CN209771374U - Distillation tower for purifying musk - Google Patents
Distillation tower for purifying musk Download PDFInfo
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- CN209771374U CN209771374U CN201920237465.7U CN201920237465U CN209771374U CN 209771374 U CN209771374 U CN 209771374U CN 201920237465 U CN201920237465 U CN 201920237465U CN 209771374 U CN209771374 U CN 209771374U
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Abstract
The utility model discloses a distillation column is used in musk purification relates to musk and makes technical field. Including first distillation column, first distillation chamber and second distillation chamber have been seted up in proper order from the top down to the inside of first distillation column, and the first board that helps of bottom fixedly connected with of first distillation chamber, the bottom swing joint of first board that helps has first liquid export, and liquid inlet has been seted up to the lateral wall department of first distillation chamber, and the fixed block net of lateral wall department fixedly connected with of first distillation chamber, the last surface packing of fixed block net have the filler, the first gas pipe of top fixedly connected with of first distillation chamber. This distillation column is used in musk purification through setting up first distillation column, first distillation chamber, second distillation chamber and second distillation column, utilizes first distillation column to reach the effect of carrying out the distillation purification work to first distillation chamber and second distillation chamber simultaneously, utilizes second distillation column to reach the effect of carrying out the purification distillation to the gas of first distillation column offtake, greatly reduced the cost of product processing.
Description
Technical Field
The utility model relates to the technical field of musk manufacturing, in particular to a distillation tower for musk purification.
Background
Musk is the dry secretion in the musk deer in musk family, musk deer or the male sachet of the original musk deer, and is also a medicinal material, namely musk, Moschus, Clerodera odorata, and navel, wherein the musk has wide application, can be used for preparing traditional Chinese medicines and also can be used for preparing spices, and the musk needs to be distilled and purified in the production and processing process and is generally finished in a distillation tower.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
To prior art not enough, the utility model provides a distillation column is used in musk purification possesses advantages such as purification efficiency height, has solved the problem that current distillation column work efficiency is low.
(II) technical scheme
In order to realize the purpose of high purification efficiency, the utility model provides a following technical scheme: a distillation tower for purifying musk comprises a first distillation tower, wherein a first distillation chamber and a second distillation chamber are sequentially arranged in the first distillation tower from top to bottom, the bottom of the first distillation chamber is fixedly connected with a first flow assisting plate, the bottom of the first flow assisting plate is movably connected with a first liquid outlet, the side wall of the first distillation chamber is provided with a liquid inlet, the side wall of the first distillation chamber is fixedly connected with a fixed blocking net, the upper surface of the fixed blocking net is filled with filler, the top of the first distillation chamber is fixedly connected with a first gas pipe, the outer wall of the first distillation chamber is fixedly connected with a first motor, the output shaft of the first motor is fixedly connected with a first rotating shaft, one end of the first rotating shaft is movably connected with a first stirring frame through a first conical gear, and the inside of the second distillation chamber is fixedly connected with a second flow assisting plate, the bottom of the second flow assisting plate is fixedly connected with a storage tank through a second liquid outlet, a second gas pipe is fixedly connected to the side wall of the second distillation chamber, the second gas pipe is fixedly connected to the side wall of the first gas pipe, the first gas pipe is fixedly connected with a condenser, and a liquid outlet of the condenser is fixedly connected with a second distillation tower through a water pipe.
Further optimize this technical scheme, the outer wall department of first distillation chamber and second distillation chamber all is provided with the temperature barometer, one side fixedly connected with first sampling device of first distillation chamber outer wall, one side fixedly connected with second sampling device of second distillation chamber outer wall, first sampling device includes the sample ball valve, the one end threaded connection of sample ball valve is in the outer wall department of first distillation chamber, the other end threaded connection of sample ball valve has the gas sampling pipe.
Further optimizing the technical scheme, the first liquid outlet and the second liquid outlet are both provided with liquid outlet valves, the first flow assisting plate is V-shaped, and the specification of the first flow assisting plate is the same as that of the second flow assisting plate.
Further optimize this technical scheme, the lateral wall department fixedly connected with second motor of second distillation chamber, the output shaft fixedly connected with second pivot of second motor, the one end of second pivot has the second stirring frame through second conical gear swing joint, the bottom of second stirring frame is provided with arc stirring leaf, the specification of second stirring frame is the same with the specification of first stirring frame.
Further optimize this technical scheme, the bottom of condenser is passed through supporting seat fixed connection at the upper surface of storage tank, one side at storage tank top and the bottom fixed connection of second distillation column, the bottom of second distillation column is provided with the third liquid outlet, the top fixedly connected with third gas pipe of second distillation column.
Further optimizing the technical scheme, a third sampling device is connected to the side wall of the second distillation tower in a threaded mode, and the specification of the third sampling device is the same as that of the first sampling device and that of the second sampling device.
(III) advantageous effects
Compared with the prior art, the utility model provides a distillation column is used in musk purification possesses following beneficial effect:
1. This distillation column is used in musk purification, through setting up first distillation column, first distillation chamber, second distillation chamber and second distillation column, utilize first distillation column to reach the effect of carrying out the distillation purification work to first distillation chamber and second distillation chamber simultaneously, utilize second distillation column to reach the effect of carrying out the purification distillation to first distillation column combustion gas, greatly reduced the cost of product processing, musk's purification efficiency and product purity have been improved greatly, the trouble of changing equipment in the production process has been reduced, save time and labor, greatly reduced cost of labor and processing equipment cost.
2. This distillation column is used in musk purification, through setting up the filler, first stirring frame, first sampling device, second stirring frame and third sampling device, the utilization is packed and has been reached the effect of getting rid of the granule impurity among the exhaust gas, the purity of musk purification has been improved, utilize first stirring frame and the effectual musk raw materials that stirs of second stirring frame, the distillation purification efficiency of musk raw materials has been improved, the time of processing purification has been practiced thrift, utilize first sampling device, second sampling device and third sampling device have reached the effect of detecting the different positions combustion gas, conveniently observe progress and the purity of inspection musk distillation purification, musk's purification efficiency and product purity have been improved greatly.
Drawings
FIG. 1 is a schematic structural view of the present invention;
Fig. 2 is a schematic structural diagram of the first sampling device of the present invention.
In the figure: 1. a first distillation column; 2. a first distillation chamber; 3. a second distillation chamber; 4. a first flow promoting plate; 5. a first liquid outlet; 6. a liquid inlet; 7. fixing the blocking net; 8. a filler; 9. a first gas pipe; 10. a first motor; 11. a first rotating shaft; 12. a first conical gear; 13. a first stirring frame; 14. a second flow promoting plate; 15. a second liquid outlet; 16. a material storage tank; 17. a second gas pipe; 18. a condenser; 19. a water pipe; 20. a second distillation column; 21. a first sampling device; 211. a sampling ball valve; 212. a gas sampling tube; 22. a second sampling device; 23. a second motor; 24. a second rotating shaft; 25. a second conical gear; 26. a second stirring frame; 27. a third liquid outlet; 28. a third gas pipe; 29. and a third sampling device.
Detailed Description
the technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-2, the utility model discloses a distillation tower for purifying musk, comprising a first distillation tower 1, wherein a first distillation chamber 2 and a second distillation chamber 3 are sequentially arranged in the first distillation tower 1 from top to bottom, the first distillation tower 1 achieves the effect of distilling and purifying the first distillation chamber 2 and the second distillation chamber 3 simultaneously, the bottom of the first distillation chamber 2 is fixedly connected with a first flow-assisting plate 4, the bottom of the first flow-assisting plate 4 is movably connected with a first liquid outlet 5, the side wall of the first distillation chamber 2 is provided with a liquid inlet 6, the side wall of the first distillation chamber 2 is fixedly connected with a fixed baffle net 7, the upper surface of the fixed baffle net 7 is filled with a filler 8, the filler 8 achieves the effect of removing particle impurities in exhaust gas, the purity of musk is improved, the top of the first distillation chamber 2 is fixedly connected with a first gas pipe 9, a first motor 10 is fixedly connected to the outer wall of the first distillation chamber 2, a first rotating shaft 11 is fixedly connected to an output shaft of the first motor 10, one end of the first rotating shaft 11 is movably connected with a first stirring frame 13 through a first bevel gear 12, the musk raw materials are effectively stirred by the first stirring frame 13 and a second stirring frame 26, the distillation and purification efficiency of the musk raw materials is improved, the processing and purification time is saved, a second flow-assisting plate 14 is fixedly connected to the inside of the second distillation chamber 3, the bottom of the second flow-assisting plate 14 is fixedly connected with a material storage tank 16 through a second liquid outlet 15, a second gas pipe 17 is fixedly connected to the side wall of the second distillation chamber 3, the second gas pipe 17 is fixedly connected to the side wall of the first gas pipe 9, a condenser 18 is fixedly connected to the first gas pipe 9, a second distillation tower 20 is fixedly connected to the liquid outlet of the condenser 18 through a water pipe 19, utilize second distillation column 20 to reach the effect of carrying out purification distillation to first distillation column 1 combustion gas, greatly reduced the cost of product processing, musk's purification efficiency and product purity have been improved greatly, the trouble of changing equipment in the production process has been reduced, and is time-saving and labor-saving, greatly reduced cost of labor and processing equipment cost, utilize first sampling device 21, second sampling device 22 and third sampling device 29 have reached the effect of detecting different positions combustion gas, conveniently observe the progress and the purity of inspection musk distillation purification, musk's purification efficiency and product purity have been improved greatly.
Concretely, the outer wall department of first distillation chamber 2 and second distillation chamber 3 all is provided with the temperature barometer, the first sampling device 21 of one side fixedly connected with of 2 outer walls of first distillation chamber, one side fixedly connected with second sampling device 22 of 3 outer walls of second distillation chamber, first sampling device 21 is including sample ball valve 211, the one end threaded connection of sample ball valve 211 is in the outer wall department of first distillation chamber 2, the other end threaded connection of sample ball valve 211 has gas sampling tube 212, utilize first sampling device 21, second sampling device 22 and third sampling device 29 have reached the effect of detecting the gas of different positions's combustion gas, conveniently observe the progress and the purity of inspection musk distillation purification, musk's purification efficiency and product purity have been improved greatly.
Specifically, the first liquid outlet 5 and the second liquid outlet 15 are both provided with liquid outlet valves, the first flow promoting plate 4 is V-shaped, and the specification of the first flow promoting plate 4 is the same as that of the second flow promoting plate 14.
Specifically, the side wall of the second distillation chamber 3 is fixedly connected with a second motor 23, the type of the second motor 23 is YE2-132S-4, the type of the second motor 23 is the same as that of the first motor 10, an output shaft of the second motor 23 is fixedly connected with a second rotating shaft 24, one end of the second rotating shaft 24 is movably connected with a second stirring frame 26 through a second bevel gear 25, the bottom of the second stirring frame 26 is provided with an arc-shaped stirring blade, the specification of the second stirring frame 26 is the same as that of the first stirring frame 13, the first stirring frame 13 and the second stirring frame 26 are used for effectively stirring the musk raw material, the distillation and purification efficiency of the musk raw material is improved, and the processing and purification time is saved.
Concretely, the bottom of condenser 18 is through the upper surface of supporting seat fixed connection at storage tank 16, one side at storage tank 16 top and the bottom fixed connection of second distillation column 20, the bottom of second distillation column 20 is provided with third liquid outlet 27, the top fixedly connected with third gas pipe 28 of second distillation column 20, utilize second distillation column 20 to reach the effect of carrying out the purification distillation to first distillation column 1 combustion gas, greatly reduced the cost of product processing, musk's purification efficiency and product purity have been improved greatly, the trouble of changing equipment in the production process has been reduced, time saving and labor saving, greatly reduced cost of labor and processing equipment cost.
Specifically, the threaded connection of lateral wall department of second distillation column 20 has third sampling device 29, and the specification of third sampling device 29 is the same with first sampling device 21, second sampling device 22, utilizes first sampling device 21, second sampling device 22 and third sampling device 29 to reach the effect that detects the gas of different positions exhanst, conveniently observes progress and the purity of inspection musk distillation purification, has improved the purification efficiency and the product purity of musk greatly.
When in use, musk raw material enters into the first distillation chamber 2 through the liquid inlet 6, the first distillation tower 1 is heated and distilled to 100 ℃, the boiling point of musk ketone in the musk raw material in the first distillation chamber 2 is 130 ℃, other solvent impurities are heated and evaporated and discharged through the first gas tube 9, the primarily purified musk raw material is discharged into the second distillation chamber 3 through the first liquid outlet 5, the second purification distillation work is carried out in the second distillation chamber 3, the gas after the second purification distillation work is discharged through the second gas tube 17, the purified liquid is discharged into the material storage tank 16 through the second liquid outlet 15, the gas discharged from the first distillation chamber 2 and the second distillation chamber 3 is cooled through the condenser 18 and then enters into the second distillation tower 20 for the third precise purification, the purified liquid enters into the material storage tank 16 through the third liquid outlet 27, the purified gas is discharged to the outside through the third gas pipe 28, and the first sampling device 21, the second sampling device 22 and the third sampling device 29 detect the gas discharged from different positions during the production process.
In conclusion, the distillation tower for purifying musk is provided with the first distillation tower 1, the first distillation chamber 2, the second distillation chamber 3 and the second distillation tower 20, the first distillation tower 1 is utilized to achieve the effect of simultaneously carrying out distillation and purification work on the first distillation chamber 2 and the second distillation chamber 3, and the second distillation tower 20 is utilized to achieve the effect of carrying out purification and distillation on gas discharged from the first distillation tower 1, so that the product processing cost is greatly reduced, the musk purification efficiency and the product purity are greatly improved, the trouble of replacing equipment in the production process is reduced, the time and the labor are saved, and the labor cost and the processing equipment cost are greatly reduced; this distillation column is used in musk purification, through setting up filler 8, first stirring frame 13, first sampling device 21, second sampling device 22, second stirring frame 26 and third sampling device 29, utilize filler 8 to reach the effect of getting rid of the granule impurity among the exhaust gas, the purity of musk purification has been improved, utilize first stirring frame 13 and the effectual musk raw materials that stirs of second stirring frame 26, the distillation purification efficiency of musk raw materials has been improved, the time of processing purification has been practiced thrift, utilize first sampling device 21, second sampling device 22 and third sampling device 29 have reached the effect of detecting the gas of different positions combustion gas, conveniently observe the progress and the purity of inspection musk distillation purification, musk's purification efficiency and product purity have been improved greatly.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A distillation column for purifying musk comprises a first distillation column (1), and is characterized in that: a first distillation chamber (2) and a second distillation chamber (3) are sequentially arranged in the first distillation tower (1) from top to bottom, a first flow assisting plate (4) is fixedly connected to the bottom of the first distillation chamber (2), a first liquid outlet (5) is movably connected to the bottom of the first flow assisting plate (4), a liquid inlet (6) is arranged on the side wall of the first distillation chamber (2), a fixed blocking net (7) is fixedly connected to the side wall of the first distillation chamber (2), a filler (8) is filled on the upper surface of the fixed blocking net (7), a first air pipe (9) is fixedly connected to the top of the first distillation chamber (2), a first motor (10) is fixedly connected to the outer wall of the first distillation chamber (2), a first rotating shaft (11) is fixedly connected to an output shaft of the first motor (10), and a first stirring frame (13) is movably connected to one end of the first rotating shaft (11) through a first bevel gear (12), the inside fixedly connected with second flow assist board (14) of second distillation chamber (3), the bottom of second flow assist board (14) is through second liquid outlet (15) fixedly connected with storage tank (16), the lateral wall department fixedly connected with second gas pipe (17) of second distillation chamber (3), second gas pipe (17) fixed connection is in the lateral wall department of first gas pipe (9), first gas pipe (9) fixed connection has condenser (18), the liquid outlet department of condenser (18) is through water pipe (19) fixedly connected with second distillation column (20).
2. The distillation column for purifying musk as claimed in claim 1, wherein: the outer wall department of first distillation chamber (2) and second distillation chamber (3) all is provided with temperature barometer, first sampling device (21) of one side fixedly connected with of first distillation chamber (2) outer wall, one side fixedly connected with second sampling device (22) of second distillation chamber (3) outer wall, first sampling device (21) are including sample ball valve (211), the outer wall department of the one end threaded connection of sample ball valve (211) in first distillation chamber (2), the other end threaded connection of sample ball valve (211) has gaseous sampling tube (212).
3. The distillation column for purifying musk as claimed in claim 1, wherein: liquid outlet valves are arranged on the first liquid outlet (5) and the second liquid outlet (15), the first flow assisting plate (4) is V-shaped, and the specification of the first flow assisting plate (4) is the same as that of the second flow assisting plate (14).
4. the distillation column for purifying musk as claimed in claim 1, wherein: the side wall of the second distillation chamber (3) is fixedly connected with a second motor (23), an output shaft of the second motor (23) is fixedly connected with a second rotating shaft (24), one end of the second rotating shaft (24) is movably connected with a second stirring frame (26) through a second bevel gear (25), an arc-shaped stirring blade is arranged at the bottom of the second stirring frame (26), and the specification of the second stirring frame (26) is the same as that of the first stirring frame (13).
5. The distillation column for purifying musk as claimed in claim 1, wherein: the bottom of the condenser (18) is fixedly connected to the upper surface of the material storage tank (16) through a support seat, one side of the top of the material storage tank (16) is fixedly connected with the bottom of the second distillation tower (20), a third liquid outlet (27) is formed in the bottom of the second distillation tower (20), and a third gas pipe (28) is fixedly connected to the top of the second distillation tower (20).
6. The distillation column for purifying musk as claimed in claim 1, wherein: a third sampling device (29) is connected to the side wall of the second distillation tower (20) in a threaded mode, and the specification of the third sampling device (29) is the same as that of the first sampling device (21) and that of the second sampling device (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920237465.7U CN209771374U (en) | 2019-02-25 | 2019-02-25 | Distillation tower for purifying musk |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920237465.7U CN209771374U (en) | 2019-02-25 | 2019-02-25 | Distillation tower for purifying musk |
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| Publication Number | Publication Date |
|---|---|
| CN209771374U true CN209771374U (en) | 2019-12-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201920237465.7U Active CN209771374U (en) | 2019-02-25 | 2019-02-25 | Distillation tower for purifying musk |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113144655A (en) * | 2021-04-28 | 2021-07-23 | 安徽金轩科技有限公司 | Jiale musk rectification unit and rectification process thereof |
-
2019
- 2019-02-25 CN CN201920237465.7U patent/CN209771374U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113144655A (en) * | 2021-04-28 | 2021-07-23 | 安徽金轩科技有限公司 | Jiale musk rectification unit and rectification process thereof |
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Address after: 123000 50 meters east of yimotu railway station, Fuxin City, Liaoning Province Patentee after: Liaoning Dongda Guangming Chemical Technology Co., Ltd Address before: 123000 50 meters east of yimotu railway station, Fuxin City, Liaoning Province Patentee before: Fuxin dongdaguang Chemical Co.,Ltd. |