CN109908852A - A kind of staggered form circulation stirring chemical reaction kettle - Google Patents

A kind of staggered form circulation stirring chemical reaction kettle Download PDF

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Publication number
CN109908852A
CN109908852A CN201910085730.9A CN201910085730A CN109908852A CN 109908852 A CN109908852 A CN 109908852A CN 201910085730 A CN201910085730 A CN 201910085730A CN 109908852 A CN109908852 A CN 109908852A
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China
Prior art keywords
paddle
liquid
circulating pump
reaction tank
water circulating
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Pending
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CN201910085730.9A
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Chinese (zh)
Inventor
孙骁
王尚林
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Taixing Jin Yan Chemical Technology Co Ltd
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Taixing Jin Yan Chemical Technology Co Ltd
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Priority to CN201910085730.9A priority Critical patent/CN109908852A/en
Publication of CN109908852A publication Critical patent/CN109908852A/en
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Abstract

The present invention provides a kind of staggered form circulation stirring chemical reaction kettle, including reaction tank, filter, stirring rod, the first paddle, the second paddle, outlet end, liquid feeding end and water circulating pump.Staggered form circulation stirring chemical reaction kettle according to the present invention, can solution in uniform stirring reaction tank, can sufficiently react, have the advantages that structure is simple, performance is stable and service life is longer.

Description

A kind of staggered form circulation stirring chemical reaction kettle
Technical field
The present invention relates to a kind of reaction kettles, particularly relate to a kind of staggered form circulation stirring chemical reaction kettle.
Background technique
Reaction kettle is comprehensive reaction vessel, the design according to reaction condition to reaction kettle structure function and configuration attachment.From Charging-reaction-discharging of beginning can complete pre-set reaction step with higher the degree of automation, to anti- The important parameters such as temperature, pressure, mechanics control (stirring, air blast etc.), reactant/product concentration during answering carry out stringent Regulation.
Reaction kettle is a kind of chemical plant commonly consersion unit, and it is anti-to stir mainly to drive agitating shaft by motor Object is answered to react it sufficiently to obtain required substance.With the continuous hair of chemical field, life of the people to chemical products The precision of finished product and chemical products all improves higher requirement, and corresponding people are to the important equipment reaction kettle in chemical reaction Higher requirements are also raised.Currently used reaction kettle realizes that long-time constant temperature is kept the temperature by way of heating, for existing After reaction kettle has reacted, reaction kettle also has a biggish temperature, present processing mode be essentially all directly be allowed to cool and It is not used, causes the waste of the energy.
Reaction kettle is the reflection container of the mixed function of heating, evaporation, cooling and the low high speed of realizing that technique requires, In, the mixing of solid-liquid material frequently encounters in chemical industry with the problem of reacting, since solid particle is bigger, it is difficult to it mixes, It affects the efficiency that solid is mixed with liquid and causes mixing uneven.
In the prior art, the aperture segment in large container is in side wall, and during use, a large amount of residuals are arranged at bottom Liquid, because of the problem in design, bottom is difficult to clear up.Its is inconvenient for use, cleaning is inconvenient, and cost of labor is caused to rise.Its Configuration design, wall surface are easy bumps, rupture.
Existing technical literature 1(CN204051670U) disclose a kind of steam-heated blocked isocyanate adhesive production With reaction kettle, as shown in Fig. 3, heat exchanger (2) is coiled in the exterior side wall of steam boiler (5), the heat exchanger (2) It recycles water inlet end and recycles water end (W.E.) and be connected with water tank (1), and be equipped on the pipeline of heat exchanger (2) circulation water inlet end Water circulating pump (21).This is a kind of reaction kettle of external water circulating pump, although may be implemented water circulation, its peripheral apparatus compared with More, volume is larger.
Existing technical literature 2(CN204074080U) disclose a kind of steam-heated blocked isocyanate adhesive production With reaction kettle, as shown in Fig. 4, the autoclave body (1) is formed with interlayer space (3), the upper and lower part difference of the autoclave body (1) It is provided with the steam inlet (4) and steam (vapor) outlet (5) communicated with interlayer space (3);Circulation motor is installed outside the kettle cover (2) (8), the interior bottom of the autoclave body (1) is equipped with water circulating pump (9), and circulation motor (8) output power end is driven by transmission shaft Dynamic water circulating pump (9) movement;The output end of the water circulating pump (9) is located at autoclave body (1) internal upper part by pipe-support connection Jet pipe (10).Although this is a kind of reaction kettle of built-in circulating water pump, its jet pipe (10) is located at the top in space in reaction kettle, The circulation of bottom solution cannot still be played a role well.
In view of this, providing, a kind of structure is simple, it is durable to facilitate, especially can be to the chemical industry that bottom solution is recycled Reaction kettle necessitates.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, a kind of staggered form circulation stirring is provided Work reaction kettle, can solution in uniform stirring reaction tank, can sufficiently react, have that structure is simple, performance is stable and makes The advantages of with lasting a long time.
To achieve the above object, the invention provides the following technical scheme:
A kind of staggered form circulation stirring chemical reaction kettle, including reaction tank, filter, stirring rod, the first paddle, the second stirring Leaf, outlet end, liquid feeding end and water circulating pump.
Further, reaction tank is columnar structured, and top is equipped with filter, and filter is round sphere structure, Its sphere top side has liquid feeding end, and sphere lower part and reaction tank top structure penetrate through.
Further, in the other side of reaction bottom of pond portion, i.e. the side opposite with liquid feeding end is provided with outlet end.
Further, top columnar structured described in the reaction tank is additionally provided with other than the interface of setting filter Stirring rod.
Further, the first paddle and the second paddle are provided on the stirring rod, the first paddle and second stir It mixes between leaf in V shape structure.
Further, the bottom of reaction tank is provided with water circulating pump, wherein the entrance of water circulating pump upward, faces stirring The position of bar lower end.
Further, water circulating pump is two export structures, i.e., is each provided with a water outlet in the two sides of water circulating pump, this Two water outlets are relative to the circular pump housing at symmetrical structure setting, and export direction is tangential on the circumference of the pump housing.
Further, a rotatable chassis is arranged in water circulating pump lower part.
The present invention also provides a kind of working methods of staggered form circulation stirring chemical reaction kettle, follow using the staggered form Ring stirs chemical reaction kettle, the method includes the steps:
Step 1: liquid is entered from the outlet end of 1 top side of reaction tank in spherical filter;
Step 2: after filter is filtered the liquid of entrance, liquid enters the opening at the top of reaction tank through filter bottom In;
Step 3: into the liquid of reaction tank, by two in V shape structure the first paddle and the second paddle it is abundant Stirring;
Step 4: two water outlets discharge through water circulating pump two sides after bottom liquid is sucked by water circulating pump, again with first Liquid after paddle and the stirring of the second paddle realizes cross-circulation;
Step 5: stirring is completed in the outlet end discharge of the reacted bottom of pond portion other side of liquid after above-mentioned steps are sufficiently mixed Reaction process.
Detailed description of the invention
Fig. 1 is the schematic diagram of staggered form circulation stirring chemical reaction kettle of the invention.
Fig. 2 is the schematic diagram of water circulating pump of the invention.
Fig. 3 is the reaction kettle schematic diagram of existing technical literature 1.
Fig. 4 is the reaction kettle schematic diagram of existing technical literature 2.
(note: shown structure in attached drawing simply to illustrate that feature of present invention signal, be not intended to according to attached drawing institute Show structure.
Specific embodiment
As shown in Figure 1, staggered form circulation stirring chemical reaction kettle according to the present invention, comprising: reaction tank 1, filtering Device 2, stirring rod 3, the first paddle 4, the second paddle 5, outlet end 6, liquid feeding end 7 and water circulating pump 8.
Wherein, reaction tank 1 is columnar structured, and top is equipped with filter 2.Filter 2 is round sphere structure, Sphere top side has liquid feeding end 7, and sphere lower part and 1 top structure of reaction tank penetrate through.So, from liquid feeding end 7 into The liquid entered can be fallen into the opening at 1 top of reaction tank with biggish area after the filtering of filter 2, be conducive to liquid and fill The circulation divided is broken up.
Further, top columnar structured described in the reaction tank 1 is also set up other than the interface of setting filter 2 There is stirring rod 3.
The first paddle 4 and the second paddle 5, the first paddle 4 and the second paddle 5 are provided on the stirring rod 3 Between be in V shape structure.Above structure allows the liquid fallen into from top columnar structured described in reaction tank more equal Even is acted on by the first paddle 4 and the second paddle 5, and V shape is formed between the first paddle 4 and the second paddle 5 Structure can be realized other better mixing effects of blade form than in the prior art.
Preferably, the width most preferably 1.5cm of the first paddle 4 and the second paddle 5.
Preferably, the angle of the V shape structure between the first paddle 4 and the second paddle 5 is 30-45 °.
Further, the bottom of reaction tank 1 is provided with water circulating pump 8, wherein the entrance of water circulating pump 8 upward, faces The position of 3 lower end of stirring rod.Such mechanism design, enables to filter by filter 2, using 4 He of the first paddle Liquid after the stirring of second paddle 5 drops into the inlet of water circulating pump 8.
Also, as shown in Fig. 2, water circulating pump 8 is two export structures, i.e., one is each provided in the two sides of water circulating pump 8 Water outlet 9, the two water outlets 9 are relative to the circular pump housing at symmetrical structure setting, and export direction is tangential on the pump housing Circumference.Therefore, recirculated water can be discharged in the two symmetrically arranged water outlets 9 in two directions, so as to realize uniformly Ringing, rather than from top as the prior art, or water circulation is only carried out from a direction.
Preferably, a rotatable chassis is arranged in 8 lower part of water circulating pump, due to two water outlets 9 in two export structures Relative to the circular pump housing at symmetrical structure setting, therefore the propulsive thrust of water flow can act on the pump housing, so that water circulating pump 8 exists It is slowly rotated on chassis, to be more conducive to the outflow of water flow in different directions, facilitates the abundant realization of water circulation.
Further, in the other side of 1 bottom of reaction tank, i.e., the side opposite with liquid feeding end 7 is provided with outlet end 6.Cause This, liquid can enter from the side of reaction tank 1, be sufficiently stirred effect through the first paddle 4 and the second paddle 5, then from another The outlet end 6 of side flows out.Also, it, can be by the liquid for being not easy to stir of bottom deposit due to the effect of the water circulating pump of bottom 8 Body drives, to realize the staggered form circulation of entire reaction tank 1.
Above description, to be followed based on above-mentioned staggered form according to staggered form circulation stirring chemical reaction kettle of the present invention Ring stirs chemical reaction kettle, workflow are as follows:
Step 1: liquid is entered from the outlet end 6 of 1 top side of reaction tank in spherical filter 2;
Step 2: after the liquid of 2 pairs of filter entrance is filtered, liquid enters opening for 1 top of reaction tank through 2 bottom of filter In mouthful;
Step 3: being in the first paddle 4 and the second paddle 5 of V shape structure by two into the liquid of reaction tank 1 It is sufficiently stirred;
Step 4: two water outlets 9 through 8 two sides of water circulating pump are discharged after bottom liquid is sucked by water circulating pump 8, again with the Liquid after one paddle 4 and the stirring of the second paddle 5 realizes cross-circulation;
Step 5: the outlet end 6 of the reacted 1 bottom other side of pond of liquid after above-mentioned steps are sufficiently mixed is discharged, and completes to stir Mix reaction process.
Staggered form circulation stirring chemical reaction kettle according to the present invention has the following characteristics that
(1) it uses top to enter liquid mode, and liquid can be broken up after filtering, tentatively mixed;
It is in V shape structure between (2) first paddles 4 and the second paddle 5, can be realized sufficient stirring action;
(3) water circulating pump 2 of bottom setting can stir bottom liquid, follow again with the first paddle 4 and the realization of the second paddle 5 Ring;
(4) water circulating pump 8 is two export structures, and recirculated water can be discharged in two directions, uniformly follow so as to realize Ring effect.
The foregoing is only a preferred embodiment of the present invention, is not intended to limit the scope of the present invention, it is all Made any modifications, equivalent replacements, and improvements etc. within the spirit and principles in the present invention, should be included in protection of the invention Within the scope of.

Claims (4)

1. a kind of staggered form circulation stirring chemical reaction kettle, comprising: reaction tank (1), filter (2), stirring rod (3), first stir Mix leaf (4), the second paddle (5), outlet end (6), liquid feeding end (7) and water circulating pump (8);
It is characterized by:
Reaction tank (1) be it is columnar structured, top is equipped with filter (2), and filter (2) is round sphere structure, ball Body top side has liquid feeding end (7), and sphere lower part and reaction tank (1) top structure penetrate through;
In the other side of reaction tank (1) bottom, i.e. the side opposite with liquid feeding end (7) is provided with outlet end (6);
At reaction tank (1) the columnar structured top other than the interface of setting filter (2), it is additionally provided with stirring rod (3);
The first paddle (4) and the second paddle (5), the first paddle (4) and the second stirring are provided on the stirring rod (3) It is in V shape structure between leaf (5);
The bottom of reaction tank (1) is provided with water circulating pump (8), wherein the entrance of water circulating pump (8) upward, faces stirring rod (3) position of lower end;
Water circulating pump (8) is two export structures, i.e., is each provided with a water outlet (9) in the two sides of water circulating pump (8), the two Water outlet (9) is relative to the circular pump housing at symmetrical structure setting, and export direction is tangential on the circumference of the pump housing;
A rotatable chassis is arranged in water circulating pump (8) lower part.
2. staggered form circulation stirring chemical reaction kettle according to claim 1, it is characterised in that:
The width of first paddle (4) and the second paddle (5) is 1.5cm.
3. staggered form circulation stirring chemical reaction kettle according to claim 2, it is characterised in that:
The angle of V shape structure between first paddle (4) and the second paddle (5) is 30-45 °.
4. a kind of working method of staggered form circulation stirring chemical reaction kettle, using the described in any item intersections of claim 1-3 Formula circulation stirring chemical reaction kettle, which is characterized in that the method includes the steps:
Step 1: liquid is entered from the outlet end (6) of reaction tank (1) top side in spherical filter (2);
Step 2: after filter (2) is filtered the liquid of entrance, liquid enters reaction tank (1) through filter (2) bottom and pushes up In the opening in portion;
Step 3: entering the liquid of reaction tank (1), is in the first paddle (4) and the second paddle of V shape structure by two (5) be sufficiently stirred;
Step 4: two water outlets (9) through water circulating pump (8) two sides are discharged after bottom liquid is sucked by water circulating pump (8), then The secondary liquid with behind the first paddle (4) and the second paddle (5) stirring realizes cross-circulation;
Step 5: outlet end (6) discharge of the reacted pond of liquid (1) bottom other side after above-mentioned steps are sufficiently mixed, it is complete At being stirred to react process.
CN201910085730.9A 2019-01-29 2019-01-29 A kind of staggered form circulation stirring chemical reaction kettle Pending CN109908852A (en)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910085730.9A CN109908852A (en) 2019-01-29 2019-01-29 A kind of staggered form circulation stirring chemical reaction kettle

Publications (1)

Publication Number Publication Date
CN109908852A true CN109908852A (en) 2019-06-21

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106582483A (en) * 2016-12-19 2017-04-26 朱小莉 Fan-shaped preheating type stirring chemical engineering reaction still
CN106582484A (en) * 2016-12-19 2017-04-26 李华 Cycle stirring type chemical reaction still
CN106669571A (en) * 2016-12-19 2017-05-17 孟志美 Inclined discharging type stirring chemical reaction kettle
CN106669569A (en) * 2016-12-19 2017-05-17 李华 Cross preheating type stirring chemical reaction kettle
CN106669570A (en) * 2016-12-19 2017-05-17 孟志美 Preheating type chemical reaction vessel with inclined arrangement
CN107051353A (en) * 2016-12-19 2017-08-18 朱小莉 A kind of fan-shaped cycling stirring type chemical reaction kettle
FR3047996A1 (en) * 2016-02-19 2017-08-25 Rampal Patou USE OF A REACTOR IN A SOAP MANUFACTURING PROCESS AND REACTOR SPECIALLY ADAPTED FOR SUCH USE

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3047996A1 (en) * 2016-02-19 2017-08-25 Rampal Patou USE OF A REACTOR IN A SOAP MANUFACTURING PROCESS AND REACTOR SPECIALLY ADAPTED FOR SUCH USE
CN106582483A (en) * 2016-12-19 2017-04-26 朱小莉 Fan-shaped preheating type stirring chemical engineering reaction still
CN106582484A (en) * 2016-12-19 2017-04-26 李华 Cycle stirring type chemical reaction still
CN106669571A (en) * 2016-12-19 2017-05-17 孟志美 Inclined discharging type stirring chemical reaction kettle
CN106669569A (en) * 2016-12-19 2017-05-17 李华 Cross preheating type stirring chemical reaction kettle
CN106669570A (en) * 2016-12-19 2017-05-17 孟志美 Preheating type chemical reaction vessel with inclined arrangement
CN107051353A (en) * 2016-12-19 2017-08-18 朱小莉 A kind of fan-shaped cycling stirring type chemical reaction kettle

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Application publication date: 20190621

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