CN208482438U - A kind of high-purity oleamide extraction element - Google Patents
A kind of high-purity oleamide extraction element Download PDFInfo
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- CN208482438U CN208482438U CN201820712429.7U CN201820712429U CN208482438U CN 208482438 U CN208482438 U CN 208482438U CN 201820712429 U CN201820712429 U CN 201820712429U CN 208482438 U CN208482438 U CN 208482438U
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Abstract
The utility model provides a kind of high-purity oleamide extraction element, is related to oleamide preparation technical field.A kind of high-purity oleamide extraction element, including reaction kettle, the bottom of the reaction kettle is fixedly connected with transverse slat, the lower surface of the fixed transverse slat is fixedly installed with stabilizer blade, riser is fixedly connected on the left of the transverse slat, top on the left of the riser is fixedly connected with loading plate, the lower surface of the loading plate is fixedly connected with motor, the output end of the motor is fixedly connected with bull stick by shaft coupling, the bull stick runs through the hole that reactor bottom opens up and the inner cavity for extending to reaction kettle, and the side surface of the bull stick is fixedly connected with stirring rod.A kind of high-purity oleamide extraction element, by increasing reflux unit, the temperature that oleamide production reaction process can be produced to high-purity oleamide is able to carry out effective control, greatly improves the effect of reaction, the cost for reducing actual production improves the quality of final products.
Description
Technical field
The utility model relates to oleamide preparation technical field, specially a kind of high-purity oleamide extraction element.
Background technique
Currently, oleamide is a kind of important higher fatty acid amide, industrially, oleamide, which is used as lubricant, reduces tree
Rouge melt viscosity, may be used as softening agent and waterproofing agent in fiber industry, be widely used in industries such as ink, dyestuffs.
Derivative of fatty acid is constantly subjected to scholars' concern as the research of steel corrosion inhibiter in neutral aqueous solution medium, it is believed that is one
The good metal erosion corrosion inhibiter of kind.As corrosion inhibiter is ecological towards the development of efficient, nuisanceless and multifunctional direction and people
The further reinforcing of environmental consciousness, more and more researchers attempt to provide chemical barrier layer with fatty acid amide to be matched with enhancing
The corrosion inhibition of product.
There are many chemical routes for preparing oleamide, wherein the route for reacting synthctic fat acid amide with ammonia with fatty acid is
Main in the presence of no catalyst, fatty acid reacted with ammonia synthesis phthalein amine need under high temperature and extra high reaction pressure into
Row.
But there is no a kind of devices of the high-purity oleic acid production oleamide of reasonable utilization at present.It is especially existing
Equipment will not control reaction temperature, cause the quality of reaction to be greatly reduced, to improve production cost.
Utility model content
Technical solution
In order to achieve the above object, the utility model is achieved by the following technical programs: a kind of high-purity oleamide mentions
Device, including reaction kettle are taken, the bottom of the reaction kettle is fixedly connected with transverse slat, and the lower surface of the fixed transverse slat is fixedly mounted
There is stabilizer blade, riser is fixedly connected on the left of the transverse slat, the top on the left of the riser is fixedly connected with loading plate, described to hold
The lower surface of support plate is fixedly connected with motor, and the output end of the motor is fixedly connected with bull stick, the bull stick by shaft coupling
The hole that opens up through reactor bottom and the inner cavity for extending to reaction kettle, the side surface of the bull stick is fixedly connected with stirring
Bar, the stirring rod are located at the inner cavity of reaction kettle, and feed pipe is fixedly connected at the feed inlet at the top of the reaction kettle, described anti-
The air inlet position in kettle top portion is answered to be fixedly connected with air inlet pipe, the side surface of the reaction kettle is provided with heating oil lagging, described to add
Oil outlet on the left of hot-oil jacket is equipped with flowline, and the flowline is fixedly connected with oil drum far from heating oil lagging one end,
Electrothermal tube is fixedly connected at the oil inlet of the oil drum, the oil outlet at the top of the oil drum is fixedly connected with flowline, institute
It states and is fixedly connected at the oil inlet opened up on the left of one end and heating oil lagging of the separate oil drum of flowline, the fuel-displaced appearance
Face is fixedly connected with oil well pump, and the inner cavity of the reaction kettle is provided with temperature sensor, the upper end setting on the left of the reaction kettle
There is Electromagnetic Flow regulating valve, is fixedly connected with drainage conduit at the discharge gate of the reaction kettle lower right-hand side.
Further, there are two the stabilizer blade is arranged altogether, and at the both ends of two stabilizer blades lower section that reaction kettle is set.
Further, the central part of the stabilizer blade is equipped with central spindle, and damping spring, the axis are equipped at the outer wall of central spindle
Damping shell is installed, the lower section of the stabilizer blade is equipped with sawtooth above core.
Further, the stabilizer blade rectangular in cross-section, is made of stainless steel material.
Further, the outer surface of the reaction kettle is fixedly connected with thermal insulation board, and heats oil lagging and be located in thermal insulation board.
Further, the temperature sensor is connected to the Electromagnetic Flow regulating valve, the electromagnetism using pilot
Flow control valve is connected to the oil well pump electricity and heat pipe using pilot.
Beneficial effect
Compare the prior art, the beneficial effects of the utility model are:
1, a kind of high-purity oleamide extraction element, by increase heating oil lagging, flowline, oil drum, electrothermal tube,
Flowline, oil well pump, temperature sensor, Electromagnetic Flow regulating valve and thermal insulation board are used cooperatively, can be to high-purity oleamide
The temperature of production oleamide production reaction process is able to carry out effective control, greatly improves the effect of reaction, reduces
The cost of actual production, improves the quality of final products.
2, a kind of high-purity oleamide extraction element, by increase stabilizer blade, axle center, damping spring, damping shell and
It is more stable in production reaction process can to make reaction kettle for the cooperation of sawtooth, while can also make to heat the heat in oil lagging
Oily heat diffusion it is more uniform, keep the temperature in reaction kettle more stable.
Detailed description of the invention
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is the cross-sectional view of the structure that the utility model is given advice
Wherein, 1 reaction kettle, 2 transverse slats, 3 risers, 4 loading plates, 5 motors, 6 bull sticks, 7 stirring rods, 8 feed pipes, 9 air inlets
Pipe, 10 heating oil laggings, 11 flowlines, 12 oil drums, 13 electrothermal tubes, 14 flowlines, 15 oil well pumps, 16 temperature sensors, 17 electricity
Magnetic current adjustable valve, 18 discharge gates, 19 stabilizer blades, 20 central spindles, 21 damping springs, 22 damping shells, 23 thermal insulation boards, 24 sawtooth.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Figs. 1-2, the utility model embodiment provides a kind of high-purity oleamide extraction element, including reaction kettle 1,
The bottom of reaction kettle 1 is fixedly connected with transverse slat 2, and the lower surface of transverse slat 2 is fixedly installed with stabilizer blade 19, and stabilizer blade 19 is provided with two altogether
It is a, and at the both ends of two stabilizer blades 19 lower section that reaction kettle 1 is set, transverse slat 2 can be made more firm, to reach reaction
More stable in reaction process in kettle 1, the central part of stabilizer blade 19 is equipped with central spindle 20, and damping is equipped at the outer wall of central spindle 20
Spring 21, the top of central spindle 20 are equipped with damping shell 22, and the lower section of stabilizer blade 19 is equipped with sawtooth 24, by the cooperation of its structure,
It can be very good to make to play the role of it when work in reaction kettle 1 buffering, keep the reaction in reaction kettle 1 more stable,
The more uniform of the hot oil diffusion in oil lagging 10 can be made to heat simultaneously, to keep in reaction kettle 1 temperature more steady
Fixed, 19 rectangular in cross-section of stabilizer blade is made of stainless steel material, can be very good high-purity oleamide extraction being placed on some
Position, while can be very good the reaction kettle 1 on support transverse slat 2 and transverse slat 2, the left side of transverse slat 2 is fixedly connected with riser 3,
The top in 3 left side of riser is fixedly connected with loading plate 4, and the lower surface of loading plate 4 is fixedly connected with motor 5, the output end of motor 5
It is fixedly connected with bull stick 6 by shaft coupling, bull stick 6 runs through the hole that 1 bottom of reaction kettle opens up and extends to the interior of reaction kettle 1
Chamber, the side surface of bull stick 6 are fixedly connected with stirring rod 7, and stirring rod 7 is located at the inner cavity of reaction kettle 1, the charging at 1 top of reaction kettle
Feed pipe 8 is fixedly connected at mouthful, the air inlet position at 1 top of reaction kettle is fixedly connected with air inlet pipe 9, the side surface of reaction kettle 1
It is provided with heating oil lagging 10, the outer surface of reaction kettle 1 is fixedly connected with thermal insulation board 23, and heats oil lagging 10 and be located at thermal insulation board
In 23, it can be very good to make around reaction kettle 1 and temperature will not should heat oil lagging 10 and increase, while also to reaction kettle 1
A good insulation effect is played, keeps the reaction in reaction kettle 1 more stable, while also saving the cost that heating needs,
The oil outlet for heating 10 left side of oil lagging is equipped with flowline 14, and flowline 14 is fixedly connected with far from heating 10 one end of oil lagging
Oil drum 12, electrothermal tube 13 is fixedly connected at the oil inlet of oil drum 2, and the oil outlet at 12 top of oil drum is fixedly connected with flowline
14, it is fixedly connected at the oil inlet opened up on the left of one end of the separate oil drum 12 of flowline 14 and heating oil lagging 10, fuel-displaced 14
Outer surface be fixedly connected with oil well pump 15, the inner cavity of reaction kettle 1 is provided with temperature sensor 16, the upper end in 1 left side of reaction kettle
It is provided with Electromagnetic Flow regulating valve 17, temperature sensor 16 is connected to Electromagnetic Flow regulating valve 17, electromagnetic current using pilot
Adjustable valve 17 is connected to oil well pump 15 and electrothermal tube 13 using pilot, and temperature sensor 16 is made to can control Electromagnetic Flow
Regulating valve 17 make Electromagnetic Flow regulating valve 17 can with automatic traction oil well pump 15 and electrothermal tube 13 in entire reaction kettle 1
Temperature can be adjusted by automating, and save human cost, while imitate the reaction in reaction kettle 1 more comprehensively
Fruit is fixedly connected with drainage conduit 18 at the discharge gate of 1 lower right-hand side of reaction kettle, which leads to
Cross increase heating oil lagging 10, flowline 14, oil drum 12, electrothermal tube 13, flowline 14, oil well pump 15, temperature sensor 16,
Electromagnetic Flow regulating valve 17 and thermal insulation board 23 are used cooperatively, and oleamide production can be produced to high-purity oleamide and be reacted
The temperature of journey is able to carry out effective control, greatly improves the effect of reaction, reduces the cost of actual production, improves
The quality of final products, a kind of high-purity oleamide extraction element, by increase stabilizer blade 19, axle center 20, damping spring 21,
It is more stable in production reaction process can to make reaction kettle 1, while can also make for the cooperation of damping shell 22 and sawtooth 24
The more uniform of the hot oil heat diffusion in oil lagging 10 is heated, keeps the temperature in reaction kettle 1 more stable.
Working principle: in use, flowing into material in reaction kettle 1 by feed pipe 8,6 turns of bull stick are driven by motor 5
It is dynamic, so that bull stick 6 drives stirring rod 7 to start turning, ammonia is being imported in reaction kettle 1 by air inlet pipe 9, is passing through heating oil folder
Set 10 rises the temperature in reaction kettle 1, and after a period of time, temperature declines in reaction kettle 1, at this moment 16 benefit of temperature sensor
So that Electromagnetic Flow regulating valve 17 is started to work with pilot, oil well pump is made using pilot by Electromagnetic Flow regulating valve 17
15 start to work with electrothermal tube 13, and the cold oil heated in oil lagging 10 is had in oil drum 12 by the inflow of flowline 14, passes through electricity
Heat pipe 13 makes the cold oil in oil drum 12 become hot oil, flows into hot oil in heating oil lagging 10 by oil well pump 15, simultaneous reactions
Kettle 1 returns generation vibration during the reaction, and transverse slat 2 can be made to teetertotter, to keep about 20 axle center flexible, causes damping spring
21 teetertotter, and making reaction kettle 1 during the reaction is not in significantly upper and lower situation, extract and fill to high-purity oleamide
It sets and plays certain cushioning effect, to reach in high-purity oleamide in process of production to the control of temperature, make it
It is always held in certain temperature difference, improves the reaction effect in high-purity oleamide production process, reduce practical life
Cost is produced, end product quality is improved.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of high-purity oleamide extraction element, including reaction kettle (1), it is characterised in that: the bottom of the reaction kettle (1) is solid
Surely it is connected with transverse slat (2), the lower surface of the fixed transverse slat (2) is fixedly installed with stabilizer blade (19), and the left side of the transverse slat (2) is solid
Surely it is connected with riser (3), the top on the left of the riser (3) is fixedly connected with loading plate (4), the following table of the loading plate (4)
Face is fixedly connected with motor (5), and the output end of the motor (5) is fixedly connected with bull stick (6), the bull stick by shaft coupling
(6) run through the hole that reaction kettle (1) bottom opens up and the inner cavity for extending to reaction kettle (1), the side surface of the bull stick (6) is fixed
It is connected with stirring rod (7), the stirring rod (7) is located at the inner cavity of reaction kettle (1), at the feed inlet at the top of the reaction kettle (1)
It is fixedly connected with feed pipe (8), the air inlet position at the top of the reaction kettle (1) is fixedly connected with air inlet pipe (9), the reaction kettle
(1) side surface is provided with heating oil lagging (10), and the oil outlet on the left of heating oil lagging (10) is equipped with flowline
(14), the flowline (14) far from heating oil lagging (10) one end be fixedly connected with oil drum (12), the oil drum (12) into
Oil port is fixedly connected with electrothermal tube (13), and the oil outlet at the top of the oil drum (12) is fixedly connected with flowline (14), institute
It states and is fixedly connected at the oil inlet opened up on the left of one end and heating oil lagging (10) of the separate oil drum (12) of flowline (14), institute
The outer surface for stating flowline (14) is fixedly connected with oil well pump (15), and the inner cavity of the reaction kettle (1) is provided with temperature sensor
(16), the upper end on the left of the reaction kettle (1) is provided with Electromagnetic Flow regulating valve (17), reaction kettle (1) lower right-hand side
Drainage conduit (18) are fixedly connected at discharge gate.
2. a kind of high-purity oleamide extraction element according to claim 1, it is characterised in that: the stabilizer blade (19) sets altogether
There are two setting, and two stabilizer blades (19) are arranged at the both ends of the lower section of reaction kettle (1).
3. a kind of high-purity oleamide extraction element according to claim 1, it is characterised in that: in the stabilizer blade (19)
Center portion is arranged with central spindle (20), and is equipped with damping spring (21) at the outer wall of central spindle (20), and the top of the central spindle (20) is installed
Have damping shell (22), the lower section of the stabilizer blade (19) is equipped with sawtooth (24).
4. a kind of high-purity oleamide extraction element according to claim 1, it is characterised in that: stabilizer blade (19) section
In rectangle, it is made of stainless steel material.
5. a kind of high-purity oleamide extraction element according to claim 1, it is characterised in that: the reaction kettle (1)
Outer surface is fixedly connected with thermal insulation board (23), and is heated oil lagging (10) and be located in thermal insulation board (23).
6. a kind of high-purity oleamide extraction element according to claim 1, it is characterised in that: the temperature sensor
(16) it is connected to the Electromagnetic Flow regulating valve (17) using pilot, the Electromagnetic Flow regulating valve (17) is led using control
Line is connected to the oil well pump (15) and electrothermal tube (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820712429.7U CN208482438U (en) | 2018-05-14 | 2018-05-14 | A kind of high-purity oleamide extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820712429.7U CN208482438U (en) | 2018-05-14 | 2018-05-14 | A kind of high-purity oleamide extraction element |
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| Publication Number | Publication Date |
|---|---|
| CN208482438U true CN208482438U (en) | 2019-02-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201820712429.7U Active CN208482438U (en) | 2018-05-14 | 2018-05-14 | A kind of high-purity oleamide extraction element |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020177459A1 (en) * | 2019-03-01 | 2020-09-10 | 浙江三赢新材料有限公司 | Jacket type oil bath drying device for high water-absorbent resin |
| CN115260471A (en) * | 2022-08-30 | 2022-11-01 | 江苏冠军科技集团股份有限公司 | Alkyd protective coating with high flash point, high solid content and low VOCs |
-
2018
- 2018-05-14 CN CN201820712429.7U patent/CN208482438U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020177459A1 (en) * | 2019-03-01 | 2020-09-10 | 浙江三赢新材料有限公司 | Jacket type oil bath drying device for high water-absorbent resin |
| CN115260471A (en) * | 2022-08-30 | 2022-11-01 | 江苏冠军科技集团股份有限公司 | Alkyd protective coating with high flash point, high solid content and low VOCs |
| CN115260471B (en) * | 2022-08-30 | 2023-09-15 | 江苏冠军科技集团股份有限公司 | Alkyd protective coating with high flash point, high solid content and low VOCs (volatile organic compounds) |
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Address after: 343000 Industrial Park South District, Yongfeng County, Ji'an City, Jiangxi Province Patentee after: Jiangxi Zhilian New Material Co.,Ltd. Address before: 343000 Industrial Park South District, Yongfeng County, Ji'an City, Jiangxi Province Patentee before: JIANGXI ZHILIAN PLASTICIZING TECHNOLOGY Co.,Ltd. |