CN208098072U - Band heating refrigeration synthesis reaction vessel - Google Patents

Band heating refrigeration synthesis reaction vessel Download PDF

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Publication number
CN208098072U
CN208098072U CN201820256807.5U CN201820256807U CN208098072U CN 208098072 U CN208098072 U CN 208098072U CN 201820256807 U CN201820256807 U CN 201820256807U CN 208098072 U CN208098072 U CN 208098072U
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stirring
pond
water
reaction kettle
hot
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CN201820256807.5U
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向必军
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Dongguan Yanlian Electronic New Material Co Ltd
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Dongguan Yanlian Electronic New Material Co Ltd
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Abstract

The utility model discloses a kind of bands to heat refrigeration synthesis reaction vessel, including reaction kettle shell, rabbling mechanism and heating refrigeration mechanism, reaction kettle shell are surrounded by water jacket;Rabbling mechanism includes stirring motor, stirring speed reducer, stirring connection frame, agitating shaft and dispersion impeller;Heating refrigeration mechanism includes hot-tub, buffering pond, cooling pond and return channel, hot-tub, cooling pond pass through water pump and water valve respectively and the water inlet of water jacket connects, hot-tub, cooling pond pass through water valve respectively and connect with buffering pond, the water outlet for buffering pond and water jacket connects, and return channel is connect with water jacket.The utility model is simple and reasonable, buffering pond is selectively recycled with hot-tub, cooling pond respectively, temperature control effect is preferable, and reaction kettle is suitable for material synthesis of the synthesis temperature between 25 DEG C~90 DEG C, and organic synthesis and modified synthesis or hot and cold spelling material is suitble to be blended.

Description

Band heating refrigeration synthesis reaction vessel
Technical field
The utility model belongs to reaction kettle technical field, and in particular to a kind of band heating refrigeration synthesis reaction vessel.
Background technique
Reaction kettle is a kind of chemical plant commonly consersion unit, mainly drives agitating shaft to be stirred to react by clicking Object reacts it sufficiently to obtain required substance.With the continuous hair of chemical field, production of the people to chemical products The precision of finished product and chemical products all improves higher requirement, and corresponding people are to the important equipment reaction kettle in chemical reaction More stringent requirements are proposed.Currently used reaction kettle realizes that long-time constant temperature is kept the temperature by way of heating, existing heating Heating water bath or electric heating is usually used in mode, and heating controllability is poor, be easy to cause the waste of the energy.
Utility model content
In order to solve the above-mentioned technical problem, the utility model provides a kind of band heating refrigeration synthesis reaction vessel.
In order to achieve the above object, the technical solution of the utility model is as follows:
The utility model provides a kind of band heating refrigeration synthesis reaction vessel, including:
Reaction kettle shell, the top cover of reaction kettle shell are equipped with feed inlet, and the bottom of reaction kettle shell is equipped with discharge port, instead The water jacket that is surrounded by of still shell body is answered, is equipped with thermometer in reaction kettle shell;
Rabbling mechanism, including stirring motor, stirring speed reducer, stirring connection frame, agitating shaft and dispersion impeller, stirring motor Output end is connect with the output end of stirring speed reducer, and the output end for stirring speed reducer is connect with stirring connection frame, stirs connection frame It is rotatably dispose on the top cover of reaction kettle shell, agitating shaft is set on stirring connection frame, and dispersion impeller is connected to stirring axis connection The bottom of frame;
Heat refrigeration mechanism, including hot-tub, buffering pond, cooling pond and return channel, hot-tub, buffering pond and cold But thermometer is respectively equipped in pond, hot-tub, cooling pond pass through water pump and water valve respectively and the water inlet of water jacket connects, heat Pond, cooling pond pass through water valve respectively and connect with buffering pond, and the water outlet for buffering pond and water jacket connects, return channel and water Set connection.
As a preferred option, above-mentioned stirring connection frame includes stirring connection main shaft and stirring terminal pad, stirring connection Main axis is set on the top cover of reaction kettle shell, and stirring terminal pad is set on stirring connection main shaft and the two is coaxially set It sets, the disk for stirring terminal pad is equipped with blade, and for blade along the radially movable setting of capstan winch terminal pad, stirring motor is variable-frequency electric Machine.
As a preferred option, above-mentioned connection main shaft is equipped with explosion-proof channel.
As a preferred option, the periphery of above-mentioned dispersion impeller is equipped with dispersion blade, and dispersion blade is bending structure, The bending structure of arbitrary neighborhood two dispersion blades is the setting of bending up and down, and the edge for dispersing blade is equipped with dispersion saw Tooth.
As a preferred option, above-mentioned dispersion impeller is equipped with axial connecting hole, on the upper disk surface of dispersion impeller and is located at axis It is equipped with bulge loop to the outside of connecting hole, also radial diversion trench is set on the upper disk surface of dispersion impeller.
As a preferred option, the fixed lid of bayonet type bolt and sealing ring are equipped at above-mentioned feed inlet.
As a preferred option, it is connected with flowmeter and valve control mechanism on above-mentioned return channel, discharge port is connected with The side wall of discharge tube, water jacket is equipped with polyimide heat-conducting layer.
The utility model has the advantages that:The utility model is compared to the prior art, simple and reasonable, buffering Pond is selectively recycled with hot-tub, cooling pond respectively, and temperature control effect is preferable, and reaction kettle is suitable for synthesis temperature 25 DEG C~90 DEG C between material synthesis, be suitble to organic synthesis and modified synthesis or the blending of hot and cold spellings material.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the utility model.
Specific embodiment
The preferred embodiment that according to the present invention will be described in detail below with reference to the accompanying drawings.
In order to reach the purpose of this utility model, as shown in Figure 1, being mentioned in one of embodiment of the utility model Refrigeration synthesis reaction vessel is heated for a kind of band, including:
The top cover of reaction kettle shell 10, reaction kettle shell 10 is equipped with feed inlet 11, and the bottom of reaction kettle shell 10 is equipped with Discharge port 12, reaction kettle shell 10 are surrounded by water jacket 13, are equipped with thermometer in reaction kettle shell 10;
Rabbling mechanism, including stirring motor 20, stirring speed reducer 21, stirring connection frame 22, agitating shaft 23 and dispersion impeller 24, The output end of stirring motor 20 is connect with the output end of stirring speed reducer 21, stirs the output end and stirring connection frame of speed reducer 21 22 connections, stirring connection frame 22 are rotatably dispose on the top cover of reaction kettle shell 10, and agitating shaft 23 is set to stirring connection frame 22 On, dispersion impeller 24 is connected to the bottom of stirring shaft holder 22;
Refrigeration mechanism is heated, including hot-tub 30, buffering pond 31, cooling pond 32 and return channel 33, hot-tub 30 delay Be respectively equipped with thermometer in bath pond 31 and cooling pond 32, hot-tub 30, cooling pond 32 respectively by water pump and water valve with The water inlet of water jacket 13 connects, and hot-tub 30, cooling pond 32 are connect by water valve with buffering pond 31 respectively, buffers pond 31 connect with the water outlet of water jacket 13, and return channel 33 is connect with water jacket 13.
Present embodiment is compared to the prior art, simple and reasonable, and buffering pond is selected with hot-tub, cooling pond respectively Selecting property is recycled, and temperature control effect is preferable, and reaction kettle is suitable for material synthesis of the synthesis temperature between 25 DEG C~90 DEG C, is suitble to Organic synthesis and modified synthesis or hot and cold spelling material are blended.
In order to further optimize the implementation result of the utility model, in the another embodiment of the utility model, On the basis of foregoing teachings, above-mentioned stirring connection frame includes stirring connection main shaft and stirring terminal pad, stirring connection main shaft It is rotatably dispose on the top cover of reaction kettle shell, stirring terminal pad is set on stirring connection main shaft and the two is coaxially disposed, and stirs The disk for mixing terminal pad is equipped with blade, and for blade along the radially movable setting of capstan winch terminal pad, stirring motor is variable-frequency motor.
Using above-mentioned preferred embodiment, blade, in radially movable setting, can carry out material under the drive of stirring motor Shearing improves stirring efficiency.
In order to further optimize the implementation result of the utility model, in the another embodiment of the utility model, On the basis of foregoing teachings, above-mentioned connection main shaft is equipped with explosion-proof channel.
Using above-mentioned preferred embodiment, explosion-proof channel is set on connection main shaft, does not need in addition to increase part, more just Just.
In order to further optimize the implementation result of the utility model, in the another embodiment of the utility model, On the basis of foregoing teachings, the periphery of above-mentioned dispersion impeller is equipped with dispersion blade, and dispersion blade is bending structure, arbitrarily The bending structure of two neighboring dispersion blade is the setting of bending up and down, and the edge for dispersing blade is equipped with dispersion sawtooth.
In addition, dispersion impeller is equipped with axial connecting hole, on the upper disk surface of dispersion impeller and it is located on the outside of axial connecting hole and sets There is bulge loop, also radial diversion trench is set on the upper disk surface of dispersion impeller.
Using above-mentioned preferred embodiment, setting dispersion sawtooth and radial diversion trench, avoid material in stirring on dispersion impeller Remain on dispersion impeller.
In order to further optimize the implementation result of the utility model, in the another embodiment of the utility model, The fixed lid of bayonet type bolt and sealing ring are equipped on the basis of foregoing teachings, at feed inlet.
In addition, being connected with flowmeter and valve control mechanism on return channel, discharge port is connected with discharge tube, the side of water jacket Wall is equipped with polyimide heat-conducting layer.
Using above-mentioned preferred embodiment, the flow of flowmeter and valve control mechanism control cooling return channel, to control Temperature in reaction kettle connects discharge tube on discharge port, convenient for discharging.
Above-described is only preferred embodiments of the present invention, it is noted that for the ordinary skill of this field For personnel, without departing from the concept of the present invention, various modifications and improvements can be made, these all belong to In the protection scope of the utility model.

Claims (7)

1. band heating refrigeration synthesis reaction vessel, which is characterized in that including:
Reaction kettle shell, the top cover of reaction kettle shell are equipped with feed inlet, and the bottom of reaction kettle shell is equipped with discharge port, reaction kettle Shell is surrounded by water jacket, is equipped with thermometer in reaction kettle shell;
Rabbling mechanism, including stirring motor, stirring speed reducer, stirring connection frame, agitating shaft and dispersion impeller, the output of stirring motor It holds and is connect with the output end of stirring speed reducer, the output end for stirring speed reducer is connect with stirring connection frame, stirring connection frame rotation It is set on the top cover of reaction kettle shell, agitating shaft is set on stirring connection frame, and dispersion impeller is connected to stirring shaft holder Bottom;
Heat refrigeration mechanism, including hot-tub, buffering pond, cooling pond and return channel, hot-tub, buffering pond and cooling water Thermometer is respectively equipped in pond, hot-tub, cooling pond pass through water pump and water valve respectively and the water inlet of water jacket connects, hot water Pond, cooling pond pass through water valve respectively and connect with buffering pond, and the water outlet for buffering pond and water jacket connects, return channel and water jacket Connection.
2. band according to claim 1 heats refrigeration synthesis reaction vessel, which is characterized in that stirring connection frame includes that stirring connects Main shaft and stirring terminal pad are connect, stirring connection main axis is set on the top cover of reaction kettle shell, and stirring terminal pad is set to On stirring connection main shaft and the two is coaxially disposed, and the disk for stirring terminal pad is equipped with blade, diameter of the blade along capstan winch terminal pad It is arranged to activity, stirring motor is variable-frequency motor.
3. band according to claim 2 heats refrigeration synthesis reaction vessel, which is characterized in that connection main shaft is equipped with explosion-proof logical Road.
4. band according to claim 1 heats refrigeration synthesis reaction vessel, which is characterized in that the periphery of dispersion impeller is equipped with Disperse blade, dispersion blade is bending structure, and the bending structure of arbitrary neighborhood two dispersion blades is that bending up and down is set It sets, the edge for dispersing blade is equipped with dispersion sawtooth.
5. band according to claim 1 heats refrigeration synthesis reaction vessel, which is characterized in that dispersion impeller is equipped with axial connection Hole on the upper disk surface of dispersion impeller and is located at the outside of axial connecting hole and is equipped with bulge loop, sets that there are also radial on the upper disk surface of dispersion impeller Diversion trench.
6. band according to claim 1 heats refrigeration synthesis reaction vessel, which is characterized in that be equipped with bayonet type spiral shell at feed inlet The fixed lid of bolt and sealing ring.
7. band according to claim 1 heats refrigeration synthesis reaction vessel, which is characterized in that be connected with flowmeter on return channel And valve control mechanism, discharge port are connected with discharge tube, the side wall of water jacket is equipped with polyimide heat-conducting layer.
CN201820256807.5U 2018-02-13 2018-02-13 Band heating refrigeration synthesis reaction vessel Active CN208098072U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820256807.5U CN208098072U (en) 2018-02-13 2018-02-13 Band heating refrigeration synthesis reaction vessel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820256807.5U CN208098072U (en) 2018-02-13 2018-02-13 Band heating refrigeration synthesis reaction vessel

Publications (1)

Publication Number Publication Date
CN208098072U true CN208098072U (en) 2018-11-16

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820256807.5U Active CN208098072U (en) 2018-02-13 2018-02-13 Band heating refrigeration synthesis reaction vessel

Country Status (1)

Country Link
CN (1) CN208098072U (en)

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