CN208476718U - A kind of H of sulfide2The detection device of S burst size - Google Patents

A kind of H of sulfide2The detection device of S burst size Download PDF

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Publication number
CN208476718U
CN208476718U CN201821036294.3U CN201821036294U CN208476718U CN 208476718 U CN208476718 U CN 208476718U CN 201821036294 U CN201821036294 U CN 201821036294U CN 208476718 U CN208476718 U CN 208476718U
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CN
China
Prior art keywords
climatic chamber
built
sealed
holding table
sample platform
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821036294.3U
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Chinese (zh)
Inventor
陈少杰
吴林斌
姚霞银
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo Institute of Material Technology and Engineering of CAS
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Ningbo Institute of Material Technology and Engineering of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201821036294.3U priority Critical patent/CN208476718U/en
Application granted granted Critical
Publication of CN208476718U publication Critical patent/CN208476718U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)

Abstract

The utility model provides a kind of H of sulfide2The detection device of S burst size, including climatic chamber and the built-in sealed compartment being arranged in inside the climatic chamber;The climatic chamber is equipped with operation window;The inner wall of the built-in sealed compartment is provided with gas probe and real time monitoring probe;Top is provided with hatchcover;Bottom is provided with articles holding table, and for placing sealed sample platform, articles holding table is internally provided with fan;Openable and closable top cover is provided at the top of the sealed sample platform.Climatic chamber in the utility model can accurately and rapidly simulate the use environment of different temperatures and humidity, and whole sealing status is presented in test device, and data acquisition in real time, accurately, provides guarantee for the safe handling of sulfide electrolyte.

Description

A kind of H of sulfide2The detection device of S burst size
Technical field
The utility model belongs to gas on-line monitoring field more particularly to a kind of H of sulfide2The detection of S burst size fills It sets.
Background technique
Since the aerial stability of sulfide electrolyte is poor, especially it is easy and water H micro in air2O is anti- Answer, destroy the structure of electrolyte, reduce the conductivity of electrolyte, and also release it is a kind of inflammable, have rotten egg smell and Poisonous gas hydrogen sulfide (H2S)。
People sucks H by respiratory tract2S (70~150mg/m31~2h of)/(), there is respiratory tract and Eye irritation symptom, vulcanizes Hydrogen can benumb olfactory nerves, no longer smell foul smell after inhaling 2~5min.(300mg/m3)/1h is sucked, 6~8min goes out urgency of losing face Sexual stimulus symptom, slightly contact causes pulmonary edema for a long time.Sucking vulcanization Hydrogen Energy causes the inhibition of central nervous system, sometimes due to Stimulation and the paralysis of breathing and lead to final death.Collapse, shock will occur in several seconds in highly concentrated hydrogen sulfide, can lead Respiratory inflammation, pulmonary edema are caused, and with headache, chest pain and expiratory dyspnea.
Therefore, before a kind of sulfide electrolyte use, its H in use environment can be understood2The burst size of S is right Its security performance is significant.
Utility model content
The utility model provides a kind of H of sulfide2The detection device of S burst size, the device energy in the utility model The enough H of detection sulfide electrolyte in different environments2S burst size.
A kind of H of sulfide of the utility model2S discharges amount detecting device, including climatic chamber and setting in the perseverance Built-in sealed compartment inside constant temperature and humidity case;
The climatic chamber is equipped with operation window;
Hatchcover is provided at the top of the built-in sealed compartment;Inner wall is provided with gas probe and real time monitoring probe;Bottom It is provided with articles holding table, for the articles holding table for placing sealed sample platform, articles holding table is internally provided with fan;
Openable and closable top cover is provided at the top of the sealed sample platform.
Preferably, constant temperature and humidity control panel is provided with outside the climatic chamber.
Preferably, solenoid valve is provided on the hatchcover of the built-in sealed compartment.
Preferably, solenoid valve is provided on the top cover of the sealed sample platform.
Preferably, the operation window is provided with rubber gloves.
The utility model provides a kind of H of sulfide2S discharges amount detecting device, including climatic chamber and setting exist Built-in sealed compartment inside the climatic chamber;The climatic chamber is equipped with operation window;The inner wall of the built-in sealed compartment It is provided with gas probe and real time monitoring probe;Top is provided with hatchcover;Bottom is provided with articles holding table, for placing sealed sample Platform, articles holding table are internally provided with fan;Openable and closable top cover is provided at the top of the sealed sample platform.In the utility model Climatic chamber can accurately and rapidly simulate the use environment of different temperatures and humidity, and whole sealing status is presented in test device, Data acquisition in real time, accurately, provides guarantee for the safe handling of sulfide electrolyte.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only It is the embodiments of the present invention, for those of ordinary skill in the art, without creative efforts, also Other attached drawings can be obtained according to the attached drawing of offer.
Fig. 1 is the H of sulfide in the utility model2The structural schematic diagram of S release amount detecting device;
1 is operation window;2 be very constant temperature and humidity case;3 be hatchcover;4 be hatchcover;5 be gas probe;6 be real time monitoring probe;7 For top cover;8 be solenoid valve;9 be sealed sample platform;10 be sample;11 be articles holding table;12 be fan;13 be built-in sealed compartment;14 For constant temperature and humidity control panel;
Fig. 2 is the H of sulfide in the utility model2S discharges amount detecting device and is wirelessly connected schematic diagram.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
The utility model provides a kind of H of sulfide2S discharges amount detecting device, including climatic chamber and setting exist Built-in sealed compartment inside the climatic chamber;
The climatic chamber is equipped with operation window;
Openable and closable hatchcover is provided at the top of the built-in sealed compartment;Inner wall is provided with gas probe and real time monitoring is visited Head;Bottom is provided with articles holding table, and for the articles holding table for placing sealed sample platform, articles holding table is internally provided with fan;
Openable and closable top cover is provided at the top of the sealed sample platform.
Detection device in the utility model can be divided into test macro and real-time data acquisition system according to function, wherein Real-time data acquisition system includes gas probe, real time monitoring probe, and the gas probe and real time monitoring probe have wireless Transfer function, the data that can be will test are real-time transmitted to the computer of wireless connection, carry out data record and analysis.
In the present invention, the climatic chamber can be arranged by the way that external constant temperature and humidity control panel is arranged in Temperature and humidity environment inside the climatic chamber, the use environment for simulated sulfuration object electrolyte.
The climatic chamber is closed structure, and is provided with operation window, and the operation window is preferably airtight connection in institute The rubber gloves on constant temperature and humidity box body is stated, operator is facilitated to protrude into hand inside the climatic chamber, progress is some must The operation wanted.
Climatic chamber is internally provided with built-in sealed compartment, is provided with hatchcover, the cabin at the top of the built-in sealed compartment Cover and be provided with solenoid valve, due to entire detection system be it is closed, built-in sealed compartment is opened and closed by solenoid valve can be minimum The disturbance of the reduction internal environment of degree.
The bottom of the built-in sealed compartment is provided with articles holding table, and gas probe and real time monitoring probe are provided on inner wall; The gas probe and real time monitoring probe are preferably provided at the middle part of the built-in sealed compartment.
The articles holding table is for placing sealed sample platform, and the sealed sample platform is for holding test sample, the sealing Top cover is provided at the top of sample stage, in order to guarantee that sealing effect, the top cover equally also control folding using solenoid valve.
Fan is provided with below the articles holding table, fan is opened, and the air flow faster in built-in sealed compartment is conducive to Accelerate the release of sulfide.
Specifically, elaborating the operating process of the utility model in conjunction with Fig. 1:
1, weigh a certain amount of sulfide electrolyte powder tabletting to be measured in glove box, and demould, by the piece pressed or Person's powder sample is put into sealed sample platform, is taken out from glove box.
2, sealed sample platform is placed on articles holding table, covers hatchcover above built-in sealed compartment and is sealed.Solenoid valve is opened, It is that hatchcover keeps sealing state, the solenoid valve of control sealed sample platform is closed always, to keep the top cover of sample stage to stay open State.Close the chamber door of climatic chamber.Start climatic chamber, allows environmental cabinet is interior to keep certain humidity and temperature, open Fan in built-in sealed compartment.
3, after the humidity in environmental cabinet and after temperature stablizes, starting test macro (gas probe and real time monitoring probe), The solenoid valve for closing control hatchcover folding, opens hatch door, opens the solenoid valve of control sealed sample platform, closes top cover.Data Acquisition system starts to acquire and record H2The concentration of S changes and the cosmetic variation of sample, and closing control is close after recording a period of time The solenoid valve of approved sample sample platform, shutdown test system and climatic chamber.

Claims (5)

1. a kind of H of sulfide2S discharges amount detecting device, including climatic chamber and is arranged in inside the climatic chamber Built-in sealed compartment;
The climatic chamber is equipped with operation window;
Hatchcover is provided at the top of the built-in sealed compartment;Inner wall is provided with gas probe and real time monitoring probe;Bottom setting There is articles holding table, for the articles holding table for placing sealed sample platform, articles holding table is internally provided with fan;
Openable and closable top cover is provided at the top of the sealed sample platform.
2. detection device according to claim 1, which is characterized in that be provided with constant temperature and humidity outside the climatic chamber Control panel.
3. detection device according to claim 1, which is characterized in that be provided with electromagnetism on the hatchcover of the built-in sealed compartment Valve.
4. detection device according to claim 1, which is characterized in that be provided with electromagnetism on the top cover of the sealed sample platform Valve.
5. detection device according to claim 1, which is characterized in that the operation window is provided with rubber gloves.
CN201821036294.3U 2018-07-02 2018-07-02 A kind of H of sulfide2The detection device of S burst size Expired - Fee Related CN208476718U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821036294.3U CN208476718U (en) 2018-07-02 2018-07-02 A kind of H of sulfide2The detection device of S burst size

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821036294.3U CN208476718U (en) 2018-07-02 2018-07-02 A kind of H of sulfide2The detection device of S burst size

Publications (1)

Publication Number Publication Date
CN208476718U true CN208476718U (en) 2019-02-05

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CN201821036294.3U Expired - Fee Related CN208476718U (en) 2018-07-02 2018-07-02 A kind of H of sulfide2The detection device of S burst size

Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111982739A (en) * 2020-08-08 2020-11-24 天目湖先进储能技术研究院有限公司 Detection device and method for detecting sulfide electrolyte material
CN112147036A (en) * 2020-09-23 2020-12-29 上海化工研究院有限公司 Device and method for testing constant-temperature substance gas-releasing reaction capability when meeting water

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111982739A (en) * 2020-08-08 2020-11-24 天目湖先进储能技术研究院有限公司 Detection device and method for detecting sulfide electrolyte material
CN112147036A (en) * 2020-09-23 2020-12-29 上海化工研究院有限公司 Device and method for testing constant-temperature substance gas-releasing reaction capability when meeting water

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190205

Termination date: 20200702