CN213966628U

CN213966628U - Crystallization reaction kettle

Info

Publication number: CN213966628U
Application number: CN202023016999.9U
Authority: CN
Inventors: 吕秀花; 杜海波; 邱曌; 任晶; 索腾腾
Original assignee: Shandong Guofengyuda Agrochemical Technology Co ltd
Current assignee: Shandong Guofengyuda Agrochemical Technology Co ltd
Priority date: 2020-12-14
Filing date: 2020-12-14
Publication date: 2021-08-17
Anticipated expiration: 2030-12-14

Abstract

The utility model discloses a crystallization reaction kettle relates to reation kettle technical field, including the crystallization kettle body, drive arrangement and purifier, the bottom of the crystallization kettle body and drive arrangement's top threaded connection, the right side pipe connection of the crystallization kettle body has the blast pipe, the bottom of blast pipe and purifier's top through connection, purifier's below is provided with the water tank, the discharge gate has been seted up in the left side of the crystallization kettle body. The utility model discloses a clean piece that sets up on the surface of driven shaft can drive clean piece and rotate in the inside of the crystallizer body at the pivoted in-process when the driven shaft to realized striking off clear process to the crystallization object that is detained on the inside of the crystallizer body, and the inlet tube that sets up in the inside of driven shaft and the cooperation of spraying the pipeline, can clean the inside of the crystallizer body, further improve the efficiency of purifying through the cooperation of active carbon filter screen and spray thrower.

Description

Crystallization reaction kettle

Technical Field

The utility model relates to a reation kettle technical field, concretely relates to crystallization reation kettle.

Background

The crystallization kettle is a crystallization device for rapidly reducing temperature after material mixing reaction, and a recrystallization reaction kettle in the prior art usually comprises a reaction kettle, a refrigerant interlayer and a stirring paddle, wherein the interlayer is filled with chilled water or refrigerant water to crystallize solute in a solution in the crystallization kettle.

At present in the in-process of crystallization have some products to be detained in the reation kettle inside, extremely inconvenient to it scrapes the clearance, and to the material difference of reactant, need wash the clearance to the inside water of carrying on of reation kettle, can produce certain harmful gas moreover at the in-process that the reactant stirring mixes and can not carry out purification treatment to it, this crystallization reation kettle's suitability variation, consequently need carry out the structure innovation and solve specific problem.

SUMMERY OF THE UTILITY MODEL

The technical problem to be solved by the utility model is to provide a crystallization reaction kettle, wherein one purpose is to clean and scrape the objects retained in the crystallization kettle body conveniently, and solve the problem that the objects retained on the inner wall of the crystallization kettle body are difficult to clean; the other purpose is to solve the problem that gas generated in the crystallization kettle body cannot be purified, so that harmful gas generated in the crystallization kettle body is filtered to reduce the influence on air.

In order to solve the technical problem, the utility model discloses the technical scheme who adopts is:

the utility model provides a crystallization reaction kettle, includes the crystallization kettle body, drive arrangement and purifier, the bottom of the crystallization kettle body and drive arrangement's top threaded connection, the right side pipe connection of the crystallization kettle body has the blast pipe, the bottom of blast pipe and purifier's top through connection, purifier's below is provided with the water tank, the discharge gate has been seted up in the left side of the crystallization kettle body.

The utility model discloses technical scheme's further improvement lies in: the driving device comprises a driving motor, a driving belt, a driven shaft and a driving shaft, the driving end of the driving motor is fixedly connected with the bottom of the driving shaft, the outer wall of the driving shaft is in transmission connection with the inner side wall of the driving belt, the upper end and the lower end of the driven shaft are in rotation connection with the inner wall of the crystallization kettle body, and the inner side wall of the driving belt is in rotation connection with the outer wall of the driven shaft.

The utility model discloses technical scheme's further improvement lies in: purifier's inner wall is provided with purifying liquid and places case, spray thrower, active carbon adsorption net, swash plate, liquid case and negative-pressure air fan of keeping in, purifying liquid places the bottom of case and the receiving terminal sealing connection of spray thrower, and the output of spray thrower and the inner wall through connection of blast pipe, purifying liquid places the left side setting that the case is located the blast pipe, and purifying liquid places the outer wall of case and purifier's inner wall fixed connection, the bottom sealing connection of blast pipe has the purifying box, and the inner wall of purifying box and the both ends joint of active carbon adsorption net, the bottom of swash plate and the inner wall fixed connection of purifying box, the top of liquid case and the bottom through connection of purifying box keep in.

The utility model discloses technical scheme's further improvement lies in: the bottom of negative-pressure air fan and purifier's inner wall bottom fixed connection, negative-pressure air fan's output and the inner wall through connection of purifying box, the bottom of liquid temporary storage case and purifier's inner wall bottom sliding connection, and liquid temporary storage case is located negative-pressure air fan's left side setting.

The utility model discloses technical scheme's further improvement lies in: the axle center department of driven shaft is provided with the inlet tube, the outer wall of inlet tube runs through in the inner wall of the crystallizer body, and the inner wall through connection of the one end of inlet tube and water tank, the outer wall through connection of inlet tube has the spray line, the outer wall of spray line runs through in the inner wall of driven shaft, the outer wall fixedly connected with cleaning block of driven shaft, the one end of cleaning block and the inner wall both sides overlap joint of the crystallizer body.

The utility model discloses technical scheme's further improvement lies in: the outer wall of drive shaft rotates with the inner wall of layer board to be connected, the driven shaft rotates with the crystallization kettle body through the drive belt that sets up to be connected, the outer wall fixedly connected with puddler of drive shaft, the feed inlet has been seted up at the top of the crystallization kettle body.

Owing to adopted above-mentioned technical scheme, the utility model discloses relative prior art, the technological progress who gains is:

1. the utility model provides a crystallization reaction kettle, through the clean piece of a plurality of that sets up on the surface of driven shaft, can drive the clean piece at the pivoted in-process and rotate in the inside of the crystallization kettle body when the driven shaft, thereby realized striking off clear process to the crystallization object that is detained on the inside of the crystallization kettle body, and the inlet tube that sets up in the inside of driven shaft and the cooperation of spraying the pipeline, can clean the inside of the crystallization kettle body, and lead to pipe will link together through water pipe and water tank, realized the process of cleaning after the crystallization kettle body work, the unchangeable problem of the present crystallization kettle body clearance has been solved.

2. The utility model provides a crystallization reaction kettle, discharge purifier's inside with the internal harmful gas of crystallization kettle through adopting the blast pipe, place the inside of case to purifying liquid and add corresponding harmful liquid of removing and handle through the harmful gas of shower in gas at first, and clear up it through the active carbon filter screen once more, improve the efficiency of purification, consider that there is the production of liquid at the in-process of purification, the cooperation through swash plate and liquid temporary storage case can be collected the liquid that produces in the purifying process, and the negative-pressure air fan who sets up is convenient for discharge the gas in the purifier inside.

Drawings

Fig. 1 is a schematic structural view of the present invention;

FIG. 2 is a sectional view of the crystallization kettle body structure of the present invention;

FIG. 3 is a top view of the driven shaft structure of the present invention;

fig. 4 is a cross-sectional view of the purification device of the present invention.

In the figure: 1. a crystallization kettle body; 2. a drive device; 21. a drive motor; 22. a transmission belt; 23. a driven shaft; 24. a drive shaft; 25. a cleaning block; 3. an exhaust pipe; 4. a purification device; 41. a purified liquid holding tank; 42. a sprayer; 43. an activated carbon adsorption net; 44. a sloping plate; 45. a liquid temporary storage tank; 46. a negative pressure fan; 5. a water tank; 6. a support plate; 7. a water inlet pipe; 8. and (4) spraying a pipeline.

Detailed Description

The present invention will be described in further detail with reference to the following examples:

example 1

As shown in fig. 1-4, the utility model provides a crystallization reaction kettle, including the crystallization kettle body 1, drive arrangement 2 and purifier 4, the bottom of the crystallization kettle body 1 and drive arrangement 2's top threaded connection, the right side pipe connection of the crystallization kettle body 1 has blast pipe 3, the bottom of blast pipe 3 and purifier 4's top through connection, and purifier 4's below is provided with water tank 5, and the discharge gate has been seted up in the left side of the crystallization kettle body 1.

In this embodiment, can realize stirring the mixture to the inside object of the crystallization kettle body 1 through the drive arrangement 2 that sets up, and can produce certain harmful gas at the in-process that the stirring was mixed, discharge the inside of purifier 4 with harmful gas through blast pipe 3, realize the purification to harmful gas, can reduce harmful gas and discharge the health that influences the staff on scene in the air, and the water tank 5 that sets up is for spraying the clearance to the inside of the crystallization kettle body 1.

As shown in fig. 2-3, in this embodiment, the driving device 2 includes a driving motor 21, a transmission belt 22, a driven shaft 23 and a driving shaft 24, a driving end of the driving motor 21 is fixedly connected to a bottom of the driving shaft 24, an outer wall of the driving shaft 24 is in transmission connection with an inner wall of the transmission belt 22, upper and lower ends of the driven shaft 23 are in rotational connection with an inner wall of the crystallization kettle body 1, the inner wall of the transmission belt 22 is in rotational connection with an outer wall of the driven shaft 23, a water inlet pipe 7 is disposed at an axial center of the driven shaft 23, an outer wall of the water inlet pipe 7 penetrates through the inner wall of the crystallization kettle body 1, one end of the water inlet pipe 7 is in through connection with the inner wall of the water tank 5, a bottom of the water inlet pipe 7 is movably connected to a water pipe, and a booster pump is disposed at one side of the water tank 5, so as to boost water in the water tank 5 to the interior of the water inlet pipe 7 through the water spraying pipe 8 and spray water to the interior of the crystallization kettle body 1, the problem of inconvenient cleaning of the interior of the reaction kettle body 1 is solved by realizing the process of cleaning the interior of the reaction kettle body 1 by water, the outer wall of the water inlet pipe 7 is connected with the spraying pipeline 8 in a penetrating way, the outer wall of the spraying pipeline 8 penetrates through the inner wall of the driven shaft 23, the outer wall of the driven shaft 23 is fixedly connected with the cleaning block 25, one end of the cleaning block 25 is in lap joint with two sides of the inner wall of the reaction kettle body 1, the cleaning block 25 can be driven to rotate by the rotation of the driving shaft 24, so that objects retained on the inner wall of the reaction kettle body 1 are scraped and cleaned, the problem that the objects are stuck in the reaction kettle body 1 for a long time and are difficult to clean is avoided, the cleaning effect of the reaction kettle body 1 is better by the matching of the water pipe 7 and the cleaning block 25, the outer wall of the driving shaft 24 is rotatably connected with the inner wall of the supporting plate 6, the driven shaft 23 is rotatably connected with the reaction kettle body 1 by the arranged driving belt 22, and the outer wall of the driving shaft 24 is fixedly connected with the stirring rod, the top of the crystallization kettle body 1 is provided with a feeding hole.

Example 2

As shown in fig. 1 and 4, on the basis of embodiment 1, the utility model provides a technical solution: the inner wall of the purification device 4 is provided with a purified liquid placing box 41, a sprayer 42, an activated carbon adsorption net 43, an inclined plate 44, a liquid temporary storage box 45 and a negative pressure fan 46, the bottom of the purified liquid placing box 41 is connected with the receiving end of the sprayer 42 in a sealing way, the output end of the sprayer 42 is connected with the inner wall of the exhaust pipe 3 in a penetrating way, the purified liquid placing box 41 is arranged on the left side of the exhaust pipe 3, the outer wall of the purified liquid placing box 41 is fixedly connected with the inner wall of the purification device 4, corresponding harmful liquid is added into the purified liquid placing box 41, harmful molecules in the gas in the exhaust pipe 3 are firstly treated by the sprayer 42, the bottom of the exhaust pipe 3 is connected with a purification box in a sealing way, the inner wall of the purification box is clamped with the two ends of the activated carbon adsorption net 43 and is cleaned again by the activated carbon filter net 43, the gas purification efficiency is improved, the bottom of the inclined plate 44 is fixedly connected with the inner wall of the purification box, the top of the liquid temporary storage box 45 is connected with the bottom of the purification box in a penetrating way, considering that liquid can be generated in the purification process, the liquid generated in the purification process can be collected through the matching of the inclined plate 44 and the liquid temporary storage box 45, the bottom of the negative pressure fan 46 is fixedly connected with the bottom of the inner wall of the purification device 4, the output end of the negative pressure fan 46 is connected with the inner wall of the purification box in a penetrating way, the arranged negative pressure fan 46 is convenient for discharging gas in the purification device 4, the bottom of the liquid temporary storage box 45 is connected with the bottom of the inner wall of the purification device 4 in a sliding way, and the liquid temporary storage box 45 is arranged on the left side of the negative pressure fan 46.

The working principle of the crystallization reaction kettle is as follows:

as shown in fig. 1-4, the utility model discloses after pouring the reactant into the inside of the crystallizer body 1, stir the mixture through starting driving motor 21 to the reactant, drive the rotation of drive shaft 24 in driving motor 21 pivoted, thereby transmit power for driven shaft 23 through drive belt 22, drive the rotation of clean piece 25 at driven shaft 23 pivoted in-process, thereby realize the process to the inside clearance of the crystallizer body 1, the inside of purifier 4 is delivered to with gas discharge through blast pipe 3 to the gas that produces at the in-process of stirring carries out filtration treatment.

The present invention has been described in detail with reference to the above general description, but it will be apparent to one of ordinary skill in the art that modifications and improvements can be made to the invention. Therefore, modifications or improvements without departing from the spirit of the invention are within the scope of the invention.

Claims

1. The utility model provides a crystallization reaction kettle, includes the crystallization kettle body (1), drive arrangement (2) and purifier (4), its characterized in that: the bottom of the crystallizer body (1) and the top threaded connection of drive arrangement (2), the right side pipe connection of the crystallizer body (1) has blast pipe (3), the bottom of blast pipe (3) and the top through connection of purifier (4), the below of purifier (4) is provided with water tank (5), the discharge gate has been seted up in the left side of the crystallizer body (1).

2. A crystallization reactor as defined in claim 1, wherein: drive arrangement (2) include driving motor (21), drive belt (22), driven shaft (23) and drive shaft (24), the drive end of driving motor (21) and the bottom fixed connection of drive shaft (24), the outer wall of drive shaft (24) is connected with the inside wall transmission of drive belt (22), the upper and lower both ends of driven shaft (23) are connected with the inner wall rotation of the crystallization kettle body (1), the inside wall rotation of drive belt (22) is connected with the outer wall rotation of driven shaft (23).

3. A crystallization reactor as defined in claim 1, wherein: the inner wall of the purification device (4) is provided with a purified liquid placing box (41), a sprayer (42), an activated carbon adsorption net (43), an inclined plate (44), a liquid temporary storage box (45) and a negative pressure fan (46), the bottom of the purified liquid placing box (41) is hermetically connected with the receiving end of the sprayer (42), and the output end of the sprayer (42) is communicated with the inner wall of the exhaust pipe (3), the purified liquid placing box (41) is arranged at the left side of the exhaust pipe (3), the outer wall of the purified liquid placing box (41) is fixedly connected with the inner wall of the purifying device (4), the bottom of the exhaust pipe (3) is hermetically connected with the purifying box, and the inner wall of the purifying box is clamped with the two ends of the activated carbon adsorption net (43), the bottom of the inclined plate (44) is fixedly connected with the inner wall of the purifying box, and the top of the liquid temporary storage box (45) is communicated with the bottom of the purifying box.

4. A crystallization reactor as defined in claim 3, wherein: the bottom of negative-pressure air fan (46) and the inner wall bottom fixed connection of purifier (4), the output of negative-pressure air fan (46) and the inner wall through connection of purifying box, the bottom of liquid temporary storage case (45) and the inner wall bottom sliding connection of purifier (4), and liquid temporary storage case (45) are located the left side setting of negative-pressure air fan (46).

5. A crystallization reactor as defined in claim 2, wherein: the axle center department of driven shaft (23) is provided with inlet tube (7), the outer wall of inlet tube (7) runs through in the inner wall of the crystallizer body (1), and the inner wall through connection of the one end of inlet tube (7) and water tank (5), the outer wall through connection of inlet tube (7) has spraying pipe way (8), the outer wall of spraying pipe way (8) runs through in the inner wall of driven shaft (23), the outer wall fixedly connected with cleaning block (25) of driven shaft (23), the one end of cleaning block (25) and the inner wall both sides overlap joint of the crystallizer body (1).

6. A crystallization reactor as defined in claim 2, wherein: the outer wall of drive shaft (24) rotates with the inner wall of layer board (6) to be connected, driven shaft (23) rotate with the crystallization kettle body (1) through drive belt (22) that sets up and are connected, the outer wall fixedly connected with puddler of drive shaft (24), the feed inlet has been seted up at the top of the crystallization kettle body (1).