CN106669570B - One kind tiltedly arranging pre-heated chemical reaction kettle - Google Patents

One kind tiltedly arranging pre-heated chemical reaction kettle Download PDF

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Publication number
CN106669570B
CN106669570B CN201611179467.2A CN201611179467A CN106669570B CN 106669570 B CN106669570 B CN 106669570B CN 201611179467 A CN201611179467 A CN 201611179467A CN 106669570 B CN106669570 B CN 106669570B
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circulating pump
water circulating
liquid
reaction tank
water
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CN106669570A (en
Inventor
孟志美
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Jiangsu Taiter New Material Technology Co ltd
Jinan Huijiying New Energy Co ltd
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JIANGSU TETRA NEW MATERIAL TECHNOLOGY Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1868Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1875Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature

Abstract

The present invention provides one kind and tiltedly arranging pre-heated chemical reaction kettle, including reaction tank, filter, stirring rod, water conservancy diversion conehead, paddle, outlet end, liquid feeding end, water circulating pump and heating plate.It is according to the present invention tiltedly to arrange pre-heated chemical reaction kettle, can solution in uniform stirring reaction tank, can fully react, have the advantages that simple in structure, performance is stable and service life is longer.

Description

One kind tiltedly arranging pre-heated chemical reaction kettle
Technical field
The present invention relates to a kind of reaction kettles, particularly relate to one kind and tiltedly arranging pre-heated chemical reaction kettle.
Background technology
Reaction kettle is comprehensive reaction vessel, the design according to reaction condition to reaction kettle structure function and configuration attachment.From Charging-reaction-discharging of beginning can complete pre-set reaction step with higher the degree of automation, to anti- Temperature, pressure, mechanics control during answering(Stirring, air blast etc.), the important parameters such as reactant/product concentration carry out it is stringent Regulation and control.
Reaction kettle is a kind of chemical plant commonly consersion unit, and it is anti-to stir mainly to drive agitating shaft by motor Object is answered so that it is fully reacted to obtain required substance.With the continuous hair of chemical field, life of the people to chemical products The precision of finished product and chemical products all improves higher requirement, and corresponding people are to the important equipment reaction kettle in chemical reaction Higher requirements are also raised.Currently used reaction kettle realizes that long-time constant temperature is kept the temperature by way of heating, for existing After reaction kettle has reacted, reaction kettle also has a larger temperature, present processing mode be essentially all directly be allowed to cool and It is not used, causes the waste of the energy.
Reaction kettle is the reflection container of the mixture function of the heating for realizing technological requirement, evaporation, cooling and low high speed, In, the mixing of solid-liquid material is frequently encountered with the problem of reacting in chemical industry, since solid particle is bigger, it is difficult to it mixes, It affects the efficiency that solid is mixed with liquid and causes to mix uneven.
In the prior art, the aperture segment in tun is in side wall, and during use, a large amount of residuals are arranged at bottom Liquid, because of the problem in design, bottom is difficult to clear up.Its is inconvenient for use, cleaning is inconvenient, and cost of labor is caused to rise.Its Configuration design, wall surface are easy bumps, rupture.
Existing technical literature 1(CN204051670U)Disclose a kind of steam-heated blocked isocyanate adhesive production With reaction kettle, as shown in Fig. 3, heat exchanger(2)It is coiled in steam boiler(5)Exterior side wall on, the heat exchanger(2)'s Cycle water inlet end and recycle water end (W.E.) and water tank(1)It is connected, and heat exchanger(2)It recycles and is equipped on the pipeline of water inlet end Water circulating pump(21).This is a kind of reaction kettle of external water circulating pump, although may be implemented water cycle, its peripheral apparatus compared with More, volume is larger.
Existing technical literature 2(CN204074080U)Disclose a kind of steam-heated blocked isocyanate adhesive production With reaction kettle, as shown in Fig. 4, the autoclave body(1)It is formed with interlayer space(3), the autoclave body(1)Upper and lower part difference It is provided with and interlayer space(3)The steam inlet communicated(4)And steam (vapor) outlet(5);The kettle cover(2)Circulation motor is installed outside (8), the autoclave body(1)Interior bottom is equipped with water circulating pump(9), the circulation motor(8)Output power end is driven by transmission shaft Dynamic water circulating pump(9)Action;The water circulating pump(9)Output end by pipe-support connection be located at autoclave body(1)Internal upper part Jet pipe(10).Although this is a kind of reaction kettle of built-in circulating water pump, its jet pipe(10)The top in space in reaction kettle, The cycle of bottom solution cannot still be played a role well.
In view of this, provide it is a kind of it is simple in structure, facilitate it is durable, especially can be to chemical industry that bottom solution is recycled Reaction kettle necessitates.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, provide that a kind of tiltedly to arrange pre-heated chemical industry anti- Answer kettle, can solution in uniform stirring reaction tank, can fully react, have that simple in structure, performance is stable and uses the longevity Order longer advantage.
To achieve the above object, the present invention provides the following technical solutions:
One kind tiltedly arranges pre-heated chemical reaction kettle, including reaction tank, filter, stirring rod, water conservancy diversion conehead, paddle, goes out Liquid end, liquid feeding end, water circulating pump and heating plate.
Further, reaction tank is columnar structured, and top is equipped with filter, and filter is round sphere structure, There is liquid feeding end, sphere lower part to be penetrated through with reaction tank top structure for its sphere top side.
Further, in the other side of reaction tank bottom, i.e., side opposite with liquid feeding end is provided with outlet end.
Further, top columnar structured described in reaction tank is additionally provided with other than the interface of setting filter Stirring rod.
Further, paddle is provided on the stirring rod, the symmetrical paddle is in fishbone shaped formation, and And relative to stirring rod in certain angle of inclination.
Further, it is equipped with water conservancy diversion conehead in the lower part of stirring rod, the water conservancy diversion conehead is rotary structure, section five Side shape structure, lower end have water conservancy diversion cusp.
Further, the bottom of reaction tank is provided with water circulating pump, the wherein entrance of water circulating pump upward, faces stirring The position of bar lower end.
Further, water circulating pump is two export structures, i.e., is each provided with a water outlet in the both sides of water circulating pump, this Two water outlets are arranged relative to the circular pump housing in symmetrical structure, and export direction is tangential on the circumference of the pump housing.
Further, the bottom of reaction tank is provided with heating plate, the heating plate is arranged in the lower part of water circulating pump;Its In, water circulating pump is set up directly on the middle position in heating plate, and heating plate is only generated heat in water circulating pump outer ring at this time, without Influence water circulating pump.
The present invention also provides a kind of working methods for tiltedly arranging pre-heated chemical reaction kettle, using tiltedly row's pre-heatedization Work reaction kettle, the method includes the steps:
Step 1:Liquid is entered from the liquid feeding end of reaction tank top side in spherical filter;
Step 2:After filter is filtered the liquid of entrance, liquid enters through filter bottom at the top of reaction tank In opening;
Step 3:It into the liquid of reaction tank, is sufficiently stirred by the paddle in fishbone shaped formation, and by leading The guide functions of flow cone head;
Step 4:Bottom liquid sucked by water circulating pump after through water circulating pump both sides two water outlets discharge, again with Liquid after water conservancy diversion conehead, paddle stirring realizes cross-circulation;
Step 5:Meanwhile part not by water circulating pump sucking bottom liquid by reaction tank bottom heating plate plus Heat;
Step 6:Liquid after heating further realizes cross-circulation with the above-mentioned liquid after stirring;
Step 7:The outlet end discharge of the reacted pond other side of liquid after above-mentioned steps are heated and are sufficiently mixed, Completion is stirred to react process.
Description of the drawings
Fig. 1 is the schematic diagram for tiltedly arranging pre-heated chemical reaction kettle of the present invention.
Fig. 2 is the schematic diagram of the water circulating pump of the present invention.
Fig. 3 is the reaction kettle schematic diagram of existing technical literature 1.
Fig. 4 is the reaction kettle schematic diagram of existing technical literature 2.
(Pay attention to:Shown structure in attached drawing simply to illustrate that feature of present invention signal, be not intended to according to attached drawing institute Show structure.
Specific implementation mode
Pre-heated chemical reaction kettle is tiltedly arranged as shown in Figure 1, according to the present invention, including:Reaction tank 1, filter 2, Stirring rod 3, water conservancy diversion conehead 4, paddle 5, outlet end 6, liquid feeding end 7 and water circulating pump 8.
Wherein, reaction tank 1 is columnar structured, and top is equipped with filter 2.Filter 2 is round sphere structure, There is liquid feeding end 7, sphere lower part to be penetrated through with 1 top structure of reaction tank for sphere top side.So, from liquid feeding end 7 into The liquid entered can be fallen into the opening at 1 top of reaction tank with larger area after the filtering of filter 2, be conducive to liquid and fill The cycle divided is broken up.
Further, top columnar structured described in reaction tank 1 is also set up other than the interface of setting filter 2 There is stirring rod 3.
Paddle 5 is provided on the stirring rod 3, the symmetrical paddle 5 is in fishbone shaped formation, and opposite In stirring rod 3 in certain angle of inclination.
It is equipped with water conservancy diversion conehead 4 in the lower part of stirring rod 3, the water conservancy diversion conehead 4 is rotary structure, and section is pentagon knot Structure, lower end has water conservancy diversion cusp, and paddle 5 is 45-60 ° relative to the angle of inclination of stirring rod 3.Water conservancy diversion conehead 4 one Liquid after aspect stirs agitated leaf 5 from top to down carries out water conservancy diversion, on the other hand from top to bottom to rising behind bottom Liquid carry out water conservancy diversion, therefore with two-way guide functions up and down, can realize other blade forms tool than in the prior art There is better mixing effect.
Preferably, the width of paddle 5 is between 1-2cm, most preferably 1.5cm.
Further, the bottom of reaction tank 1 is provided with water circulating pump 8, the wherein entrance of water circulating pump 8 upward, faces The position of 3 lower end of stirring rod.Such mechanism design, enables to filter by filter 2, using water conservancy diversion conehead 4 and stir Mix the inlet that the liquid after leaf 5 stirs drops into water circulating pump 8.
Also, as shown in Fig. 2, water circulating pump 8 is two export structures, i.e., it is each provided with one in the both sides of water circulating pump 8 Water outlet 9, the two water outlets 9 are arranged relative to the circular pump housing in symmetrical structure, and export direction is tangential on the pump housing Circumference.Therefore, recirculated water can be discharged in the two symmetrically arranged water outlets 9 in two directions, so as to realize uniformly Ringing, rather than from top as the prior art, or water cycle is only carried out from a direction.
Preferably, a rotatable chassis is arranged in 8 lower part of water circulating pump, due to two water outlets 9 in two export structures It is arranged in symmetrical structure relative to the circular pump housing, therefore the propulsive thrust of flow can act on the pump housing so that water circulating pump 8 exists It is slowly rotated on chassis, to be more conducive to the outflow of flow in different directions, contributes to the abundant realization of water cycle.
Further, in the other side of 1 bottom of reaction tank, i.e., the side opposite with liquid feeding end 7 is provided with outlet end 6.Cause This, liquid can enter from the side of reaction tank 1, and effect is sufficiently stirred through water conservancy diversion conehead 4 and paddle 5, then from the other side Outlet end 6 flows out.Also, it, can be by the liquid band for being not easy to stir of bottom deposit due to the effect of the water circulating pump of bottom 8 It is dynamic, to realize the staggered form cycle of entire reaction tank 1.
Further, the bottom of reaction tank 1 is provided with heating plate 10, the heating plate 10 is arranged in water circulating pump 8 Lower part.Wherein, water circulating pump 8 is set up directly on the middle position in heating plate 10, and heating plate 10 is only outside water circulating pump 8 at this time Circle fever, without influencing whether water circulating pump 8.When water circulating pump 8 has rotatable chassis, then chassis, which is similarly disposed at, adds Middle position on hot plate 10, heating plate 10 is only in the fever of 8 chassis outer ring of water circulating pump at this time, without influencing whether water circulating pump 8 chassis.
As a result, when heating plate 10 heats, since the liquid in reaction tank 1 is all in the superjacent air space of heating plate, and Rise according to the liquid after heating, the principle that not heated liquid declines, it is easy to which the liquid in entire reaction tank 1 is carried out Adequately heating.Also, since water circulating pump 8 is arranged in the top of heating plate 10, secondly export structure, it can be in both direction Upper discharge recirculated water, so as to realize uniform ringing.
Above description tiltedly arranges pre-heatedization tiltedly to arrange pre-heated chemical reaction kettle according to of the present invention based on above-mentioned Work reaction kettle, workflow are:
Step 1:Liquid is entered from the liquid feeding end 7 of 1 top side of reaction tank in spherical filter 2;
Step 2:After filter 2 is filtered the liquid of entrance, liquid enters 1 top of reaction tank through 2 bottom of filter Opening in;
Step 3:Into the liquid of reaction tank 1, it is sufficiently stirred by the paddle 5 in fishbone shaped formation, and pass through The guide functions of water conservancy diversion conehead 4;
Step 4:Two water outlets 9 through 8 both sides of water circulating pump are discharged after bottom liquid is sucked by water circulating pump 8, again Liquid after being stirred with water conservancy diversion conehead 4, paddle 5 realizes cross-circulation;
Step 5:Meanwhile the bottom liquid partly not sucked by water circulating pump 8 is by the heating plate 10 of 1 bottom of reaction tank Heating;
Step 6:Liquid after heating further realizes cross-circulation with the above-mentioned liquid after stirring;
Step 7:6 row of outlet end of reacted 1 other side of pond of liquid after above-mentioned steps are heated and are sufficiently mixed Go out, completion is stirred to react process.
It is according to the present invention tiltedly to arrange pre-heated chemical reaction kettle and have the characteristics that:
(1)Liquid mode is entered using top, and liquid can be broken up after filtering, is tentatively mixed;
(2)Paddle 5 is in fishbone shaped formation, using oblique row's mode, can realize sufficient stirring action;
(3)The water circulating pump 2 of bottom setting can stir bottom liquid, realize and recycle with water conservancy diversion conehead 4, paddle 5, Water conservancy diversion conehead 4 has bidirectional guide effect;
(4)Water circulating pump 8 is two export structures, and recirculated water can be discharged in two directions, so as to realize uniformly Ringing.
(5)Liquid reaches behind reaction tank 1 bottom by heating, realizes that secondary cross-circulation is made with aforesaid liquid when rising With heating and mixed effect are more preferable.
The foregoing is only a preferred embodiment of the present invention, is not intended to limit the scope of the present invention, it is all All any modification, equivalent and improvement made by within the spirit and principles in the present invention etc. should be included in the protection of the present invention Within the scope of.

Claims (5)

1. one kind tiltedly arranging pre-heated chemical reaction kettle, including:Reaction tank(1), filter(2), stirring rod(3), water conservancy diversion conehead (4), paddle(5), outlet end(6), liquid feeding end(7), water circulating pump(8)And heating plate(10);
It is characterized in that:
Reaction tank(1)To be columnar structured, top is equipped with filter(2), filter(2)For round sphere structure, ball Body top side has liquid feeding end(7), sphere lower part and reaction tank(1)Top structure penetrates through;
In reaction tank(1)The other side of bottom, i.e., and liquid feeding end(7)Opposite side is provided with outlet end(6);
In reaction tank(1)The columnar structured top is in addition to being arranged filter(2)Interface outside, be additionally provided with stirring rod (3);
The stirring rod(3)On be provided with paddle(5), the paddle(5)Symmetrical is in fishbone shaped formation, and phase For stirring rod(3)In certain angle of inclination;
In stirring rod(3)Lower part be equipped with water conservancy diversion conehead(4), the water conservancy diversion conehead(4)For rotary structure, section is pentagon Structure, lower end have water conservancy diversion cusp;
In reaction tank(1)Bottom be provided with water circulating pump(8), wherein water circulating pump(8)Entrance upward, face stirring rod (3)The position of lower end;
Water circulating pump(8)For two export structures, i.e., in water circulating pump(8)Both sides be each provided with a water outlet(9), the two Water outlet(9)It is arranged in symmetrical structure relative to the circular pump housing, and export direction is tangential on the circumference of the pump housing;
In reaction tank(1)Bottom be provided with heating plate(10), the heating plate(10)It is arranged in water circulating pump(8)Lower part; Wherein, water circulating pump(8)It is set up directly on heating plate(10)On middle position, heating plate at this time(10)Only in water circulating pump (8)Outer ring generates heat, without influencing whether water circulating pump(8).
2. according to claim 1 tiltedly arrange pre-heated chemical reaction kettle, it is characterised in that:
Paddle(5)Width be 1-2cm.
3. according to claim 2 tiltedly arrange pre-heated chemical reaction kettle, it is characterised in that:
Paddle(5)Relative to stirring rod(3)Angle of inclination be 45-60 °.
4. according to claim 3 tiltedly arrange pre-heated chemical reaction kettle, it is characterised in that:
Water circulating pump(8)A rotatable chassis is arranged in lower part;
Work as water circulating pump(8)When with rotatable chassis, then chassis is similarly disposed at heating plate(10)On middle position, this When heating plate(10)Only in water circulating pump(8)Chassis outer ring generates heat, without influencing whether water circulating pump(8)Chassis.
5. a kind of working method for tiltedly arranging pre-heated chemical reaction kettle tiltedly arranges preheating using claim 1-4 any one of them Formula chemical reaction kettle, which is characterized in that the method includes the steps:
Step 1:Liquid is from reaction tank(1)The liquid feeding end of top side(7)Enter spherical filter(2)In;
Step 2:Filter(2)After being filtered to the liquid of entrance, liquid is through filter(2)Bottom enters reaction tank(1)Top In the opening in portion;
Step 3:Into reaction tank(1)Liquid, by the paddle in fishbone shaped formation(5)Be sufficiently stirred, and pass through Water conservancy diversion conehead(4)Guide functions;
Step 4:Bottom liquid is by water circulating pump(8)Through water circulating pump after sucking(8)Two water outlets of both sides(9)Discharge, then Secondary and water conservancy diversion conehead(4), paddle(5)Liquid after stirring realizes cross-circulation;
Step 5:Meanwhile part is not by water circulating pump(8)The bottom liquid of sucking is by reaction tank(1)The heating plate of bottom (10)Heating;
Step 6:Liquid after heating further realizes cross-circulation with the above-mentioned liquid after stirring;
Step 7:The reacted pond of liquid after above-mentioned steps are heated and are sufficiently mixed(1)The outlet end of the other side(6)Row Go out, completion is stirred to react process.
CN201611179467.2A 2016-12-19 2016-12-19 One kind tiltedly arranging pre-heated chemical reaction kettle Active CN106669570B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109908852A (en) * 2019-01-29 2019-06-21 泰兴金燕化学科技有限公司 A kind of staggered form circulation stirring chemical reaction kettle
CN111187605B (en) * 2020-02-11 2021-01-15 海兴县新源化工有限公司 Petroleum resistance-reducing viscosity reducer for low-temperature cold transportation pipeline, preparation device and preparation method

Citations (3)

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Publication number Priority date Publication date Assignee Title
WO2002024317A1 (en) * 2000-09-22 2002-03-28 Iso-Mix A/S A method and a process plant for treating a batch of liquids
CN203944376U (en) * 2014-06-10 2014-11-19 赣县鑫亿化工有限公司 A kind of highly effective reaction still with filter
CN204602046U (en) * 2015-01-29 2015-09-02 江苏华光新材料科技有限公司 The equal mixing device of powdery paints production raw material

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Publication number Priority date Publication date Assignee Title
JPH02173666A (en) * 1988-12-26 1990-07-05 Sharp Corp Manufacture of spherical particles for toner

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002024317A1 (en) * 2000-09-22 2002-03-28 Iso-Mix A/S A method and a process plant for treating a batch of liquids
CN203944376U (en) * 2014-06-10 2014-11-19 赣县鑫亿化工有限公司 A kind of highly effective reaction still with filter
CN204602046U (en) * 2015-01-29 2015-09-02 江苏华光新材料科技有限公司 The equal mixing device of powdery paints production raw material

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