CN207601184U - A kind of measurement device of glassy solids high-temperature conductivity - Google Patents

A kind of measurement device of glassy solids high-temperature conductivity Download PDF

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Publication number
CN207601184U
CN207601184U CN201721826532.6U CN201721826532U CN207601184U CN 207601184 U CN207601184 U CN 207601184U CN 201721826532 U CN201721826532 U CN 201721826532U CN 207601184 U CN207601184 U CN 207601184U
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China
Prior art keywords
glass
muffle furnace
temperature
direct current
determined
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CN201721826532.6U
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Inventor
仲召进
马立云
曹欣
倪嘉
石丽芬
崔介东
王萍萍
单传丽
韩娜
操芳芳
高强
赵凤阳
王巍巍
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CNBM Bengbu Design and Research Institute for Glass Industry Co Ltd
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CNBM Bengbu Design and Research Institute for Glass Industry Co Ltd
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Abstract

The utility model discloses a kind of measurement device of glassy solids high-temperature conductivity, including Muffle furnace, direct current galvanometer and DC voltage generator, corundum porcelain boat is equipped in muffle furnace hearth, corundum porcelain boat both ends are respectively equipped with platinum piece, glass to be determined is placed in corundum porcelain boat, glass is in cuboid, and glass both ends are corresponding with platinum piece to be in contact;For Muffle furnace for heating and making glass to maintain solid state to glass to be determined, DC voltage generator, direct current galvanometer, platinum piece are in series with glass to be determined by platinum wire forms circuit;DC voltage generator output voltage, direct current galvanometer detect to flow through the electric current of glass, then can calculate the resistance value of glass at such a temperature, the conductivity of glass at such a temperature can be calculated further according to the size of glass;Change the furnace temperature of Muffle furnace, you can measure at various temperatures, conductivity of the glass in solid state;It is simple in structure, it is easy to use.

Description

A kind of measurement device of glassy solids high-temperature conductivity
Technical field
The utility model is related to glass detection technique field, the measure dress of specifically a kind of glassy solids high-temperature conductivity It puts.
Background technology
Semiconducting glass is the core for manufacturing microchannel plate electron multiplier, conductive plates, printing fiber and electro-optical device The relationship of material, glass conductivity and temperature is the key that research semiconducting glass, so the conductance of glassy solids at high temperature Rate measure is just particularly important.
The environment of raising in terms of with the rapid development of glass smelting technology and to(for) glass melter exhaust emission standard, Electric boosting is widely adopted in glass melter, everybody accreditation has been obtained with its unique advantage:Improve melting rate and Refining quality reduces the formation of some calculus defects, extends furnace service life, reduces environmental pollution.
It is analyzed from the meaning of glass high-temperature conductivity test, under different temperatures, analyzes the conductivity parameters variation of glass Good reference role can be provided for the adjustment of material side;In electric boosting kiln, the high-temperature conductivity variation of glass is direct relation Whether melten glass liquid can effectively facilitate glass melting, reduce calculus, and an ancient unit of weight and clarification, the key for reducing glass defect is promoted to refer to Mark;The high-temperature conductivity for understanding associated glass is the premise for designing electric boosting kiln.
With the progress of glass cause, some performances, formula and simple glass have the need of the special glass of greatest differences Ask increasing, such as:TFT-LCD glass substrates, but the high-temperature conductivity of this P series glass does not have related data also, institute Positive impetus will be played for the further research and production of glass material with the measurement device of glass high-temperature conductivity.
Utility model content
The purpose of this utility model is to provide a kind of measurement devices of glassy solids high-temperature conductivity, which can be right Glass in the solid state each temperature when conductivity be measured, it is simple in structure, easy to use.
Technical solution is used by the utility model solves its technical problem:
A kind of measurement device of glassy solids high-temperature conductivity occurs including Muffle furnace, direct current galvanometer and DC voltage Device, muffle furnace hearth is interior to be equipped with corundum porcelain boat, and corundum porcelain boat both ends are respectively equipped with platinum piece, are placed in corundum porcelain boat to be determined Glass, glass are in cuboid, and glass both ends are corresponding with platinum piece to be in contact, and the height of glass is less than the height of platinum piece;Muffle Stove is used to heat glass to be determined and glass is made to maintain solid state, DC voltage generator, direct current galvanometer, platinum piece It is in series with glass to be determined by platinum wire and forms circuit.
The beneficial effects of the utility model are that the glass in corundum porcelain boat is heated by Muffle furnace, at the same time, DC voltage generator output voltage, direct current galvanometer are detected to flow through the electric current of glass, then can be calculated in the temperature The resistance value of lower glass can calculate the conductivity of glass at such a temperature further according to the size of glass;Change Muffle furnace Furnace temperature, you can measure at various temperatures, conductivity of the glass in solid state;It is simple in structure, it is easy to use.
Description of the drawings
The utility model is further illustrated with reference to the accompanying drawings and examples:
Fig. 1 is the structure diagram of the utility model;
Fig. 2 is the close-up schematic view of Fig. 1.
Specific embodiment
With reference to shown in Fig. 1 and Fig. 2, the utility model provides a kind of measurement device of glassy solids high-temperature conductivity, including Muffle furnace 1, direct current galvanometer 2 and DC voltage generator 3,1 burner hearth of Muffle furnace is interior to be equipped with corundum porcelain boat 4,4 both ends of corundum porcelain boat It being respectively equipped with platinum piece 5, places glass 6 to be determined in corundum porcelain boat 4, glass 6 is in cuboid, and 6 both ends of glass coat 0.5~ The conducting resinl of 1.0mm is corresponding with platinum piece 5 to be in contact, and the height of glass is less than the height of platinum piece;DC voltage generator 3rd, direct current galvanometer 2, platinum piece 5 are in series with glass 6 to be determined by platinum wire 7 forms circuit.
During measure, control Muffle furnace 1 heats up, and the temperature of Muffle furnace 1 is always in glass melting point hereinafter, measuring glass It is solid state always in journey.The present embodiment makes Muffle furnace 1 be warming up to 600 DEG C with the heating rate of 3 DEG C/min, then adjusts straight 3 output voltage U of voltage generator is flowed, direct current galvanometer 2 is detected to flow through the corresponding electric current I of glass, be calculated at such a temperature Resistance R=U/I of glass can acquire one group of data every 5s, read 2~4 groups of voltages and corresponding electric current at this temperature, so The resistance of calculating is averaged afterwards.The resistance value of platinum piece and platinum wire is far smaller than the electricity of glassy solids at this temperature Resistance value can be neglected.
In this way, you can obtain the conductivity of glass at various temperatures.
The above descriptions are merely preferred embodiments of the present invention, and not the utility model is made in any form Limitation;Any those skilled in the art, it is all available in the case where not departing from technical solutions of the utility model ambit The methods and technical content of the disclosure above is made technical solutions of the utility model many possible changes and modifications or is revised as The equivalent embodiment of equivalent variations.Therefore, every content without departing from technical solutions of the utility model, according to the utility model Technical spirit any simple modification made to the above embodiment, equivalent replacement, equivalence changes and modification, still fall within this practicality In the range of the protection of new technique scheme.

Claims (1)

1. a kind of measurement device of glassy solids high-temperature conductivity, which is characterized in that including Muffle furnace, direct current galvanometer and direct current Voltage generator, muffle furnace hearth is interior to be equipped with corundum porcelain boat, and corundum porcelain boat both ends are respectively equipped with platinum piece, are placed in corundum porcelain boat Glass to be determined, glass are in cuboid, and glass both ends are corresponding with platinum piece to be in contact, and the height of glass is less than the height of platinum piece Degree;Muffle furnace for heating and making glass to maintain solid state to glass to be determined, flow by DC voltage generator, direct current inspection Meter, platinum piece are in series with glass to be determined by platinum wire forms circuit.
CN201721826532.6U 2017-12-25 2017-12-25 A kind of measurement device of glassy solids high-temperature conductivity Active CN207601184U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721826532.6U CN207601184U (en) 2017-12-25 2017-12-25 A kind of measurement device of glassy solids high-temperature conductivity

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721826532.6U CN207601184U (en) 2017-12-25 2017-12-25 A kind of measurement device of glassy solids high-temperature conductivity

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Publication Number Publication Date
CN207601184U true CN207601184U (en) 2018-07-10

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114965576A (en) * 2021-12-02 2022-08-30 胡波 Method for detecting whether glass product contains silver

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114965576A (en) * 2021-12-02 2022-08-30 胡波 Method for detecting whether glass product contains silver

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