CN208103951U - A kind of high-purity barium chloride purifying plant - Google Patents
A kind of high-purity barium chloride purifying plant Download PDFInfo
- Publication number
- CN208103951U CN208103951U CN201721762265.0U CN201721762265U CN208103951U CN 208103951 U CN208103951 U CN 208103951U CN 201721762265 U CN201721762265 U CN 201721762265U CN 208103951 U CN208103951 U CN 208103951U
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- CN
- China
- Prior art keywords
- heating kettle
- barium chloride
- feed inlet
- purifying plant
- rotation axis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
A kind of high-purity barium chloride purifying plant, including heating kettle, the side wall of the heating kettle are hollow structure, and electric heating wire is equipped in hollow cavity, and the outermost layer of the heating kettle is insulating layer；The upper end of the heating kettle is equipped with lid, industrial chlorinating titanate feed inlet, deionized water feed inlet and motor, the barium chloride feed inlet and deionized water feed inlet, the output shaft and rotation axis connection of motor are equipped on lid, rotation axis is set in heating kettle, is equipped with agitating paddle on the rotating shaft；The lower section of rotation axis is equipped with filter plate in heating kettle, is equipped with discharge port in the lower end of heating kettle.The utility model provides a kind of high-purity barium chloride purifying plant, industrial chlorinating titanate can be dissolved in deionized water in heating kettle, and can be carried out primary filter, filters out the solid impurity in solution, improves the purity of barium chloride purification.
Description
Technical field
The utility model relates to Production of Barium Chloride technical field, especially a kind of high-purity barium chloride purifying plant.
Background technique
Barium chloride is colorless and transparent crystal, soluble easily in water, is slightly soluble in hydrochloric acid and nitric acid is insoluble in ethyl alcohol and ether, is easily inhaled
It is wet, it need to be sealed.Perform an analysis reagent, dehydrating agent, barium salt processed, and for industry such as electronics, instrument, metallurgy.High-purity chlorination
Barium is, by dissolution, removal of impurities, crystallization, cleaning, drying process, to obtain the less barium chloride of impurity using industrial chlorinating titanate as raw material,
However the solid sediment in solution cannot be completely eliminated in the process.
Summary of the invention
The technical problem to be solved by the utility model is to provide a kind of high-purity barium chloride purifying plants, can eliminate solution
In solid sediment.
In order to solve the above technical problems, technical solution used by the utility model is：A kind of high-purity barium chloride purification dress
It sets, including heating kettle, the side wall of the heating kettle is hollow structure, and electric heating wire, the heating kettle are equipped in hollow cavity
Outermost layer be insulating layer；The upper end of the heating kettle is equipped with lid, and industrial chlorinating titanate feed inlet, deionization are equipped on lid
Water feed inlet and motor, the barium chloride feed inlet and deionized water feed inlet, the output shaft and rotation axis connection of motor, rotation
It is located in heating kettle, is equipped with agitating paddle on the rotating shaft；The lower section of rotation axis is equipped with filter plate in heating kettle, in heating kettle
Lower end be equipped with discharge port.
Preferably, the inner sidewall of the heating kettle is equipped with limit stops, and filter plate is threadedly coupled with limit stops.
Preferably, the filter plate includes upper layer and lower layer stainless steel stratum reticulare, is set between the upper layer and lower layer stainless steel stratum reticulare
There is upper layer and lower layer filter cloth, is equipped with carbon fibre cloth layer between the upper layer and lower layer filter cloth.
Preferably, the top of the heating kettle is equipped with nitrogen forcing pipe.
Preferably, the barium chloride feed inlet is equipped with sealing cover, and the deionized water feed inlet is equipped with valve.
Preferably, the heating kettle is successively dried with flocculation deposition apparatus, crystallization apparatus, crystallization cleaning device and crystal
Device connection.
Preferably, the filter plate is equipped with handle.
The utility model provides a kind of high-purity barium chloride purifying plant, can be dissolved in industrial chlorinating titanate in heating kettle
It in ionized water, and can be carried out primary filter, filter out the solid impurity in solution, improve the purity of barium chloride purification.
Detailed description of the invention
The utility model is described in further detail with reference to the accompanying drawings and examples：
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the structural schematic diagram of the utility model limit stops；
Fig. 3 is the structural schematic diagram of the utility model filter plate；
Fig. 4 is the structural schematic diagram of another embodiment of the utility model；
In figure：Heating kettle 1, electric heating wire 2, insulating layer 3, lid 4, barium chloride feed inlet 5, deionized water feed inlet 6, electricity
Machine 7, rotation axis 8, agitating paddle 9, filter plate 10, stainless steel stratum reticulare 101, filter cloth 102, carbon fibre cloth layer 103, limit stops 11,
Discharge port 12, nitrogen forcing pipe 13, sealing cover 14, valve 15, crystallization apparatus 16 crystallize cleaning device 17, crystal drying dress
Set 18, handle 19, flocculation deposition apparatus 20.
Specific embodiment
As shown in Figure 1, a kind of high-purity barium chloride purifying plant, including heating kettle 1, the side wall of the heating kettle 1 are hollow
Structure, is equipped with electric heating wire 2 in hollow cavity, and the outermost layer of the heating kettle 1 is insulating layer 3；The upper end of the heating kettle 1
Equipped with lid 4, on lid 4 be equipped with industrial chlorinating titanate feed inlet 5, deionized water feed inlet 6 and motor 7, the barium chloride into
The output shaft of material mouth 5 and deionized water feed inlet 6, motor 7 is connect with rotation axis 8, and rotation axis is set in heating kettle 1, is being rotated
Axis 8 is equipped with agitating paddle 9；The lower section of rotation axis 8 is equipped with filter plate 10 in heating kettle 1, is equipped with discharging in the lower end of heating kettle 1
Mouth 12.Solution is mixed with solvent in heating kettle, and by filter plate, primary filtration is carried out to solution, after improving
Purity in continuous production process.
Preferably, as shown in Fig. 2, the inner sidewall of the heating kettle 1 is equipped with limit stops 11, filter plate 10 stops with limit
Gear 11 is threadedly coupled.After the sediment of filtering is more, openable lid 4, then rotary filter plate 10, filter plate is taken out,
It is cleaned.
Preferably, as shown in figure 3, the filter plate 10 includes upper layer and lower layer stainless steel stratum reticulare 101, the upper layer and lower layer are not
It is equipped with upper layer and lower layer filter cloth 102 between rust steel mesh layer 101, is equipped with carbon fibre cloth layer 103 between the upper layer and lower layer filter cloth 102.
Preferably, the filter plate 10 is equipped with handle 19.
Preferably, the top of the heating kettle 1 is equipped with nitrogen forcing pipe 13.
Preferably, the barium chloride feed inlet 5 is equipped with sealing cover 14, and the deionized water feed inlet 6 is equipped with valve
15.Nitrogen progress pressure filtration is passed through using nitrogen forcing pipe all to close sealing cover 14 and valve 15 in pressure filtration.
Preferably, as shown in figure 4, the heating kettle 1 is successively cleaned with flocculation deposition apparatus 20, crystallization apparatus 16, crystallization
Device 17 and crystal drying unit 18 connect.Aforesaid operations are repeated several times, finally obtain the barium chloride of high-purity.
The above embodiments are only the optimal technical scheme of the utility model, and are not construed as the limit for the utility model
System, the technical solution that the protection scope of the utility model should be recorded with claim, the technical solution recorded including claim
The equivalents of middle technical characteristic are protection scope.Equivalent replacement i.e. within this range is improved, also in the utility model
Protection scope within.
Claims (7)
1. a kind of high-purity barium chloride purifying plant, including heating kettle（1）, it is characterised in that：The heating kettle（1）Side wall be
Hollow structure is equipped with electric heating wire in hollow cavity（2）, the heating kettle（1）Outermost layer be insulating layer（3）；The heating
Kettle（1）Upper end be equipped with lid（4）, in lid（4）It is equipped with industrial chlorinating titanate feed inlet（5）, deionized water feed inlet（6）And
Motor（7）, the barium chloride feed inlet（5）And deionized water feed inlet（6）, motor（7）Output shaft and rotation axis（8）Even
It connects, rotation axis is set to heating kettle（1）It is interior, in rotation axis（8）It is equipped with agitating paddle（9）；In heating kettle（1）Interior rotation axis（8）'s
Lower section is equipped with filter plate（10）, in heating kettle（1）Lower end be equipped with discharge port（12）.
2. a kind of high-purity barium chloride purifying plant according to claim 1, it is characterised in that：The heating kettle（1）Inside
Wall is equipped with limit stops（11）, filter plate（10）With limit stops（11）It is threadedly coupled.
3. a kind of high-purity barium chloride purifying plant according to claim 2, it is characterised in that：The filter plate（10）Including upper
Lower two layers of stainless steel stratum reticulare（101）, the upper layer and lower layer stainless steel stratum reticulare（101）Between be equipped with upper layer and lower layer filter cloth（102）, institute
State upper layer and lower layer filter cloth（102）Between be equipped with carbon fibre cloth layer（103）.
4. a kind of high-purity barium chloride purifying plant according to claim 1, it is characterised in that：The heating kettle（1）Top
Equipped with nitrogen forcing pipe（13）.
5. a kind of high-purity barium chloride purifying plant according to claim 1, it is characterised in that：The barium chloride feed inlet（5）
It is equipped with sealing cover（14）, the deionized water feed inlet（6）It is equipped with valve（15）.
6. a kind of high-purity barium chloride purifying plant according to claim 1, it is characterised in that：The heating kettle（1）Successively with
Flocculation deposition apparatus（20）, crystallization apparatus（16）, crystallization cleaning device（17）And crystal drying unit（18）Connection.
7. a kind of high-purity barium chloride purifying plant according to claim 2, it is characterised in that：The filter plate（10）It is equipped with
Handle（19）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721762265.0U CN208103951U (en) | 2017-12-18 | 2017-12-18 | A kind of high-purity barium chloride purifying plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721762265.0U CN208103951U (en) | 2017-12-18 | 2017-12-18 | A kind of high-purity barium chloride purifying plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208103951U true CN208103951U (en) | 2018-11-16 |
Family
ID=64131026
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721762265.0U Expired - Fee Related CN208103951U (en) | 2017-12-18 | 2017-12-18 | A kind of high-purity barium chloride purifying plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208103951U (en) |
-
2017
- 2017-12-18 CN CN201721762265.0U patent/CN208103951U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181116 Termination date: 20201218 |