CN106345383A - Circulating reactor - Google Patents

Circulating reactor Download PDF

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Publication number
CN106345383A
CN106345383A CN201611016981.4A CN201611016981A CN106345383A CN 106345383 A CN106345383 A CN 106345383A CN 201611016981 A CN201611016981 A CN 201611016981A CN 106345383 A CN106345383 A CN 106345383A
Authority
CN
China
Prior art keywords
kettle
spring
shaft
pipeline
semiaxis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611016981.4A
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Chinese (zh)
Inventor
王超群
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangxi University
Original Assignee
Guangxi University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangxi University filed Critical Guangxi University
Priority to CN201611016981.4A priority Critical patent/CN106345383A/en
Publication of CN106345383A publication Critical patent/CN106345383A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1868Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a circulating reactor, comprising a reactor body, a motor, stirring blades, a shaft barrel, a circulating discharge port, a raw material feed pipeline, an in-reactor feed pipeline, an in-reactor discharge pipeline and a finished product outlet pipeline, wherein the motor is fixedly arranged in the middle of the top of the reactor body and drives a stirring device, and the stirring device comprises a stirring shaft and the stirring blades; the stirring shaft comprises an upper half shaft and a lower half shaft, and the outer side of the upper half shaft is coaxially sleeved with the shaft barrel; a spring is arranged in the shaft barrel, and the upper end of the lower half shaft is inserted into an inner barrel of the spring; the spring is fixedly clamped inside the shaft barrel, and the lower end of the spring is connected with the upper end of the lower half shaft; a silica gel layer for closing the spring is filled in the shaft barrel, and reinforcing ribs are arranged above the shaft barrel and are fixedly welded to the side wall of the upper half shaft; two groups of stirring blades are arranged at the bottom of the lower half shaft, and a circulating discharge port is arranged at the bottom of the reactor body. The circulating reactor provided by the invention has the advantages of ensuring the uniform mixing of raw materials, improving the reaction rate and effects, and effectively ensuring product quality.

Description

A kind of circular response kettle
Technical field
The present invention relates to reactor, specifically a kind of circular response kettle.
Background technology
During work produces, the mixing of too busy to get away raw material and synthesis, the mode feeding intake in the mixing of raw material and building-up process and In reaction unit, the impact to production efficiency, production cost, product quality for the mixing uniformity of raw material is most important.
Reactor is a kind of conventional chemical industry equipment, is generally added into multiple industrial chemicals in reactor, and allows this There is chemical reaction in multiple industrial chemicals in reactor, and then obtain required product;In industrial chemicals course of reaction In, in order to contact the purposes such as abundant, quickening balancing response heat, there iing viscosity big, during the chemical reagent such as magnetic solution, generally Using mechanical stirring device, and the conventional stirring paddle of agitating device is very inconvenient with motor connection, simultaneously altitude mixture control also ten Divide trouble.
Content of the invention
It is an object of the invention to provide a kind of ensure raw material mix homogeneously, improve reaction rate and effect, effectively guarantee The circular response kettle of product quality, to solve the problems, such as to propose in above-mentioned background technology.
For achieving the above object, the following technical scheme of present invention offer:
A kind of circular response kettle, including charging in kettle, motor, stirring paddle, beam barrel, circulation discharging opening, feedstock pipeline, kettle Discharge pipe and product outlet pipeline in pipeline, kettle;Motor is fixedly installed, Motor drive is stirred at described kettle crown center position Mix device, wherein, agitating device includes shaft and stirring paddle, shaft includes semiaxis and lower semiaxis;Outside described upper semiaxis Side is coaxially socketed setting beam barrel, is provided with spring inside beam barrel, and wherein, lower semiaxis upper end is inserted in the inner core of spring, and spring is fixed It is connected in inside beam barrel, lower spring end connects the upper end of lower semiaxis, is filled with the layer of silica gel for closing spring inside beam barrel;Institute State setting reinforcement above beam barrel, reinforcement is fixed with upper semiaxis sidewall weld;Described lower semiaxis bottom arranges two groups of stirring paddles; Described autoclave body bottom is provided with circulation discharging opening, and circulation discharging opening connects discharge pipe in kettle, and in kettle, discharge pipe is also simultaneously connected with Feedstock pipeline and water pump;It is provided with recycle feed mouth, recycle feed mouth and feed pipe in kettle on described kettle top One end connects, and in kettle, the other end of feed pipe connects the outlet of water pump, and is connected with filter on feed pipe in kettle;Described Filter is connected with feed pipe in kettle by filter inlet pipeline, and the bottom of filter is provided with product outlet pipeline;Described It is equipped with list on discharge pipe, product outlet pipeline and filter inlet pipeline in feed pipe in feedstock pipeline, kettle, kettle To valve;In feed pipe in described kettle, kettle, kettle, discharge pipe constitutes blood circulation.
Further: described kettle includes upper kettle and lower kettle, and upper kettle, lower kettle mutually fasten, and by hinge Chain is connected, and is provided with sealing ring between upper kettle, lower kettle.
Further: described motor is frequency conversion motor.
Compared with prior art, the invention has the beneficial effects as follows:
In the present invention, material enters inside kettle, and motor drives the rotation of upper half axle, and upper semiaxis drives beam barrel rotation, and beam barrel passes through Spring drives lower half axle to rotate, and so that stirring paddle is worked, and stirring paddle drives raw material mix homogeneously;When the rotating speed of motor reduces When, the power crispaturaed that spring is subject to can diminish, thus the length elongation of spring, drives lower semiaxis and stirring paddle to move downward;With Reason, when faster rotational speed, stirring paddle moves upwards, and moving up and down of stirring paddle, raw material not only can be stirred in horizontal level, And can stir in upper and lower position so that mixing more uniform, effectively raise reaction rate and effect so that reacting More thorough;
In the present invention, in feedstock pipeline, water pump and kettle feed pipe by feedstock transportation to kettle, by agitating device to former Material is stirred mixing, and during hybrid reaction, is driven by water pump;
In the present invention, blood circulation is driven by water pump, carries out the circulation of storeroom in raw material and kettle Outer Tube in kettle in production process Mixing, not only low cost, efficiency high, and achieve the circulation mixing of raw material turnover, make raw material can mix homogeneously effectively, solution Raw material of having determined mixing is uneven, the remaining impact problem to product quality of feed conduit, improves product quality;During discharging, finished product By discharge pipe, water pump, filter in kettle by product outlet pipeline discharging, finished product be filtered after from product outlet pipe Road flow out, the setting of filter, product quality has been carried out secondary check on, effectively guarantee product quality.
Brief description
Fig. 1 is the structural representation of circular response kettle.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation description is it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of not making creative work Embodiment, broadly falls into the scope of protection of the invention.
Refer to Fig. 1, in the embodiment of the present invention, a kind of circular response kettle, including kettle 1, motor 4, stirring paddle 7, beam barrel 18th, circulation discharging opening 10, feedstock pipeline 11, feed pipe 12 in kettle, discharge pipe 13 and product outlet pipeline 14 in kettle; Described kettle 1 includes upper kettle and lower kettle, and upper kettle, lower kettle mutually fasten, and by hinge be connected, upper kettle, under It is provided with sealing ring between kettle;Motor 4 is fixedly installed, motor 4 is frequency conversion motor, electricity at described kettle 1 crown center position Machine 4 drives agitating device, and wherein, agitating device includes shaft and stirring paddle 7, and shaft includes semiaxis 5 and lower semiaxis 6; Described upper semiaxis 5 outside is coaxial to be socketed setting beam barrel 18, is provided with spring 20, wherein, bullet is inserted in lower semiaxis 6 upper end inside beam barrel 18 In the inner core of spring 20, spring 20 fixation is connected in inside beam barrel 18, and spring 20 lower end connects the upper end of lower semiaxis 6, in beam barrel 18 Portion is filled with the layer of silica gel 19 for closing spring;Described beam barrel 18 top setting reinforcement 17, reinforcement 17 and upper semiaxis 5 side Wall is welded and fixed;Described lower semiaxis 6 bottom arranges two groups of stirring paddles 7;In work, material enters inside kettle 1, and motor 4 drives Upper semiaxis 5 rotates, and upper semiaxis 5 drives beam barrel 18 to rotate, and beam barrel 18 passes through spring 20 and drives lower semiaxis 6 to rotate, and finally makes to stir Mix oar 7 to work, stirring paddle 7 drives raw material mix homogeneously;When the rotating speed of motor 4 reduces, the power meeting that what spring 20 was subject to crispatura Diminish, thus the length elongation of spring 20, drive lower semiaxis 6 and stirring paddle 7 to move downward;In the same manner, when faster rotational speed, stirring Oar 7 moves upwards, and moving up and down of stirring paddle 7, raw material not only can be stirred in horizontal level, and can be in upper and lower position Put and stir so that mixing more uniform, effectively raise reaction rate and effect so that reaction is more thorough;Described kettle 1 Bottom is provided with circulation discharging opening 10, and circulation discharging opening 10 connects discharge pipe 13 in kettle, and in kettle, discharge pipe 13 is also simultaneously connected with Feedstock pipeline 11 and water pump 2;It is provided with recycle feed mouth 9, recycle feed mouth 9 and charging in kettle on described kettle 1 top One end of pipeline 12 connects, and in kettle, the other end of feed pipe 12 connects the outlet of water pump 2, and connects on feed pipe 12 in kettle There is filter 3;Described filter 3 is connected with feed pipe in kettle 12 by filter inlet pipeline 15, and the bottom of filter 3 sets There is product outlet pipeline 14;Discharge pipe 13, product outlet pipe in feed pipe 12 in described feedstock pipeline 11, kettle, kettle It is equipped with check valve 16 on road 14 and filter inlet pipeline 15;In work, charging in feedstock pipeline 11, water pump 2 and kettle Pipeline 12, by feedstock transportation to kettle 1, is stirred to raw material mixing by agitating device 2, during hybrid reaction, by water pump 2 drives;In feed pipe 12 in described kettle 1, kettle, kettle, discharge pipe 13 constitutes blood circulation, and blood circulation is carried by water pump 2 Dynamic, carry out raw material in kettle in production process and mix with the circulation of storeroom in kettle Outer Tube, not only low cost, efficiency high, and Achieve the circulation mixing of raw material turnover, make raw material can mix homogeneously effectively, solve that raw material mixing is uneven, feed conduit is residual The remaining impact problem to product quality, improves product quality;During discharging, finished product passes through discharge pipe 13, water pump 2, mistake in kettle By product outlet pipeline 14 discharging, finished product flows out after filter 3 filtration filter 3 from product outlet pipeline 14, the setting of filter 3 Put, product quality has been carried out secondary check on, effectively guarantee product quality.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie In the case of the spirit or essential attributes of the present invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling Change is included in the present invention.Any reference in claim should not be considered as limiting involved claim.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment only wraps Containing an independent technical scheme, only for clarity, those skilled in the art should for this narrating mode of description Using description as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined Understandable other embodiment.

Claims (3)

1. a kind of circular response kettle, including kettle (1), motor (4), stirring paddle (7), beam barrel (18), circulation discharging opening (10), former Expect discharge pipe (13) and product outlet pipeline (14) in feed pipe (12) in feed pipe (11), kettle, kettle;Its feature exists In motor (4) being fixedly installed at described kettle (1) crown center position, motor (4) drives agitating device, wherein, agitating device Including shaft and stirring paddle (7), shaft includes semiaxis (5) and lower semiaxis (6);Coaxial sleeve outside described upper semiaxis (5) Connect and be provided with spring (20) inside setting beam barrel (18), beam barrel (18), wherein, the inner core of spring (20) is inserted in lower semiaxis (6) upper end In, spring (20) fixation is connected in beam barrel (18) inside, and spring (20) lower end connects the upper end of lower semiaxis (6), in beam barrel (18) Portion is filled with the layer of silica gel (19) for closing spring;Above described beam barrel (18) setting reinforcement (17), reinforcement (17) with Upper semiaxis (5) sidewall weld is fixed;Described lower semiaxis (6) bottom arranges two groups of stirring paddles (7);Described kettle (1) bottom is provided with Circulation discharging opening (10), circulation discharging opening (10) connects discharge pipe (13) in kettle, and in kettle, discharge pipe (13) is also simultaneously connected with Feedstock pipeline (11) and water pump (2);It is provided with recycle feed mouth (9), recycle feed mouth (9) on described kettle (1) top It is connected with one end of feed pipe in kettle (12), in kettle, the other end of feed pipe (12) connects the outlet of water pump (2), and in kettle Filter (3) is connected with feed pipe (12);Described filter (3) passes through filter inlet pipeline (15) and feed pipe in kettle Road (12) connects, and the bottom of filter (3) is provided with product outlet pipeline (14);Charging in described feedstock pipeline (11), kettle It is equipped with check valve on discharge pipe (13), product outlet pipeline (14) and filter inlet pipeline (15) in pipeline (12), kettle (16);In feed pipe (12) in described kettle (1), kettle, kettle, discharge pipe (13) constitutes blood circulation.
2. circular response kettle according to claim 1 is it is characterised in that described kettle (1) includes upper kettle and lower kettle, And upper kettle, lower kettle mutually fasten, and it is connected by hinge, between upper kettle, lower kettle, be provided with sealing ring.
3. circular response kettle according to claim 1 is it is characterised in that described motor (4) is frequency conversion motor.
CN201611016981.4A 2016-11-18 2016-11-18 Circulating reactor Pending CN106345383A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611016981.4A CN106345383A (en) 2016-11-18 2016-11-18 Circulating reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611016981.4A CN106345383A (en) 2016-11-18 2016-11-18 Circulating reactor

Publications (1)

Publication Number Publication Date
CN106345383A true CN106345383A (en) 2017-01-25

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611016981.4A Pending CN106345383A (en) 2016-11-18 2016-11-18 Circulating reactor

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107774219A (en) * 2017-11-17 2018-03-09 安徽赛立科硅材料有限公司 A kind of surface modification device of superfine powder
CN111171425A (en) * 2019-12-31 2020-05-19 江苏百兴管业科技有限公司 High-temperature-resistant environment-friendly plastic particle and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204485861U (en) * 2015-03-18 2015-07-22 夏争先 A kind of circulating resin reaction kettle
CN205517733U (en) * 2016-03-12 2016-08-31 宁波大学 Biological medicine preparation has multifunctional reaction kettle
CN205550262U (en) * 2016-01-31 2016-09-07 林紫晴 Multifunctional reaction kettle for chemical production
CN205613416U (en) * 2016-05-03 2016-10-05 黄翀 Chemical production is with high -efficient safe reation kettle

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204485861U (en) * 2015-03-18 2015-07-22 夏争先 A kind of circulating resin reaction kettle
CN205550262U (en) * 2016-01-31 2016-09-07 林紫晴 Multifunctional reaction kettle for chemical production
CN205517733U (en) * 2016-03-12 2016-08-31 宁波大学 Biological medicine preparation has multifunctional reaction kettle
CN205613416U (en) * 2016-05-03 2016-10-05 黄翀 Chemical production is with high -efficient safe reation kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107774219A (en) * 2017-11-17 2018-03-09 安徽赛立科硅材料有限公司 A kind of surface modification device of superfine powder
CN111171425A (en) * 2019-12-31 2020-05-19 江苏百兴管业科技有限公司 High-temperature-resistant environment-friendly plastic particle and preparation method thereof

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Application publication date: 20170125