CN207805614U - A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system - Google Patents
A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system Download PDFInfo
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- CN207805614U CN207805614U CN201721874388.3U CN201721874388U CN207805614U CN 207805614 U CN207805614 U CN 207805614U CN 201721874388 U CN201721874388 U CN 201721874388U CN 207805614 U CN207805614 U CN 207805614U
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- support plate
- rotation seat
- hydrothermal synthesis
- synthesis device
- stirs
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Abstract
The utility model provides a kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system, belongs to hydrothermal synthesis device field.It includes magnetic stirring apparatus, heater box and reaction kettle；Heater box is mounted on magnetic stirring apparatus；Supporting mechanism, including the first support plate, the first connecting pole, the first rotation seat, driver, the second support plate, the second connecting pole and the second rotation seat are equipped in babinet；First rotation seat is mounted on the bottom of babinet, and the first support plate is connect by the first connecting pole with the first rotation seat, and the rotation of the first rotation seat is driven by driver；Second rotation seat is mounted on the bottom of babinet, and the second support plate is connect by the second connecting pole with the second rotation seat, and the second support plate is engaged with the first support plate；Offer multiple first mounting holes and multiple second mounting holes in first support plate, the second support plate respectively, multiple reaction kettles are separately positioned on multiple first mounting holes, on multiple second mounting holes.The reaction system can obtain the mixed liquor that mixing is more uniformly distributed.
Description
Technical field
The utility model is related to multifunctional magnetic-force stirring hydrothermal synthesis device fields, in particular to a kind of multi-function magnetic
Power stirs hydrothermal synthesis device and reaction system.
Background technology
Hydrothermal synthesis reaction kettle is the common small sized reactor of chemical laboratory, can be used for low dose of synthetic reaction；May be used also
Using strong acid in tank body or highly basic and high temperature high pressure enclosed environment achievees the purpose that rapid-digestion indissoluble substance.
Hydrothermal synthesis reaction kettle is a kind of closed container that can decompose indissoluble substance.Can be used for atomic absorption spectrum and wait from
Molten sample pretreatment in the analyses such as son transmitting；It can also be used for low dose of synthetic reaction；Also using strong acid in tank body or highly basic
And high temperature high pressure enclosed environment achievees the purpose that rapid-digestion indissoluble substance.Gas phase, liquid phase, plasma spectrum mass spectrum,
Sample pre-treatments are done in the chemical analysis methods such as Atomic absorption and atomic fluorescence.It is to be cleared up when measuring trace element and trace element
The competent assistant of sample.
Hydrothermal synthesis reaction kettle can be applied in the determining heavy metals such as lead, copper, cadmium, zinc, calcium, manganese, iron, mercury, be alternatively arranged as
A kind of reaction vessel that high-temperature-resistant high-pressure-resistant anti-corrosion is high-purity and organic synthesis, hydrothermal synthesis, crystal growth or Specimen eliminating extraction
Take etc..Residual heavy metal, agriculture, food, mud, rare earth, aquatic products, organic matter etc. are cleared up in sample pre-treatments.Therefore, in stone
The research and life of the departments such as oiling work, biomedicine, material science, geologic chemistry, environmental science, Food Science, commodity inspection
It is widely used in production.
In the prior art, traditional hydrothermal synthesis reaction kettle structure design is more unreasonable, can not be effectively to reaction
Mixed liquor is stirred in kettle.
Utility model content
The utility model provides a kind of multifunctional magnetic-force stirring hydrothermal synthesis device, it is intended to solve multi-functional in the prior art
The above problem existing for magnetic agitation hydrothermal synthesis device.
What the utility model embodiment was realized in：
A kind of multifunctional magnetic-force stirring hydrothermal synthesis device, the multifunctional magnetic-force stirring hydrothermal synthesis device includes magnetic agitation
Device, heater box and multiple reaction kettles；
The heater box is mounted on the magnetic stirring apparatus；
The heater box has columned babinet, is provided with supporting mechanism in the babinet, the supporting mechanism includes
First support plate, the first connecting pole, the first rotation seat, driver, the second support plate, the second connecting pole and the second rotation seat；
First rotation seat is installed in rotation on the bottom of the babinet, first support plate by first connecting pole with
The first rotation seat connection, the driver are mounted on the box house, and described first turn is driven by the driver
Dynamic seat rotation；Second rotation seat is installed in rotation on the bottom of the babinet, and second support plate passes through described
Two connecting poles are connect with second rotation seat, and second support plate is engaged with first support plate；
Multiple first mounting holes and multiple second installations are offered in first support plate, second support plate respectively
Hole, multiple reaction kettles are separately positioned on multiple first mounting holes, on multiple second mounting holes.
As a kind of optimal technical scheme of the utility model, multiple first mounting holes are circumferential and open evenly and at intervals
It is located in first support plate.
As a kind of optimal technical scheme of the utility model, multiple second mounting holes are circumferential and open evenly and at intervals
It is located in second support plate.
As a kind of optimal technical scheme of the utility model, the bottom of the babinet offers first positioning hole, described
There is the first groove, first rotation seat to be in the form of a column structure on the inner wall of first positioning hole, first rotation seat with it is described
First groove is equipped with, and first rotation seat can rotate in first groove.
As a kind of optimal technical scheme of the utility model, the bottom of the babinet offers second location hole, described
There is the second groove, second rotation seat to be in the form of a column structure on the inner wall of second location hole, second rotation seat with it is described
Second groove is equipped with, and second rotation seat can rotate in second groove.
As a kind of optimal technical scheme of the utility model, the reaction kettle includes autoclave body and lid, the autoclave body tool
There is columned inner cavity, the cover cap is on the autoclave body.
As a kind of optimal technical scheme of the utility model, the outside spacers of the lid it is provided with multiple pressure reducing valves
And two handles of the setting at interval, described two handles are oppositely arranged.
As a kind of optimal technical scheme of the utility model, pressure gauge is provided on the lid.
As a kind of optimal technical scheme of the utility model, multiple first are provided on the outside of first support plate
Sawtooth, is provided with multiple second sawtooth on the outside of second support plate, first support plate by first sawtooth,
Second sawtooth is engaged with second support plate.
A kind of reaction system, the reaction system include above-described multifunctional magnetic-force stirring hydrothermal synthesis device.
The utility model has the beneficial effects that：
The utility model stirs hydrothermal synthesis device by the multifunctional magnetic-force that above-mentioned design obtains, with magnetic agitation
Device, heater box and multiple reaction kettles；Wherein, due to being provided with supporting mechanism in the babinet of heater box, supporting mechanism has the
One support plate and the second support plate offer multiple first mounting holes and multiple respectively in the first support plate and the second support plate
Therefore second mounting hole can place multiple reaction kettles simultaneously thereon, can when starting heater and magnetic stirring apparatus
Mixing is stirred to the solution in multiple reaction kettles simultaneously so that solution mixing therein is more uniformly distributed fully, and is carried
The mixing efficiency of high solution.Simultaneously as being respectively arranged with the first sawtooth and the second saw in the first support plate and the second support plate
Tooth, therefore, the two can drive the first support plate opposite case by the first sawtooth and the second engagement when starting driver
When rotation, the rotation of the second support plate can be driven by the meshing relation of the two, heater can be from all angles pair as a result,
Multiple reaction kettles are carried out while being heated so that and the characteristics of homogeneity is presented in the heating degree of reaction kettle, so that its inside
Solution can be mixed more uniformly.It follows that stirring hydrothermal synthesis device by this multifunctional magnetic-force, can make
Mixed liquor is sufficiently mixed in reaction kettle, obtains the mixed liquor being more uniformly distributed.
The reaction system that the utility model is obtained by above-mentioned design, the reaction system is due to above-mentioned multi-function magnetic
Therefore power stirring hydrothermal synthesis device can be such that mixed liquor in reaction kettle is sufficiently mixed, obtain the mixed liquor being more uniformly distributed.
Description of the drawings
It, below will be to required in embodiment in order to illustrate more clearly of the technical solution of the utility model embodiment
The attached drawing used is briefly described, it should be understood that the following drawings illustrates only some embodiments of the utility model, therefore not
The restriction to range is should be considered as, for those of ordinary skill in the art, without creative efforts,
It can also be obtained according to these attached drawings other relevant attached drawings.
Fig. 1 is the structural schematic diagram for the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides；
Fig. 2 is that the structure of reaction kettle in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides is shown
It is intended to；
Fig. 3 is the knot of the first support plate in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides
Structure schematic diagram；
Fig. 4 is the knot of the second support plate in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides
Structure schematic diagram；
Fig. 5 is the first support plate and the in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides
Two support plate fit structure schematic diagrames；
Fig. 6 is first positioning hole and the in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides
One groove structure schematic diagram；
Fig. 7 is first positioning hole and the in the multifunctional magnetic-force stirring hydrothermal synthesis device that the utility model embodiment provides
One groove structure schematic diagram.
Icon：1- multifunctional magnetic-forces stir hydrothermal synthesis device；2- magnetic stirring apparatus；3- heater boxes；4- reaction kettles；5- is supported
Mechanism；The first support plates of 6-；The first connecting poles of 7-；The first rotation seats of 8-；9- drivers；The second support plates of 10-；11- second connects
Connect column；The second rotation seats of 12-；The first mounting holes of 13-；The second mounting holes of 14-；15- first positioning holes；The first grooves of 16-；17-
Second location hole；The second grooves of 18-；19- autoclave bodies；20- lids；The first sawtooth of 25-；The second sawtooth of 26-.
Specific implementation mode
To keep the purpose, technical scheme and advantage of the utility model embodiment clearer, below in conjunction with this practicality
The technical solution in the utility model embodiment is clearly and completely described in attached drawing in novel embodiment, shows
So, described embodiment is a part of embodiment of the utility model, rather than whole embodiments.Based on this practicality
Embodiment in novel, those of ordinary skill in the art are obtained every other without creative efforts
Embodiment shall fall within the protection scope of the present invention.Therefore, the implementation to the utility model provided in the accompanying drawings below
The detailed description of mode is not intended to limit claimed the scope of the utility model, but is merely representative of the utility model
Selected embodiment.
In the description of the present invention, it should be understood that the term of indicating position or position relationship is based on attached drawing
Shown in orientation or positional relationship, be merely for convenience of describing the present invention and simplifying the description, rather than indicate or imply institute
The element of finger must have a particular orientation, with specific azimuth configuration and operation, therefore should not be understood as to the utility model
Limitation.
In the present invention unless specifically defined or limited otherwise, term " installation ", " connected ", " connection ", " Gu
It is fixed " etc. terms shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integral；Can be
Mechanical connection can also be electrical connection；It can be directly connected, can also can be indirectly connected through an intermediary two
The interaction relationship of connection or two elements inside element.It for the ordinary skill in the art, can basis
Concrete condition understands the concrete meaning of above-mentioned term in the present invention.
In the present invention unless specifically defined or limited otherwise, fisrt feature is on or below second feature
It may include that the first and second features are in direct contact, can also not be to be in direct contact but pass through it including the first and second features
Between other characterisation contact.Moreover, fisrt feature is on second feature, top and above include fisrt feature the
Right over two features and oblique upper, or be merely representative of fisrt feature level height and be higher than second feature.Fisrt feature is in the second spy
Under sign, lower section and fisrt feature included below are immediately below second feature and obliquely downward, or are merely representative of fisrt feature level
Height is less than second feature.
Embodiment：
Present embodiments provide a kind of reaction system comprising multifunctional magnetic-force stirs hydrothermal synthesis device 1, mainly profit
With strong acid in tank body or highly basic and high temperature high pressure enclosed environment achievees the purpose that rapid-digestion indissoluble substance.
It please referring to Fig.1 to Fig. 7, this multifunctional magnetic-force stirring hydrothermal synthesis device 1 is integral into cylindric, with shell,
Enclosure interior is provided with magnetic stirring apparatus 2, heater box 3 and multiple reaction kettles 4；Wherein, heater box 3 is mounted on magnetic stirring apparatus
On 2, multiple reaction kettles 4 are mounted in heater box 3 so that it can fully be heated, internal solution can realize fully and
Equably mix.
It should be noted that insulation shell sets within it reaction unit and transmission device, entire dress can either be protected
The safety set, and play a part of heat preservation.The design size of insulation shell is 1000 × 800 × 800mm.In addition, its babinet branch
Frame length (i.e. height of the babinet apart from ground) is 400mm.
Further, heater box 3 is provided with supporting mechanism 5, supporting mechanism 5 include the first support plate 6, the first connecting pole 7,
First rotation seat 8, driver 9, the second support plate 10, the second connecting pole 11 and the second rotation seat 12；First rotation seat 8 can turn
It is mounted on the bottom of babinet dynamicly, the first support plate 6 is connect by the first connecting pole 7 with the first rotation seat 8, and driver 9 is installed
In box house, the rotation of the first rotation seat 8 is driven by driver 9；Second rotation seat 12 is installed in rotation on the bottom of babinet
Portion, the second support plate 10 are connect by the second connecting pole 11 with the second rotation seat 12, and the second support plate 10 is nibbled with the first support plate 6
It closes；Multiple first mounting holes 13 and multiple second mounting holes 14 are offered in first support plate 6, the second support plate 10 respectively, it is more
A reaction kettle 4 is separately positioned on multiple first mounting holes 13, on multiple second mounting holes 14.
It should be noted that in the present embodiment, multiple first mounting holes 13 are circumferential and are opened in first evenly and at intervals
In support plate 6, multiple second mounting holes 14 are circumferential and are opened in evenly and at intervals in the second support plate 10.
It should be noted that multiple first sawtooth 25 are provided on the outside of the first support plate 6, outside the second support plate 10
Multiple second sawtooth 26 are provided on side, the first support plate 6 is nibbled by the first sawtooth 25, the second sawtooth 26 and the second support plate 10
It closes.
When starting driving 6 opposite case of the first support plate rotation of driver 9, the meshing relation band of the two can be passed through
Dynamic second support plate 10 rotation；Meanwhile heater is mounted on two of heater box 3 relatively on side wall, it can be from each angle
Degree is carried out while being heated to multiple reaction kettles 4 so that and the characteristics of homogeneity is presented in the heating degree of reaction kettle 4, so that its
Internal solution can be mixed more uniformly.
It should be noted that the heater can control temperature, reaction kettle 4 can be heated to 250 DEG C.
Further, the bottom of babinet offers first positioning hole 15, has on the inner wall of first positioning hole 15 first recessed
Slot 16, the first rotation seat 8 are in the form of a column structure, and the first rotation seat 8 is equipped with the first groove 16, and the first rotation seat 8 can be
Rotation in first groove 16.
Further, the bottom of babinet offers second location hole 17, has on the inner wall of second location hole 17 second recessed
Slot 18, the second rotation seat 12 are in the form of a column structure, and the second rotation seat 12 is equipped with the second groove 18, and the second rotation seat 12 can
The rotation in the second groove 18.
It should be noted that in the present embodiment, heater is set as loop configuration and the side wall mounted on heater box 3
On so that heater can heat reaction kettle 4 from the side of reaction kettle 4, so that mixed liquor in reaction kettle 4 is heated, plays
The effect for accelerating reaction, reaches the suitable temperature of experiment；In other examples, other shape knots be may be set to be
Structure.
Further, reaction kettle 4 includes autoclave body 19 and lid 20, and there is autoclave body 19 columned inner cavity, lid 20 to cover
On autoclave body 19, agitating shaft is connected on lid 20, agitating shaft stretches into autoclave body 19, and agitating shaft deviates the axis of inner cavity.By reaction kettle 4
It is set as, with lid 20 and autoclave body 19, mixed liquor being enable to be added in reaction kettle 4.
It should be noted that relatively independent between each reaction kettle 4, wherein the maximum value of 19 pressure resistance of autoclave body is not less than
3MPa, operating temperature is at 220 DEG C.By using reaction kettle 4 so that reaction carries out under pressure, and gives certain
Volume and heat-retaining condition, to reach the synthesis condition of synthetic reaction.The reaction kettle 4 installed and used every time can be according to specific reality
Situation decision is tested, can be lab scale rank or pilot scale rank.
Further, two handles of the setting at multiple pressure reducing valves and interval are provided with to the outside spacers of lid 20,
Two handles are oppositely arranged.Two handles, which are oppositely arranged, enables lid 20 easily to hold, and conveniently removes and installs；Pass through
Pressure reducing valve can reduce the pressure in reaction kettle 4, play safety guarantee.
Further, pressure is provided on lid 20, meter pressure table can reflect the pressure in reaction kettle 4, facilitate sight
It surveys.Pressure gauge connects magnetic stirring apparatus 2, reponse system can be arranged, by pressure feedback to magnetic stirring apparatus 2.
It should be noted that the operating process of the device is：Under the effect of magnetic stirring apparatus 2, by barium hydroxide, two
Titanium oxide, deionized water, absolute ethyl alcohol are placed in reaction vessel, are uniformly mixed；Or under the effect of magnetic stirring apparatus 2,
Barium hydroxide is dissolved in deionized water, titanium dioxide is equably dissolved in absolute ethyl alcohol, and mutual with the solution of gained
Mixing；KOH is added to the solution of gained, is uniformly mixed；The solution of gained is moved into 4 polytetrafluoroethylene (PTFE) of hydrothermal reaction kettle
In liner, KOH is added under the action of stirring；The reaction system of gained is washed through deionized water and absolute ethyl alcohol, in baking oven
Middle drying, obtains barium carbonate powder.
In conclusion the utility model stirs hydrothermal synthesis device 1 by the multifunctional magnetic-force that above-mentioned design obtains, have
Magnetic stirring apparatus 2, heater box 3 and multiple reaction kettles 4；Wherein, it due to being provided with supporting mechanism 5 in the babinet of heater box 3, props up
Support mechanism 5 has the first support plate 6 and the second support plate 10, is offered respectively in the first support plate 6 and the second support plate 10
Therefore multiple first mounting holes 13 and multiple second mounting holes 14 can place multiple reaction kettles 4 simultaneously thereon, add when starting
When hot device and magnetic stirring apparatus 2, can mixing be stirred to the solution in multiple reaction kettles 4 simultaneously so that therein molten
Liquid mixing is more uniformly distributed fully, and improves the mixing efficiency of solution.Simultaneously as the first support plate 6 and the second support plate
The first sawtooth 25 and the second sawtooth 26 are respectively arranged on 10, therefore, the two can pass through the first sawtooth 25 and the second sawtooth 26
Engagement can be driven when starting driving 6 opposite case of the first support plate rotation of driver 9 by the meshing relation of the two
Second support plate 10 rotates, and heater can carry out while heating to multiple reaction kettles 4 from all angles as a result, so that reaction
The characteristics of homogeneity is presented in the heating degree of kettle 4, so that its internal solution can be mixed more uniformly.By
This can be such that mixed liquor in reaction kettle 4 is sufficiently mixed, obtain it is found that by this multifunctional magnetic-force stirring hydrothermal synthesis device 1
The mixed liquor being more uniformly distributed.The reaction system that the utility model is obtained by above-mentioned design, the reaction system is due to above-mentioned
Multifunctional magnetic-force stirring hydrothermal synthesis device 1, therefore, mixed liquor in reaction kettle 4 can be made to be sufficiently mixed, obtained more equal
Even mixed liquor.
Above description is merely a prefered embodiment of the utility model, is not intended to limit the utility model, for
For those skilled in the art, various modifications and changes may be made to the present invention.All spirit and original in the utility model
Within then, any modification, equivalent replacement, improvement and so on should be included within the scope of protection of this utility model.
Claims (10)
1. a kind of multifunctional magnetic-force stirs hydrothermal synthesis device, which is characterized in that the multifunctional magnetic-force stirs hydrothermal synthesis device packet
Include magnetic stirring apparatus, heater box and multiple reaction kettles；
The heater box is mounted on the magnetic stirring apparatus；
The heater box has columned babinet, and supporting mechanism is provided in the babinet, and the supporting mechanism includes first
Support plate, the first connecting pole, the first rotation seat, driver, the second support plate, the second connecting pole and the second rotation seat；It is described
First rotation seat is installed in rotation on the bottom of the babinet, first support plate by first connecting pole with it is described
First rotation seat connects, and the driver is mounted on the box house, and first rotation seat is driven by the driver
Rotation；Second rotation seat is installed in rotation on the bottom of the babinet, and second support plate connects by described second
It connects column to connect with second rotation seat, second support plate is engaged with first support plate；
Multiple first mounting holes and multiple second mounting holes are offered respectively in first support plate, second support plate,
Multiple reaction kettles are separately positioned on multiple first mounting holes, on multiple second mounting holes.
2. multifunctional magnetic-force according to claim 1 stirs hydrothermal synthesis device, which is characterized in that multiple first installations
Hole is circumferential and is opened in evenly and at intervals in first support plate.
3. multifunctional magnetic-force according to claim 2 stirs hydrothermal synthesis device, which is characterized in that multiple second installations
Hole is circumferential and is opened in evenly and at intervals in second support plate.
4. multifunctional magnetic-force according to claim 1 stirs hydrothermal synthesis device, which is characterized in that open the bottom of the babinet
Equipped with first positioning hole, there is the first groove, first rotation seat to be in the form of a column structure, institute on the inner wall of the first positioning hole
It states the first rotation seat to be equipped with first groove, first rotation seat can rotate in first groove.
5. multifunctional magnetic-force according to claim 4 stirs hydrothermal synthesis device, which is characterized in that open the bottom of the babinet
Equipped with second location hole, there is the second groove, second rotation seat to be in the form of a column structure, institute on the inner wall of the second location hole
It states the second rotation seat to be equipped with second groove, second rotation seat can rotate in second groove.
6. multifunctional magnetic-force according to claim 1 stirs hydrothermal synthesis device, which is characterized in that the reaction kettle includes kettle
Body and lid, the autoclave body have columned inner cavity, and the cover cap is on the autoclave body.
7. multifunctional magnetic-force according to claim 6 stirs hydrothermal synthesis device, which is characterized in that between the outside of the lid
Two handles of the setting at multiple pressure reducing valves and interval are provided with every ground, described two handles are oppositely arranged.
8. multifunctional magnetic-force according to claim 7 stirs hydrothermal synthesis device, which is characterized in that be provided on the lid
Pressure gauge.
9. multifunctional magnetic-force according to claim 8 stirs hydrothermal synthesis device, which is characterized in that first support plate
It is provided with multiple first sawtooth on outside, is provided with multiple second sawtooth on the outside of second support plate, described first
Support plate is engaged by first sawtooth, second sawtooth with second support plate.
10. a kind of reaction system, which is characterized in that the reaction system includes that claim 1-9 any one of them is multi-functional
Magnetic agitation hydrothermal synthesis device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721874388.3U CN207805614U (en) | 2017-12-27 | 2017-12-27 | A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721874388.3U CN207805614U (en) | 2017-12-27 | 2017-12-27 | A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207805614U true CN207805614U (en) | 2018-09-04 |
Family
ID=63327499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721874388.3U Expired - Fee Related CN207805614U (en) | 2017-12-27 | 2017-12-27 | A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207805614U (en) |
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2017
- 2017-12-27 CN CN201721874388.3U patent/CN207805614U/en not_active Expired - Fee Related
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