CN207950744U - It is a kind of efficiently to extract organic component device in glycerine - Google Patents
It is a kind of efficiently to extract organic component device in glycerine Download PDFInfo
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- CN207950744U CN207950744U CN201721907756.XU CN201721907756U CN207950744U CN 207950744 U CN207950744 U CN 207950744U CN 201721907756 U CN201721907756 U CN 201721907756U CN 207950744 U CN207950744 U CN 207950744U
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- extractant
- storage tank
- glycerine
- valve
- extraction
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Abstract
The utility model is related to organic component devices in a kind of efficiently extraction glycerine, including extraction container, glycerol mixture storage tank, extractant storage tank, glycerine storage tank, organic matter storage tank and extractant destilling tower, glycerol mixture storage tank connects extraction container top by glycerol mixture valve, extractant storage tank connects extraction container top by extractant feed valve, extraction container bottom is connected to by the first glycerine recovery valve with glycerine storage tank, extraction container is connected to extractant destilling tower by extract liquor transfer line, extractant destilling tower is connect by organic matter valve with organic matter storage tank, extractant storage tank is connected to by extractant valve at the top of extractant destilling tower.The utility model has the beneficial effects that：Remaining high added value organic components in glycerine can rapidly, efficiently and thoroughly be separated by this extraction equipment；Using cone separator, can it is rapid, easily upper layer of extraction liquid a small amount of in extraction container and lower layer's glycerin layer are directly separated completely, improve sample utilisation, avoid wasting, greatly raising separative efficiency and usability.
Description
Technical field
The utility model belongs to chemical apparatus field, is filled more particularly, to organic component in a kind of efficiently extraction glycerine
It sets.
Background technology
The method at present industrially detaching glycerine with aliphatic ester type organic will typically be added glycerine and mix
Object, allows light specific gravity aliphatic ester after standing, flows from above, and glycerine sinks to bottom.Since organic matter can have one in glycerine
Fixed dissolubility, and its solubility becomes higher with organic matter physical property and operating condition sometimes, thus can
Cause larger loss, especially when these organic matters have compared with high added value when, this method is not just suitable for.
Invention content
In order to solve the above technical problems, the utility model, which provides one kind, efficiently extracting organic component device in glycerine.
The technical solution adopted in the utility model is：It is a kind of efficiently to extract organic component device in glycerine, including extraction appearance
Device, glycerol mixture storage tank, extractant storage tank, glycerine storage tank, organic matter storage tank and extractant destilling tower, glycerol mixture storage
Tank connects extraction container top by glycerol mixture valve, and extractant storage tank is connected by extractant feed valve on extraction container
Portion, extraction container bottom are connected to by the first glycerine recovery valve with glycerine storage tank, and extraction container is connected by extract liquor transfer line
Logical extractant destilling tower, extractant destilling tower are connect by organic matter valve with organic matter storage tank, and extractant distills tower top
Portion is connected to extractant storage tank by extractant valve.
Preferably, extract liquor transfer line includes suction pipe, liquid pump and cone separator, and suction pipe probes into the liquid of extraction container
In tolerant in vivo, suction pipe is connected to cone separator by liquid pump, and cone separator, which passes through to distill valve and connect extractant, to be steamed
Tower is evaporated, cone separator is connected to by the second glycerine recovery valve with glycerine storage tank.
Preferably, pipette tip is connected with floating ball.
Preferably, extract liquor valve is equipped between liquid pump and cone separator.
Preferably, visor window is equipped between liquid pump and cone separator.
Preferably, blender is equipped in extraction container.
The utility model has the advantages and positive effects of：It can be attached by remaining height in glycerine by this extraction equipment
Value added organic components (glycerin weight 3-10%) are rapid, separate efficiently and thoroughly；Utilize cone separator, Ke Yixun
Upper layer of extraction liquid a small amount of in extraction container and lower layer's glycerin layer are easily directly separated by speed completely, can thoroughly will rapidly
The organic matter of high added value is detached from glycerine, is improved sample utilisation, is avoided wasting；Gradation extraction and separation, can be additional by height
Value organic matter is kept completely separate out；It is detached by taper grader, during large dosage of glycerine can be avoided to convey, due to glycerine viscosity
It is high, than great, and caused by the problem of being difficult to convey and be easy to remain；
The present apparatus uses the extractant of polarity very little that two-phase liquid is made to become to be easy to be layered, it will be able to greatly shorten
Quiescent time, and so that the range of applicable temperature expands, (solidification point of pure high added value organic matter is higher, the low item of temperature
Under part, it is easy solidification), greatly improve separative efficiency and usability.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model one embodiment.
In figure：
1, extraction container 11, blender 12, suction pipe
13, floating ball 14, liquid pump 21, extract liquor valve
22, valve 23, extractant valve 24, organic matter valve are distilled
25, the second glycerine recovery valve 26, the first glycerine recovery valve 27, extractant feed valve
28, glycerol mixture valve 3, visor window 4, cone separator
5, extractant destilling tower 6, organic matter storage tank 7, glycerine storage tank
8, extractant storage tank 9, glycerol mixture storage tank
Specific implementation mode
It explains below in conjunction with the accompanying drawings to one embodiment of the utility model.
As shown in Figure 1, organic component device in a kind of efficiently extraction glycerine, including extraction container 1, glycerol mixture storage tank
9, extractant storage tank 8, glycerine storage tank 7, organic matter storage tank 6 and extractant destilling tower 5；Glycerol mixture storage tank 9 is for storing
Glycerol mixture raw material, glycerol mixture storage tank 9 connect 1 top of extraction container by glycerol mixture valve 28, mixed by glycerine
The control for closing object valve 28 transmits glycerol mixture into extraction container 1；Extractant storage tank 8 is for storing extract liquor, extractant storage
Tank 8 connects 1 top of extraction container by extractant feed valve 27, and extractant is held by the control of extractant feed valve 27 to extraction
It is conveyed in device 1；Blender 11, glycerol mixture and extractant are equipped in extraction container 1 in extraction container 1 in blender 11
It is mixed well under effect, the organic component in glycerine is extracted into extractant, glycerine is separated, due to glycerine and extraction
The density of agent, glycerine exist with lower liquid, and after mixing is stood, extractant can float on upper layer, can be transmitted by extract liquor
Line, which enters, carries out distillation separation in extractant destilling tower 5.
Extract liquor transfer line includes suction pipe 12, liquid pump 14 and cone separator 4, and 12 end of suction pipe is connected with floating ball
13, floating ball 13 can float on extractant, ensure that the liquid substance drawn is the supernatant liquid after layering, suction pipe 12 probes into extraction
In the liquid contents of container 1, suction pipe 12 is connected to cone separator 4 by liquid pump 14, under the action of extract liquor valve 21
First volume extract liquor is transported to cone separator 4, visor window 3 is additionally provided between liquid pump 14 and cone separator 4, is passed for observing
Transfusion fluid state should carry out subsequent processing for extract liquor in if limpid if liquid if liquid muddiness is mixed liquor.
Extraction liquids can be detached further in cone separator 4, is increased extraction and separation precision, is also avoided advising greatly
Mould remains caused by transmitting glycerine；Cone separator 4 connects extractant destilling tower 5 by distilling valve 22, opens distillation valve 22,
Extract liquor is transferred to extractant destilling tower 5, carries out the separation of extractant, by distillation, extractant is arranged at the top of destilling tower
Go out, is transmitted back in extractant storage tank 8 by extractant valve 23, applies again；The mailing component extracted left is by having
Machine object valve 24 enters organic matter storage tank 6.The bottom of extraction container 1 and cone separator 4 passes through the first glycerine recovery valve 26 respectively
Enter glycerine storage tank 7 with the second glycerine recovery valve 25, to complete the mesh for separating the organic component in glycerol mixture
's.
The operating procedure of the present apparatus is as follows：
The first step：In the state that all valves are all in closing, glycerine mixed liquor and extractant are proportionally added into extraction
Extracting container, stirring with extractant until fully carry out hybrid extraction, and then the gradual mixing speed that reduces at leisure is until stirring
Mix stopping, static a period of time (5-30 minutes)；
Second step：It puts down with floating ball-and suction pipe can be moved up and down, open extract liquor valve, later on valve liquid pump will
Clear extract liquor passes through visor window on upper layer, pumps in cone separator, opens distillation valve, allows clear extract flow
Enter in extractant destilling tower；Once there is muddy object to pass through visor, distillation valve should be closed immediately, pay attention to observing and adjusted with floating
Extract liquor is extracted clean and carries glycerine as little as possible, makes these a small amount of by ball-and the height that can move up and down suction pipe as possible
Mixture in cone separator it is static for a moment, open valve 2 first the glycerine of lower layer is put into glycerin storage tank, then close
Valve closing door 2 is again turned on distillation valve, and the extract liquor on upper layer is put into destilling tower；Extract carrying out second to the glycerine being extracted
When taking, first a certain amount of extractant is added in extraction container, is detached according to above-mentioned same process.
Third walks：Extract liquor in a distillation column is distilled, the extractant distilled out is sent back to extractant holding vessel,
The organic matter of high added value is placed into organic matter holding vessel.
One embodiment of the utility model is described in detail above, but the content is only the utility model
Preferred embodiment should not be considered as limiting the scope of the present invention.It is all to be made according to application scope of the utility model
All the changes and improvements etc., should all still belong within the patent covering scope of the utility model.
Claims (6)
1. organic component device in a kind of efficiently extraction glycerine, it is characterised in that：Including extraction container, glycerol mixture storage tank,
Extractant storage tank, glycerine storage tank, organic matter storage tank and extractant destilling tower, the glycerol mixture storage tank are mixed by glycerine
Object valve connects the extraction container top, and the extractant storage tank connects the extraction container top by extractant feed valve,
The extraction container bottom is connected to by the first glycerine recovery valve with the glycerine storage tank, and the extraction container is passed by extract liquor
Defeated pipeline is connected to the extractant destilling tower, and the extractant destilling tower is connected by organic matter valve and the organic matter storage tank
It connects, the extractant storage tank is connected to by extractant valve at the top of the extractant destilling tower.
2. organic component device in efficient extraction glycerine according to claim 1, it is characterised in that：The extract liquor transmission
Pipeline includes suction pipe, liquid pump and cone separator, and the suction pipe probes into the liquid contents of extraction container, and the suction pipe is logical
It crosses the liquid pump and is connected to the cone separator, the cone separator connects the extractant distillation by distilling valve
Tower, the cone separator are connected to by the second glycerine recovery valve with the glycerine storage tank.
3. organic component device in efficient extraction glycerine according to claim 2, it is characterised in that：The pipette tip connects
It is connected to floating ball.
4. organic component device in efficient extraction glycerine according to claim 2 or 3, it is characterised in that：The liquid pump
Extract liquor valve is equipped between the cone separator.
5. organic component device in efficient extraction glycerine according to claim 2 or 3, it is characterised in that：The liquid pump
Visor window is equipped between the cone separator.
6. organic component device in efficient extraction glycerine according to claim 2, it is characterised in that：In the extraction container
Equipped with blender.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721907756.XU CN207950744U (en) | 2017-12-30 | 2017-12-30 | It is a kind of efficiently to extract organic component device in glycerine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721907756.XU CN207950744U (en) | 2017-12-30 | 2017-12-30 | It is a kind of efficiently to extract organic component device in glycerine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207950744U true CN207950744U (en) | 2018-10-12 |
Family
ID=63731069
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721907756.XU Expired - Fee Related CN207950744U (en) | 2017-12-30 | 2017-12-30 | It is a kind of efficiently to extract organic component device in glycerine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207950744U (en) |
-
2017
- 2017-12-30 CN CN201721907756.XU patent/CN207950744U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wei Wenhao Inventor after: Li Guanjun Inventor after: Li Yunwei Inventor before: Wei Yunhao Inventor before: Li Guanjun Inventor before: Li Yunwei |
|
| CB03 | Change of inventor or designer information | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181012 Termination date: 20201230 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |