analysis by sampling valve 309 and is connect；Sampler 2 passes through
Return valve 310 is connect with the analyzer of water content 304 in bearing analysis sled main body 3；It is equipped between sampler 2 and filter device 301
Inlet bend 311 is equipped with outlet elbow 312 between sampler 2 and analyzer of water content 304.
Data collection system 4 includes for acquiring or the data of the data information of receiving sensor and/or analysis instrument are adopted
Collect unit, the data analysis and processing unit for data acquisition unit data information obtained to be analyzed and processed is used for
The data information after data analysis and processing unit is stored, and provides the data storage of data information for data analysis and processing unit
Unit, and the output unit for exporting above-mentioned data to user terminal；Data collection system and cloud server are wirelessly connected.
Density measuring equipment 303 connects data collection system 4 by signal-transmitting cable respectively with analyzer of water content 304；
The amplitude that density signal, flow/flow velocity signal and the driving coil that data acquisition unit acquisition density measuring equipment measures issue
Signal, and send a signal to data analysis and processing unit and be analyzed and processed；Data acquisition unit acquires analyzer of water content and surveys
The moisture content signal and temperature signal obtained, and send a signal to data analysis and processing unit and be analyzed and processed；Based on density
Signal, flow/flow velocity signal, temperature signal and moisture content signal, data analysis and processing unit to moisture content signal by temperature into
Row amendment, moisture content signal is modified by density, further to moisture content signal by density be segmented in the way of carry out
Amendment；Correcting mode is segmented by using density to eliminate oil and water zonation form or oil viscosity height difference and make to measurement result
At influence, to obtain accurately aqueous rate score.
As known from the above, Roxar company below the utility model with the micro- of automatic component debugging functions (Autozero)
The wave online bearing analysis product of resonance technique High Cut type is as core sensor, in conjunction with a high performance online coriolis force
The skid system that densitometer and intelligent data acqusition system form for core component, is aided with the sampling pump in system and is mounted on
The hub spoke multiple spot oil sampling device and intelligent data acqusition system being measured on medium pipeline are carried out according to oil property
It is segmented modified software algorithm, to realize the ultralow moisture content on-line analysis of oil product and obtain highly reliable data, can be passed through
Intelligent data acqusition system carries out remote online data management and device diagnostic service, realizes to the moisture content of oil product and quality
Online in real time, efficiently to monitor, the interference for reducing human factor and oil product change of component are to the influence containing water gaging；System is also
Can be sampled by the way that the manual sampling mouth in analyzer of water content downstream is arranged in the reliability of the data of systematic survey is compared and
Calibration.
Finally, it should be noted that the above various embodiments is only to illustrate the technical solution of the utility model, rather than it is limited
System；Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should
Understand: it is still possible to modify the technical solutions described in the foregoing embodiments, or to some or all of
Technical characteristic is equivalently replaced；And these are modified or replaceed, it does not separate the essence of the corresponding technical solution, and this is practical new
The range of each embodiment technical solution of type.
Claims (10)
1. a kind of online nytron water content of matter and pure oil density analyze skid system, which is characterized in that including being arranged in quilt
Sampler on measuring medium pipeline, the bearing analysis being connected with sampler sled main body and data collection system；
The bearing analysis sled main body includes being sequentially connected the filter device connect, sampling pump, density measuring equipment and bearing analysis
Instrument；
The density measuring equipment and analyzer of water content are electrically connected the data collection system.
2. online nytron water content of matter according to claim 1 and pure oil density analyze skid system, feature exists
In the analyzer of water content is the online analyzer of water content of Roxar microwave resonance.
3. online nytron water content of matter according to claim 1 and pure oil density analyze skid system, feature exists
In the density measuring equipment is online coriolis force densitometer or the coriolis force flowmeter with density output；
And/or the mounting means of the density measuring equipment is vertically-mounted.
4. online nytron water content of matter according to claim 1 and pure oil density analyze skid system, feature exists
In the filter device is y-type filter；
And/or differential pressure transmitter is connect by the inlet and outlet both ends of the filter device, the differential pressure transmitter and the data acquire
System electrical connection.
5. online nytron water content of matter according to claim 1 and pure oil density analyze skid system, feature exists
In the sampling pump is booster pump；
And/or the input end of the sampling pump is provided with threeway before pump；The outlet end of the sampling pump is provided with threeway after pump.
6. online nytron water content of matter according to claim 1 and pure oil density analyze skid system, feature exists
In the bearing analysis sled main body further includes the sampling valve with contact output, and the sampling valve with contact output contains with described
The outlet of water analyzer connects, and the sampling valve with contact output is also electrically connected with the data collection system.
7. described in any item online nytron water content of matter and pure oil density analyze skid system according to claim 1~6,
It is characterized in that, the sampler is hub spoke multiple spot oil sampling device；
And/or the sampler is prized the filter device in main body with bearing analysis by sampling valve and is connect；
And/or the sampler is prized the analyzer of water content in main body with bearing analysis by return valve and is connect.
8. described in any item online nytron water content of matter and pure oil density analyze skid system according to claim 1~6,
It is characterized in that, the data collection system includes for acquiring or the data information of receiving sensor and/or analysis instrument
Data acquisition unit, the Data Analysis Services list for data acquisition unit data information obtained to be analyzed and processed
Member provides number for storing the data information after the data analysis and processing unit, and for the data analysis and processing unit
It is believed that the data storage cell of breath, and for the output unit to user terminal output data；
The data collection system and cloud server are wirelessly connected.
9. online nytron water content of matter according to claim 8 and pure oil density analyze skid system, feature exists
In the density measuring equipment passes through signal-transmitting cable with analyzer of water content respectively and connects data collection system；
The data acquisition unit acquires density signal, flow/flow velocity signal and the driving line that the density measuring equipment measures
The amplitude signal issued is enclosed, and sends a signal to data analysis and processing unit and is analyzed and processed；
The data acquisition unit acquires the moisture content signal and temperature signal that the analyzer of water content measures, and signal is sent
It is analyzed and processed to data analysis and processing unit；
Based on density signal, flow/flow velocity signal, temperature signal and moisture content signal, the data analysis and processing unit is to containing
Water rate signal is modified by temperature, is modified to moisture content signal by density, is further utilized to moisture content signal close
The mode of degree segmentation is modified；Correcting mode is segmented by using density to eliminate oil and water zonation form or oil viscosity height
Difference is influenced caused by measurement result, to obtain accurately aqueous rate score.
10. described in any item online nytron water content of matter and pure oil density analyze skid system according to claim 1~6
System, which is characterized in that further include alarm, the alarm is connect with the data collection system.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108760773A (en) * | 2018-08-21 | 2018-11-06 | 上海东易电气有限公司 | Online nytron water content of matter and pure oil density analyze skid system |
| WO2021066797A1 (en) * | 2019-09-30 | 2021-04-08 | Schlumberger Technology Corporation | Water-in-oil monitoring apparatus and related methods |
| CN112666185A (en) * | 2020-10-27 | 2021-04-16 | 西安交通大学 | Remote crude oil water content measuring device based on microwave transmission method and measuring method thereof |
| RU2803906C1 (en) * | 2019-09-30 | 2023-09-21 | Шлюмбергер Текнолоджи Б.В. | Device for monitoring water content in oil and related methods |
-
2018
- 2018-08-21 CN CN201821347823.1U patent/CN208588686U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108760773A (en) * | 2018-08-21 | 2018-11-06 | 上海东易电气有限公司 | Online nytron water content of matter and pure oil density analyze skid system |
| CN108760773B (en) * | 2018-08-21 | 2024-01-19 | 上海东易电气有限公司 | On-line analysis prying seat system for water content of hydrocarbon and density of pure oil |
| WO2021066797A1 (en) * | 2019-09-30 | 2021-04-08 | Schlumberger Technology Corporation | Water-in-oil monitoring apparatus and related methods |
| RU2803906C1 (en) * | 2019-09-30 | 2023-09-21 | Шлюмбергер Текнолоджи Б.В. | Device for monitoring water content in oil and related methods |
| CN112666185A (en) * | 2020-10-27 | 2021-04-16 | 西安交通大学 | Remote crude oil water content measuring device based on microwave transmission method and measuring method thereof |
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