CN208407003U - A kind of chemical reaction kettle with detection system - Google Patents

A kind of chemical reaction kettle with detection system Download PDF

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Publication number
CN208407003U
CN208407003U CN201820783114.1U CN201820783114U CN208407003U CN 208407003 U CN208407003 U CN 208407003U CN 201820783114 U CN201820783114 U CN 201820783114U CN 208407003 U CN208407003 U CN 208407003U
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CN
China
Prior art keywords
gas
autoclave body
gas transmission
sensor
transmission ring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820783114.1U
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Chinese (zh)
Inventor
邓长全
余朝庆
刘群兵
邓友全
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wenchuan Xiangning Chlorate Co Ltd
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Wenchuan Xiangning Chlorate Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to CN201820783114.1U priority Critical patent/CN208407003U/en
Application granted granted Critical
Publication of CN208407003U publication Critical patent/CN208407003U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of chemical reaction kettle and its monitoring systems, including autoclave body, kettle cover and support base, exhaust outlet is equipped at the top of kettle cover, it is equipped on exhaust outlet equipped with gas-filtering device, the upper surface of the support base is fixed with gas transmission ring by more batter posts, gas transmission ring set is located at the outside of autoclave body, gas distribution channel is provided in gas transmission ring, multiple gas-charging connections are provided on gas transmission ring, and the inner wall of gas transmission ring is provided with the more appendixs being connected to gas distribution channel, appendix one end tilts down and protrudes into autoclave body inner cavity, the air taking port of all gas transmission bottom of the tube is arranged in circle, and the air supply direction of air taking port and the circle are tangent, it is intracavitary in the autoclave body to be equipped with sensor;Support base is equipped with PLC controller.For the utility model by the appendix of setting circumferential array, appendix can be whirled up gas in autoclave body, to be stirred to chemical reagent, avoid and agitating shaft is arranged in autoclave body, not only reduce installation cost, and repair or replace more convenient.

Description

A kind of chemical reaction kettle with detection system
Technical field
The utility model relates to technical field of chemical production equipment, and in particular to a kind of chemical reaction with detection system Kettle.
Background technique
The kettle that reconciles is also known as reactor tank or reaction kettle, it is that one or more of raw materials are carried out mixed reaction by processing compound Stainless steel is stirred to react class container.In chemical production field, it is often necessary to various solution reagents are deployed, so that life is adjusted It produces, and the reconciliation of solution reagent would generally be used to reconciliation reaction kettle.
Existing reconciliation reaction kettle is to be stirred by motor drive to mix reagent mostly, and structure is in reaction kettle Motor is installed at top, and by shaft coupling and a stirring axis connection, agitating shaft protrudes into autoclave body and on agitating shaft the output shaft of motor It is provided with stirrer paddle, starting motor drives stirrer paddle rotation, to be stirred mixing to chemical reagent.This top is set The structure one for setting motor is conveniently to increase the cost of reaction kettle, is on the other hand not easy to repair or replaces agitating shaft, due to stirring The shape for mixing blade makes it difficult to take out out of autoclave body.In addition, can generate some gases in reaction kettle reaction process, will affect Air pressure, temperature in reaction kettle etc. are likely to result in one if operator opens reaction kettle in situation not knowing in reaction kettle A little injuries need to be monitored the situation in reaction kettle in order to avoid these injuries.
Summary of the invention
The purpose of this utility model is to provide a kind of chemical reaction kettle with detection system, the reaction kettle is without passing through Setting stirring motor just can be stirred chemical reagent, while can monitor temperature, air pressure, gas componant and pH in reaction kettle Value.
The purpose of this utility model is achieved through the following technical solutions:
A kind of chemical reaction kettle with detection system is equipped at the top of kettle cover including the autoclave body and kettle cover being detachably connected Feed inlet and exhaust outlet, feed inlet, which goes out, is equipped with feeding device, and autoclave body bottom is equipped with leakage fluid dram, and autoclave body bottom is equipped with support bottom , it is equipped on the exhaust outlet equipped with gas-filtering device, gas-filtering device outlet is connected with water tank, water tank by pipeline It is mounted on gas-filtering device side, the top of water tank is equipped with gas outlet, and gas outlet is equipped with gas composition sensor;
The upper surface of the support base is fixed with gas transmission ring by more batter posts, and gas transmission ring set is located at the outside of autoclave body, Be provided with gas distribution channel in gas transmission ring, be provided with multiple gas-charging connections on gas transmission ring, and the inner wall of gas transmission ring be provided with more with The appendix of gas distribution channel connection, appendix one end tilts down and protrudes into autoclave body inner cavity, the air taking port of all gas transmission bottom of the tube It is arranged in circle, and the air supply direction of air taking port and the circle are tangent, the appendix outside autoclave body is equipped with electronic valve;
Intracavitary temperature sensor, baroceptor, gas sensor, pH sensor and the concentration of being equipped with passes in the autoclave body Sensor;
The support base is equipped with support rod, and support rod is equipped with PLC controller, and PLC controller includes that signal is located in advance Reason module, PLC main control module, display module, LED display, drive module, alarm and memory module, the signal are located in advance Reason module, display module, drive module and memory module are connect with PLC main control module, and display module and LED display connect It connects, drive module is connect with electronic valve and alarm, signal pre-processing module and gas composition sensor, temperature sensor, gas Pressure sensor, gas sensor, pH sensor are connected with concentration sensor.
Further, the autoclave body includes outer gallbladder and liner, is separated with gap between outer gallbladder and liner, and outer gallbladder and liner it Between be fixed with multiple packing rings, aluminium hydroxide or magnesium hydroxide powder are filled in packing ring.
Further, the gas-filtering device includes shell and is successively set on the intracorporal active carbon of shell from top to bottom Layer, cao layers and microbe stuffing layer.
The utility model has the following beneficial effects:
(1) by the appendix of setting circumferential array, appendix can be whirled up gas in autoclave body, to try chemical industry Agent is stirred, and avoids and agitating shaft is arranged in autoclave body, not only reduces installation cost, and is repaired or replaced more square Just;
(2) by filling aluminium hydroxide or magnesium hydroxide powder between the liner of autoclave body and outer gallbladder, autoclave body can be improved Fire retardancy, to improve the safety of device entirety;
(3) reconciliation can be reacted by the toxic and harmful gas generated by setting gas-filtering device and filters out purification in time, protected The safety of card device, while also ensuring that the intracorporal air pressure of kettle is normal;
(4) by the way that various sensors are arranged in reaction kettle, temperature, air pressure, concentration, pH value etc. in monitoring reaction kettle, Allow operator to will be clearly understood that the situation in reaction kettle, avoid blindly open reaction kettle and caused by injury.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the schematic diagram of internal structure of autoclave body in the utility model;
Fig. 3 is the arrangement mode schematic diagram of appendix in the utility model;
Fig. 4 is the electrical structure connection schematic diagram of the utility model.
Marked in the figure: 1, autoclave body;11, packing ring;12, temperature sensor;13, baroceptor;14, gas sensor; 15, pH sensor;16, concentration sensor;2, kettle cover;3, support base;4, PLC controller;5, gas-filtering device, 51, Solenoid valve;52, microbe stuffing layer;53, cao layers;54, active carbon layer;6, water tank;61, discharge outlet;7, feeding device; 8, gas transmission ring;81, gas-charging connection;82, appendix;83, electronic valve;84, air taking port.
Specific embodiment
As shown in Figure 1 and Figure 2, the chemical reaction kettle provided in this embodiment with detection system includes autoclave body, kettle cover, branch Filler central shoring pedestal, PLC controller, gas-filtering device, water tank and feeding device;The autoclave body includes liner and outer gallbladder, interior It is separated with gap between gallbladder and outer gallbladder, and is fixed with multiple packing rings, aluminium hydroxide or magnesium hydroxide powder are filled in packing ring End, when autoclave body, which is met, to be fired, aluminium hydroxide or magnesium hydroxide powder burning can generate a large amount of fire-retardant gas, to avoid in autoclave body 1 Gallbladder further burns, and guarantees the security performance of autoclave body.The kettle cover is connect with autoclave body by lock ear and is detachably cooperated with it;Institute The top for stating kettle cover is equipped with feed inlet and exhaust outlet, is equipped with feeding device on feed inlet, adds when can no longer opening kettle cover Enter other a small amount of chemical substances;The autoclave body is mounted in support base and its bottom is equipped with leakage fluid dram, the support base It is upper to be fixed with gas transmission ring by more batter posts, gas transmission ring set be located at the outside of autoclave body and its in equipped with gas distribution channel, on gas transmission ring Multiple gas-charging connections are provided with, gas-charging connection is connected with jet chimney.More and gas transmission are provided on the inner wall of the gas transmission ring The appendix of channel connection, the quantity of appendix is preferably 6, and appendix one end tilts down and protrude into the inner cavity of autoclave body, and 6 The air taking port of root gas transmission bottom of the tube is evenly distributed to justify, and the air supply direction of air taking port and the circle are tangent, the appendix position Part outside autoclave body is provided with electronic valve, electronic valve preferentially selects electronics check-valves, can prevent the intracorporal liquid reflux of kettle.? The root appendix of circumferential array can be made to be whirled up gas in autoclave body after being passed through high-temperature steam in gas transmission ring, on the one hand to autoclave body Interior chemical reagent is stirred, and on the other hand can be reconciled for chemical reagent and be provided heat, to improve its reaction efficiency.
Exhaust ports at the top of the kettle cover are connected with gas-filtering device by exhaust pipe, are provided on exhaust pipe Safety valve, gas-filtering device include shell and be successively set on from top to bottom the intracorporal active carbon layer of shell, cao layers and Microbe stuffing layer can filter out the intracorporal sour gas of kettle, irritative gas and floating impurity, to improve gas Clean-up performance;The side of filter device is provided with water tank, is connected between gas-filtering device and water tank by pipeline, pipeline one End is fixed on the top of gas-filtering device, and the water level that the other end protrudes into water tank is hereinafter, the top of water tank is provided with row Mouth is put, the gas after Water warfare can further improve its clean-up performance, and gas componant detector is arranged on discharge outlet, be used for The gas componant excluded is detected, when containing pernicious gas in the gas of exclusion, operator's closed safe valve is prevented excessive Pernicious gas is discharged into air, and the gas componant detector uses Shenzhen Ji Shunan Science and Technology Ltd. model JK50-I compound gas detector.
The support base is equipped with support rod, and support rod is equipped with PLC controller.It is intracavitary in the autoclave body to be equipped with temperature Sensor, baroceptor, gas sensor, pH sensor and concentration sensor, the temperature sensor, air pressure sensing Device, gas sensor, pH sensor and concentration sensor shell be all made of etch-proof material and be made, such as outside metal Shell finish coatings, plating chemically form fine and close corrosion resistant oxidation film;It is provided with cable-through hole on the autoclave body, makes temperature Sensor, baroceptor, gas sensor, pH sensor and concentration sensor signal give PLC control by wire transmission Device processed, PLC controller can show the signal of acquisition, make operator that can observe the situation in autoclave body in real time.
The PLC controller includes signal pre-processing module, PLC main control module, display module, LED display screen, driving Module, alarm and memory module, the signal pre-processing module, display module, drive module and memory module with PLC master Module connection is controlled, display module is connect with LED display, and drive module is connect with electronic valve and alarm, Signal Pretreatment mould Block and gas composition sensor, temperature sensor, baroceptor, gas sensor, pH sensor and concentration sensor connect It connects;Each sensor by the data of acquisition by line transmission to signal pre-processing module, signal pre-processing module is by acquisition Data are sent to PLC main control module, and PLC main control module is stored and be sent to display module, display module for data are acquired The data of acquisition are shown, operator carries out corresponding operation to reaction kettle according to data, is reacted with more preferable completion Journey.
The course of work of the utility model is: chemical reagent is added into reaction kettle, chemical reagent is fallen into autoclave body, then will High-temperature steam is passed through in gas transmission ring, high-temperature steam enters the inner cavity of autoclave body by electronics check-valves, and steam is discharged simultaneously from air taking port Gyration airflow is formed, to be stirred to chemical reagent, while the heat of steam can react the reconciliation of chemical reagent and play Catalytic action, the murder by poisoning exhaust gas that finally reconciliation generates is by way of pressurization by the intracorporal toxic gas force feed of kettle to gas filtration It is filtered out in device, the gas after final purification is discharged by discharge outlet.
The above is only the utility model preferred embodiment, but the protection scope of the utility model is not limited to This, any transformation carried out based on technical solution provided by the utility model and utility model design and replacement should all be covered In the protection scope of the utility model.

Claims (3)

1. a kind of chemical reaction kettle with detection system, including the autoclave body and kettle cover being detachably connected, be equipped at the top of kettle cover into Material mouth and exhaust outlet, feed inlet, which goes out, is equipped with feeding device, and autoclave body bottom is equipped with leakage fluid dram, and autoclave body bottom is equipped with support bottom Seat, it is characterised in that: be equipped on the exhaust outlet equipped with gas-filtering device, gas-filtering device outlet is connected by pipeline There is water tank, water tank is mounted on gas-filtering device side, and the top of water tank is equipped with gas outlet, and gas outlet is equipped with gas componant point Analyzer;
The upper surface of the support base is fixed with gas transmission ring by more batter posts, and gas transmission ring set is located at the outside of autoclave body, gas transmission It is provided with gas distribution channel in ring, multiple gas-charging connections are provided on gas transmission ring, and the inner wall of gas transmission ring is provided with more and gas transmission The appendix of channel connection, appendix one end tilt down and protrude into autoclave body inner cavity, the air taking port arrangement of all gas transmission bottom of the tube Cheng Yuan, and the air supply direction of air taking port and the circle are tangent, the appendix outside autoclave body is equipped with electronic valve;
It is intracavitary in the autoclave body to be equipped with temperature sensor, baroceptor, gas sensor, pH sensor and concentration sensing Device;
The support base is equipped with support rod, and support rod is equipped with PLC controller, and PLC controller includes Signal Pretreatment mould Block, PLC main control module, display module, LED display, drive module, alarm and memory module, the Signal Pretreatment mould Block, display module, drive module and memory module are connect with PLC main control module, and display module is connect with LED display, are driven Dynamic model block is connect with electronic valve and alarm, signal pre-processing module and temperature sensor, baroceptor, gas sensor, PH sensor is connected with concentration sensor.
2. the chemical reaction kettle according to claim 1 with detection system, it is characterised in that: the autoclave body includes outer gallbladder And liner, it is separated with gap between outer gallbladder and liner, and be fixed with multiple packing rings between outer gallbladder and liner, is filled in packing ring Aluminium hydroxide or magnesium hydroxide powder.
3. the chemical reaction kettle according to claim 1 with detection system, it is characterised in that: the gas-filtering device It is successively set on the intracorporal active carbon layer of shell, cao layers and microbe stuffing layer including shell and from top to bottom.
CN201820783114.1U 2018-05-24 2018-05-24 A kind of chemical reaction kettle with detection system Expired - Fee Related CN208407003U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820783114.1U CN208407003U (en) 2018-05-24 2018-05-24 A kind of chemical reaction kettle with detection system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820783114.1U CN208407003U (en) 2018-05-24 2018-05-24 A kind of chemical reaction kettle with detection system

Publications (1)

Publication Number Publication Date
CN208407003U true CN208407003U (en) 2019-01-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109821459A (en) * 2019-04-01 2019-05-31 北京清大元农生物科技有限公司 A kind of earthworm manure base fluid Liquid Fertilizer base fluid balance-type air inlet surge device and its production method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109821459A (en) * 2019-04-01 2019-05-31 北京清大元农生物科技有限公司 A kind of earthworm manure base fluid Liquid Fertilizer base fluid balance-type air inlet surge device and its production method
CN109821459B (en) * 2019-04-01 2023-08-22 北京清大元农生物科技有限公司 Earthworm excrement base liquid fertilizer base liquid balanced type air inlet agitation device and production method thereof

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190122

Termination date: 20200524