CN209221549U - Anti-aging agent crystallization apparatus - Google Patents

Anti-aging agent crystallization apparatus Download PDF

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Publication number
CN209221549U
CN209221549U CN201821933057.7U CN201821933057U CN209221549U CN 209221549 U CN209221549 U CN 209221549U CN 201821933057 U CN201821933057 U CN 201821933057U CN 209221549 U CN209221549 U CN 209221549U
Authority
CN
China
Prior art keywords
aging agent
fuel sucking
pipe
sucking pipe
crystallization apparatus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821933057.7U
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Chinese (zh)
Inventor
许其民
胥成功
陈恒
杨亚平
张艳兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yichang Xingchun Chemical Co Ltd
Original Assignee
Yichang Xingchun Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yichang Xingchun Chemical Co Ltd filed Critical Yichang Xingchun Chemical Co Ltd
Priority to CN201821933057.7U priority Critical patent/CN209221549U/en
Application granted granted Critical
Publication of CN209221549U publication Critical patent/CN209221549U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

Anti-aging agent crystallization apparatus, including crystallizing tank and alembic, further include pot for storing up liquid, and crystallizing tank is respectively communicated with alembic and pot for storing up liquid by two groups of oil slick adsorbent equipments;Oil slick adsorbent equipment includes fuel sucking pipe and bracket, and multiple floating balls are connected on bracket, and fuel sucking pipe lower end is rack-mount, and fuel sucking pipe upper end is equipped with water pump by hose and inlet tube on inlet tube.The utility model can accurately separate fuel-displaced phase and emulsion layer from crystallizing tank.

Description

Anti-aging agent crystallization apparatus
Technical field
The utility model relates to anti-aging agent crystallization apparatus.
Background technique
Anti-aging agent water crystallization is to put into anti-aging agent mother liquor and soft water in crystallizing tank, stands and divides after heating stirring Layer, upper layer are oily phase, and lower layer is the water phase containing anti-aging agent crystalline particle, there is Emulsion Phase between upper layer and lower layer;Upper oil phase It can recycle by alembic active principle extracted and utilize again, lower layer's water phase is made dry anti-after being centrifuged, filtering Old agent;And extract upper oil phase and drawn generally by pipeline, oil is mutually mixed into crystalline particle water phase in order to prevent, and pipeline is logical Can often sub-fraction water phase be drawn more, this will allow oily phase, Emulsion Phase and sub-fraction water phase to be inhaled into alembic together, It will definitely increase distillation burden, and also improve distillation impurity level.
Utility model content
The technical problem to be solved by the present invention is to provide anti-aging agent crystallization apparatus, can accurately divide from crystallizing tank Separate out oily phase and emulsion layer.
To solve the above-mentioned problems, technical solution to be solved in the utility model are as follows: anti-aging agent crystallization apparatus, including crystallization Tank and alembic, further include pot for storing up liquid, and crystallizing tank is respectively communicated with alembic and pot for storing up liquid by two groups of oil slick adsorbent equipments;Oil slick Adsorbent equipment includes fuel sucking pipe and bracket, multiple floating balls is connected on bracket, fuel sucking pipe lower end is rack-mount, fuel sucking pipe Upper end is equipped with water pump by hose and inlet tube on inlet tube.
The floating ball includes hollow ball, is communicated with the first feed pipe in sphere upper end, is equipped on the first feed pipe Sealing cover.
Transparent glass tube is installed on inlet tube.
Tubaeform oil suction bucket is communicated in fuel sucking pipe lower end.
Hood-opening device is equipped at the top of crystallizing tank, the hood-opening device includes the opening being arranged at the top of crystallizing tank, is being opened It is equipped with end cap in mouthful, pipe sleeve is fixedly connected in the middle part of end cap, the fuel sucking pipe is located in pipe sleeve, and oil slick adsorbent equipment can be from It is passed through in opening.
The technical effect of the utility model are as follows: can be fast and accurately in crystallizing tank using two groups of oil slick adsorbent equipments It is oily to be mutually drawn into alembic and pot for storing up liquid respectively with Emulsion Phase, it realizes the accurate extraction to oily phase, keeps oil mutually and water phase is pure Only, mitigate alembic and distill burden;On the other hand, it avoids water phase from entering alembic to be volatilized, reduces impurity level.
Detailed description of the invention
The utility model is described further with reference to the accompanying drawing:
Fig. 1 is the schematic view of the front view of the utility model,
Fig. 2 is the schematic diagram of the section structure of the utility model about oil slick adsorbent equipment.
In figure: crystallizing tank 1, alembic 2, pot for storing up liquid 3, oil slick adsorbent equipment 4, hood-opening device 5, glass tube 6, drainage conduit 11, bracket 41, fuel sucking pipe 42, sphere 43, hose 44, oil suction bucket 45, the first feed pipe 46, sealing cover 47, inlet tube 48, water pump 49, end cap 51, pipe sleeve 52.
Specific embodiment
As illustrated in fig. 1 and 2, anti-aging agent crystallization apparatus, including crystallizing tank 1 and alembic 2,1 bottom of crystallizing tank are connected to discharge Pipe, further includes pot for storing up liquid 3, and crystallizing tank 1 is respectively communicated with alembic 2 and pot for storing up liquid 3 by two groups of oil slick adsorbent equipments 4;Oil slick is inhaled Adsorption device 4 includes fuel sucking pipe 42 and bracket 41, multiple floating balls is connected on bracket 41,42 lower end of fuel sucking pipe is mounted on bracket 41 On, 42 upper end of fuel sucking pipe is equipped with water pump 49 by hose 44 and inlet tube 48 on inlet tube 48;Two groups of oil slick adsorbent equipments Two inlet tubes 48 are respectively communicated with 2 inlet of 3 inlet of pot for storing up liquid and alembic in 4.
Anti-aging agent water crystallization is to put into anti-aging agent mother liquor and soft water in crystallizing tank 1, after heating, stirring and standing Layering, upper layer are oily phase, and lower layer is the water phase containing anti-aging agent crystalline particle, there is Emulsion Phase between upper layer and lower layer;Upper layer oil It can mutually recycle by the active principle extracted of alembic 2 and utilize again, drying is made after being centrifuged, filtering in lower layer's water phase Anti-aging agent.
The application method of the utility model are as follows: each floating buoyancy or adjustment oil suction in two groups of oil slick adsorbent equipments 4 of setting The height of 42 lower end nozzle of pipe makes the 42 lower end nozzle of fuel sucking pipe being connected in two groups of oil slick adsorbent equipments 4 with pot for storing up liquid 3 be located at cream Change the faying face of phase with aqueous layer, the 42 lower end nozzle of fuel sucking pipe that transference alembic 2 is connected to is located at the combination of oil phase and Emulsion Phase The water pump 49 being connected in oil slick adsorbent equipment 4 with alembic 2 is then first opened in face, and upper upper oil phase, which is sent in alembic 2, to be extracted It takes;The water pump 49 being connected in oil slick adsorbent equipment 4 with pot for storing up liquid 3 is then opened, emulsion is drawn into pot for storing up liquid 3 and is kept in, Pot for storing up liquid 3 is then sent to treatment center of sewage after being filled with;The water phase remained in crystallizing tank 1 then enters junior's processing unit In.
The floating ball includes hollow ball 43, the first feed pipe 46 is communicated in 43 upper end of sphere, in the first feed pipe 46 On sealing cover 47 is installed.This structure, which can be convenient, is adjusted the buoyancy of oil slick adsorbent equipment 4, method of adjustment are as follows: A certain amount of solution to be separated can be taken out in crystallizing tank 1 into laboratory, then successively put two groups of oil slick adsorbent equipments 4 Enter into solution, Buoyance adjustment liquid is then poured into sphere 43 by the first feed pipe 46, due to pouring into for Buoyance adjustment liquid, The position of fuel sucking pipe 42 also and then changes, and 42 lower end nozzle of fuel sucking pipe is allowed to be located on designated position, then will using sealing cover 47 The closing of first feed pipe 46.Wherein Buoyance adjustment liquid can be the liquid such as water or silicone oil.
Transparent glass tube 6 is installed on inlet tube 48.During 49 drawing liquid of water pump, when worker observes glass tube There is no liquid then to represent oily phase or Emulsion Phase when perhaps only a small amount of liquid passes through by pumping light, to facilitate worker to observe knot in 6 Drawing liquid situation in brilliant tank 1.
Tubaeform oil suction bucket 45 is communicated in 42 lower end of fuel sucking pipe.Make the mutually direction-free inflow oil suction bucket 45 of oil, reaches To it is more convenient, quickly remove oil slick.
Hood-opening device 5 is equipped at the top of crystallizing tank 1, the hood-opening device 5 includes the opening that 1 top of crystallizing tank is arranged in, It is equipped with end cap 51 in opening, pipe sleeve 52 is fixedly connected in the middle part of end cap 51, the fuel sucking pipe 42 is located in pipe sleeve 52, oil slick Adsorbent equipment 4 can be passed through from opening.This structure can be convenient oil slick adsorbent equipment 4 taken out from crystallizing tank 1 or It is put into, in order to repair to oil slick adsorbent equipment 4 and be adjusted to its buoyancy.

Claims (5)

1. anti-aging agent crystallization apparatus, including crystallizing tank (1) and alembic (2), it is characterised in that: it further include pot for storing up liquid (3), crystallization Tank (1) is respectively communicated with alembic (2) and pot for storing up liquid (3) by two groups of oil slick adsorbent equipments (4);Oil slick adsorbent equipment (4) includes Fuel sucking pipe (42) and bracket (41), are connected with multiple floating balls on bracket (41), and fuel sucking pipe (42) lower end is mounted on bracket (41) On, fuel sucking pipe (42) upper end is equipped with water pump (49) by hose (44) and inlet tube (48) on inlet tube (48).
2. anti-aging agent crystallization apparatus according to claim 1, it is characterised in that: the floating ball includes hollow ball (43), The first feed pipe (46) are communicated in sphere (43) upper end, sealing cover (47) are installed on the first feed pipe (46).
3. anti-aging agent crystallization apparatus according to claim 1, it is characterised in that: be equipped with transparent glass on inlet tube (48) Glass pipe (6).
4. anti-aging agent crystallization apparatus according to claim 1, it is characterised in that: be communicated with loudspeaker in fuel sucking pipe (42) lower end The oil suction bucket (45) of shape.
5. anti-aging agent crystallization apparatus according to claim 1, it is characterised in that: be equipped with dress of uncapping at the top of crystallizing tank (1) It sets (5), the hood-opening device (5) includes the opening being arranged at the top of crystallizing tank (1), is equipped with end cap (51) in opening, is holding It is fixedly connected with pipe sleeve (52) in the middle part of lid (51), it is interior that the fuel sucking pipe (42) is located at pipe sleeve (52), and oil slick adsorbent equipment (4) can be with It is passed through from opening.
CN201821933057.7U 2018-11-22 2018-11-22 Anti-aging agent crystallization apparatus Expired - Fee Related CN209221549U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821933057.7U CN209221549U (en) 2018-11-22 2018-11-22 Anti-aging agent crystallization apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821933057.7U CN209221549U (en) 2018-11-22 2018-11-22 Anti-aging agent crystallization apparatus

Publications (1)

Publication Number Publication Date
CN209221549U true CN209221549U (en) 2019-08-09

Family

ID=67504041

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821933057.7U Expired - Fee Related CN209221549U (en) 2018-11-22 2018-11-22 Anti-aging agent crystallization apparatus

Country Status (1)

Country Link
CN (1) CN209221549U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113476897A (en) * 2021-07-21 2021-10-08 三马紧固件(浙江)股份有限公司 Oil-water separation device
CN114669093A (en) * 2022-02-25 2022-06-28 安徽东至广信农化有限公司 Material separation device for reduction synthesis of o-phenylenediamine

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113476897A (en) * 2021-07-21 2021-10-08 三马紧固件(浙江)股份有限公司 Oil-water separation device
CN114669093A (en) * 2022-02-25 2022-06-28 安徽东至广信农化有限公司 Material separation device for reduction synthesis of o-phenylenediamine
CN114669093B (en) * 2022-02-25 2023-11-07 安徽东至广信农化有限公司 Material separation device for reduction synthesis of o-phenylenediamine

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190809

Termination date: 20201122