CN201969551U - Separation kettle for producing T acid - Google Patents

Separation kettle for producing T acid Download PDF

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Publication number
CN201969551U
CN201969551U CN2011200266100U CN201120026610U CN201969551U CN 201969551 U CN201969551 U CN 201969551U CN 2011200266100 U CN2011200266100 U CN 2011200266100U CN 201120026610 U CN201120026610 U CN 201120026610U CN 201969551 U CN201969551 U CN 201969551U
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CN
China
Prior art keywords
kettle
acid
cooling
coil pipe
produced
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2011200266100U
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Chinese (zh)
Inventor
孟庆升
王玉章
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANDONG YUYUAN GROUP CO Ltd
Original Assignee
SHANDONG YUYUAN GROUP CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to CN2011200266100U priority Critical patent/CN201969551U/en
Application granted granted Critical
Publication of CN201969551U publication Critical patent/CN201969551U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a separation kettle for producing T acid, which comprises a kettle body, wherein the kettle body is provided with a material feeding port and a material discharging port, the kettle body is provided with a stirring device driven by a power device, a coil pipe cooling device is arranged in the kettle body, the kettle body is provided with a cooling liquid inlet and a cooling liquid outlet communicated with the coil pipe cooling device. The temperature of the separation kettle is reduced rapidly, the energy conversation rate is high, the material separation process is accelerated and the production efficiency is improved.

Description

T acid is produced with the segregation still
Technical field
The utility model relates to a kind of segregation still, relates in particular to a kind of T acid and produces with the segregation still.
Background technology
T acid is naphthalidine-3,6, the 8-trisulfonic acid, in the production process of T acid, need use the segregation still, the segregation still is the material place of emanating, and the cooling method of present segregation still is the kettle outer wrap chuck at the segregation still, thereby by the segregation still being lowered the temperature to feeding cooling fluid in the chuck, the cooling of this structure, cooling efficient is low, and capacity usage ratio is low, thereby the segregation process of segregation still is prolonged, reduced production efficiency.
Summary of the invention
Technical problem to be solved in the utility model is: provide a kind of T acid to produce with the segregation still, this emanates the still cooling rapidly, and the energy conversion rate height quickens material segregation process, enhances productivity.
For solving the problems of the technologies described above, the technical solution of the utility model is: a kind of T acid is produced with the segregation still, comprise kettle, described kettle is provided with charging aperture and discharging opening, the agitating device that is driven by power set is installed on the described kettle, the coil pipe cooling device is installed in the described kettle, and described kettle is provided with cooling fluid inlet and the cooling liquid outlet that is communicated with described coil pipe cooling device.
As a kind of preferred scheme, described coil pipe cooling device comprises the support that abuts in described inner wall of kettle, is fixed with cooling coil on the described support.
As a kind of preferred scheme, described cooling coil is the cooling coil of plumbous system.
As a kind of preferred scheme, described agitating device comprises the shaft that is rotatably installed on the described kettle, and described shaft is provided with stirring vane, and described shaft is connected with described power set.
As a kind of preferred scheme, described power set comprise a motor.
As a kind of preferred scheme, described kettle is the kettle of fiberglass material.
As a kind of preferred scheme, described charging aperture is arranged at the top of kettle, and described discharging opening is arranged at the side bottom of described kettle, and the bottom of described kettle is provided with the guide inclined plane to the discharging opening inclination.
After having adopted technique scheme, effect of the present utility model is: because described T acid is produced with the segregation still, comprise kettle, described kettle is provided with charging aperture and discharging opening, the agitating device that is driven by power set is installed on the described kettle, the coil pipe cooling device is installed in the described kettle, described kettle is provided with cooling fluid inlet and the cooling liquid outlet that is communicated with described coil pipe cooling device, therefore cooling fluid enters from the cooling fluid inlet, through the coil pipe cooling device in the kettle material is carried out heat exchange then, cooling fluid flows out from cooling liquid outlet then, and heat is taken away, and so just can reach the purpose of cooling, because the coil pipe cooling device is positioned at kettle, directly and material carry out heat exchange, cool with respect to the chuck of kettle outside, its cooling is more direct, cooling rapidly, the energy conversion rate height quickens material segregation process, enhances productivity.
Description of drawings
Below in conjunction with drawings and Examples the utility model is further specified.
Fig. 1 is the structural representation of the utility model embodiment;
Fig. 2 is the vertical view of the kettle of the utility model embodiment;
In the accompanying drawing: 1. kettle; 2. discharging opening; 3. shaft; 4. motor; 5. cooling coil; 6. cooling liquid outlet; 7. cooling fluid enters the mouth; 8. support; 9. thermometer running-on; 10. wash water import; 11. add sour import; 12. Steam Heating mouth; 13. suction opeing; 14. charging aperture; 15. guide inclined plane.
The specific embodiment
A kind of T acid is produced with the segregation still, as depicted in figs. 1 and 2, it comprises kettle 1, described kettle 1 is provided with charging aperture 14 and discharging opening 2, described charging aperture 14 is arranged at the top of kettle 1, described discharging opening 2 is arranged at the side bottom of described kettle 1, and the bottom of described kettle 1 is provided with to the guide inclined plane 15 of discharging opening 2 inclinations, helps material and puts only.The top of described kettle 1 also is provided with thermometer running-on 9, wash water import 10, adds sour import 11, Steam Heating mouth 12 and suction opeing 13.The agitating device that is driven by power set is installed on the described kettle 1, and described agitating device comprises the shaft 3 that is rotatably installed on the described kettle 1, and described shaft 3 is provided with stirring vane, and described shaft 3 is connected with described power set.Described power set comprise a motor 4.In the described kettle 1 the coil pipe cooling device is installed, described kettle 1 is provided with cooling fluid inlet 7 and the cooling liquid outlet 6 that is communicated with described coil pipe cooling device.Described coil pipe cooling device comprises the support 8 that abuts in described kettle 1 inwall, is fixed with cooling coil 5 on the described support 8.Preferably, described cooling coil 5 is the cooling coil 5 of plumbous system.Described kettle 1 is the kettle 1 of fiberglass material, thereby kettle 1 anti-highly basic, high temperature resistant (reaching 120 ℃) is convenient to repair.And kettle 1 can be provided with diameter greatly, highly relatively little, gas discharging is convenient in the steam vent overstriking, helps the abundant discharging of SO2 and the formation of material crystalline particle, has improved yield greatly.
Operation principle of the present utility model is: prepare pickle earlier 1.: add a certain amount of running water from wash water import 10, add a certain amount of 93% sulfuric acid from adding sour import 11 then, start agitating device and stir, and after reaction a period of time, sample analysis;
2. in still, drip the molten thing of alkali and be warmed up to technological temperature from charging aperture 14,, detect whether material pH reaches technological requirement in the still with material acidity in the pH detection paper still;
3. feed cooling fluid from cooling fluid inlet 7, lower the temperature by the cooling coil 5 in the kettle 1;
4. begin when temperature is reduced to the technological requirement temperature to be discharged to the suction strainer groove from discharging opening 2.
Because the coil pipe cooling device is positioned at kettle 1, directly and material carry out heat exchange, cool with respect to the chuck of kettle 1 outside, its cooling is more direct, cooling rapidly, energy conversion rate height, the acceleration material process of emanating is enhanced productivity.

Claims (5)

1.T acid is produced with the segregation still, comprise kettle, described kettle is provided with charging aperture and discharging opening, the agitating device that is driven by power set is installed on the described kettle, it is characterized in that: the coil pipe cooling device is installed in the described kettle, and described kettle is provided with cooling fluid inlet and the cooling liquid outlet that is communicated with described coil pipe cooling device.
2. T acid as claimed in claim 1 is produced with the segregation still, and it is characterized in that: described coil pipe cooling device comprises the support that abuts in described inner wall of kettle, is fixed with cooling coil on the described support.
3. T acid as claimed in claim 1 is produced with the segregation still, and it is characterized in that: described agitating device comprises the shaft that is rotatably installed on the described kettle, and described shaft is provided with stirring vane, and described shaft is connected with described power set.
4. T acid as claimed in claim 3 is produced with the segregation still, and it is characterized in that: described power set comprise a motor.
5. T acid as claimed in claim 1 is produced with the segregation still, and it is characterized in that: described charging aperture is arranged at the top of kettle, and described discharging opening is arranged at the side bottom of described kettle, and the bottom of described kettle is provided with the guide inclined plane to the discharging opening inclination.
CN2011200266100U 2011-01-24 2011-01-24 Separation kettle for producing T acid Expired - Fee Related CN201969551U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011200266100U CN201969551U (en) 2011-01-24 2011-01-24 Separation kettle for producing T acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011200266100U CN201969551U (en) 2011-01-24 2011-01-24 Separation kettle for producing T acid

Publications (1)

Publication Number Publication Date
CN201969551U true CN201969551U (en) 2011-09-14

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011200266100U Expired - Fee Related CN201969551U (en) 2011-01-24 2011-01-24 Separation kettle for producing T acid

Country Status (1)

Country Link
CN (1) CN201969551U (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102641608A (en) * 2012-04-27 2012-08-22 苏州市金翔钛设备有限公司 Leaching tank for titanium lining
CN102701505A (en) * 2012-06-18 2012-10-03 山东裕源集团有限公司 Equipment for treating H-acid production wastewater
CN103432980A (en) * 2013-09-02 2013-12-11 四川顺源化工有限公司 Biodiesel reaction still
CN104084079A (en) * 2014-06-24 2014-10-08 芜湖富春染织有限公司 Mixing device of anhydrous sodium sulfate used for dye
CN104190298A (en) * 2014-08-15 2014-12-10 容家杨 Temperature adjustable type fruit pulp mixer

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102641608A (en) * 2012-04-27 2012-08-22 苏州市金翔钛设备有限公司 Leaching tank for titanium lining
CN102641608B (en) * 2012-04-27 2015-04-29 苏州市金翔钛设备有限公司 Leaching tank for titanium lining
CN102701505A (en) * 2012-06-18 2012-10-03 山东裕源集团有限公司 Equipment for treating H-acid production wastewater
CN103432980A (en) * 2013-09-02 2013-12-11 四川顺源化工有限公司 Biodiesel reaction still
CN104084079A (en) * 2014-06-24 2014-10-08 芜湖富春染织有限公司 Mixing device of anhydrous sodium sulfate used for dye
CN104190298A (en) * 2014-08-15 2014-12-10 容家杨 Temperature adjustable type fruit pulp mixer

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110914

Termination date: 20150124

EXPY Termination of patent right or utility model