CN207408264U - Quick analysis measurement device containing solid heavy oil - Google Patents
Quick analysis measurement device containing solid heavy oil Download PDFInfo
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- CN207408264U CN207408264U CN201721572935.2U CN201721572935U CN207408264U CN 207408264 U CN207408264 U CN 207408264U CN 201721572935 U CN201721572935 U CN 201721572935U CN 207408264 U CN207408264 U CN 207408264U
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- containing solid
- heavy oil
- extractor
- solid heavy
- extractor body
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Abstract
Quick analysis measurement device of the utility model containing solid heavy oil is related to using the production technology and research field containing solid heavy oil as raw material, more particularly to the measurement device of a kind of solid content containing solid heavy oil, asphalitine and oil content, the solid content containing solid heavy oil, asphalitine and oil content can be measured；Including constant temperature heating device and extraction device, the constant temperature heating device includes heating mantle and the heated at constant temperature controlling and regulating system being connected in heating mantle；The utility model realizes the solid content containing solid heavy oil, asphalitine, the measurement result of oily three kinds of analysis projects, by adding stainless billet, the effect washed away and impregnated of solvent is added, and then increases effective contact area, can quickly and easily separate solid, asphalitine and oil.Three parallel samples can be once done simultaneously, more difficult due to containing solid heavy oil homogenize process, the utility model solution samples the deviation for doing belt transect containing solid mink cell focus repeatedly, and data result accuracy is high.
Description
Technical field
The utility model is related to using the production technology and research field containing solid heavy oil as raw material, and in particular to one kind is containing solid weight
The solid content of oil, the measurement device of asphalitine and oil content, can measure the solid content containing solid heavy oil, asphalitine and oil content.
Background technology
Include containing solid heavy oil：Residue, catalytic slurry that coal tar, kerosene refine altogether etc..Existing soxhlet type glass sheathing
Extraction equipment weighs dewatered be placed on containing solid heavy oil in filtration paper cylinder, after the filtration paper cylinder of carry sample entered into soxhlet type glass
Device adds in solvent simultaneously in flask and is extracted.After the solvent in extractor reaches certain altitude, and carry oil or drip
Blue or green matter is returned in flask, and due to the solvent liquid vaporization cycle of flask, oil or asphalitine are reciprocally brought back in flask, are passed through
Liquid in regular hour siphon pipe becomes clear, colorless, i.e., extracting separation overall process terminates.To containing solid heavy oil by adding not
Solid content, asphalitine and oil are may separate out with reagent, finally calculates the solid content containing solid heavy oil, asphalitine and oil content.
The device of existing soxhlet type glass sheathing extraction equipment and patent CN201620248304.4 have the following problems：
1. the solvent and the effective contact area of sample of existing apparatus and patent CN201620248304.4 devices are few, it is only suitable for
The sample separation of low-solid content；And the sample of high solids content cannot be completely dissolved in a short time, ultimately result in measure analysis knot
Fruit deviation is big.
2. having the thermometer with rubber stopper at the top of the device of patent CN201620248304.4, increase is thus needed to extract
When steam pressure, otherwise extractive process be difficult to continue, be as a result easy to make steam to break through rubber stopper and spray condenser.
3. when if existing soxhlet type glass sheathing extraction equipment does solid content high heavy oil sample, filtration paper cylinder is making sample
Process cracky.
The content of the invention
To solve the above-mentioned problems, the utility model, which provides one kind, sample to be made fully to dissolve, and it is completely molten to reduce sample
The sample time is solved and done, there is stable, the accurate and quick quick analysis measurement device containing solid heavy oil.
Quick analysis measurement device of the utility model containing solid heavy oil, it is described including constant temperature heating device and extraction device
Constant temperature heating device includes heating mantle and the heated at constant temperature controlling and regulating system being connected in heating mantle；
The extraction device includes the condenser, extractor and the flask that are sequentially connected, and the flask is located in heating mantle, and
Heating mantle is stretched out in openend；A siphon pipe is provided on the extractor, valve is provided on the siphon pipe；
The extractor includes extractor body and steam communicating pipe, a stainless steel pad being provided in the extractor body
Plate is provided with several through holes on the stainless billet, a filtration paper cylinder is additionally provided on the stainless billet；
The steam communicating pipe, both ends were connected with extractor body, and one end is located at the lower part of stainless billet, another
End is positioned at the top of filtration paper cylinder；
The extractor body upper part is provided with a thermometer, and one end of thermometer is stretched into extractor body.
Preferably, height of the stainless billet on extractor exports the height phase on extractor body with siphon pipe
Together.
Or preferably, condenser has lotus nozzle formula distributor, the lotus spray with the end set that extractor body is connected
Several discharge holes, number and the aperture and the number of through hole on stainless billet of the discharge hole are provided on hair style distributor
It is identical with aperture.
Preferably, thermometer stretches into one end of extractor body and is located at steam communicating pipe and extractor body junction, and
The end steam communicating pipe is located at filtration paper cylinder top.
Preferably, cooling water is connected in condenser, the cooling water temperature is 15 DEG C -20 DEG C.
The utility model realizes the solid content containing solid heavy oil, asphalitine, the measurement result of oily three kinds of analysis projects, passes through
Stainless billet is added, adds the effect washed away and impregnated of solvent, and then increases effective contact area, it can be square rapidly
Just solid, asphalitine and oil are separated.Three parallel samples can be once done simultaneously, it is more difficult due to containing solid heavy oil homogenize process,
The utility model solution samples the deviation for doing belt transect containing solid mink cell focus repeatedly, and data result accuracy is high.
The end set that condenser is connected with extractor has lotus nozzle formula distributor, from lotus nozzle formula when steam condensation is fallen
Distributor equably instills filtration paper cylinder, thus controls the frequency to flow back in extractive process.
The present apparatus greatly reduces the chance that human interference factor and organic solvent are contacted with people, ensures the standard of measurement result
True property and raising security.
Description of the drawings
Fig. 1 is the utility model structure diagram.
Fig. 2 is lotus nozzle formula distributor schematic diagram in Fig. 1（It sees from bottom to top）.
Fig. 3 is stainless billet schematic diagram in Fig. 1（It is seen from above）.
Reference numeral：1- condensers, 2- thermometers, 3- valves, 4- heated at constant temperature controlling and regulating systems, 5- heating mantles, 6-
Stainless billet, 7- filtration paper cylinders, 8- lotus nozzle formula distributors, 9- steam communicating pipes, 10- extractor bodies.
Specific embodiment
Quick analysis measurement device of the utility model containing solid heavy oil, it is described including constant temperature heating device and extraction device
Constant temperature heating device includes heating mantle 5 and the heated at constant temperature controlling and regulating system 4 being connected in heating mantle 5；
The extraction device includes the condenser 1, extractor and the flask that are sequentially connected, and the flask is located in heating mantle 5,
And heating mantle 5 is stretched out in openend；A siphon pipe is provided on the extractor, valve 3 is provided on the siphon pipe；
The extractor includes extractor body 10 and steam communicating pipe 9, one being provided with not in the extractor body 10
Become rusty billet 6, is provided with several through holes on the stainless billet 6, a filtration paper cylinder is additionally provided on the stainless billet 6
7, by adding stainless billet 6, the effect washed away and impregnated of solvent is added, and then effective contact area is increased,
Solid, asphalitine and oil can quickly and easily be separated；9 both ends of steam communicating pipe are connected with extractor body 10, and one
End is located at the top of filtration paper cylinder 7 positioned at the lower part of stainless billet 6, the other end；10 top of extractor body is provided with one
Thermometer 2, and one end of thermometer 2 is stretched into extractor.Height of the stainless billet 6 on extractor is exported with siphon pipe
Height on extractor body 10 is identical.
The end set that condenser 1 is connected with extractor has a lotus nozzle formula distributor 8, on the lotus nozzle formula distributor 8
Several discharge holes are provided with, the number of the discharge hole is identical with aperture with the number of through hole on stainless billet 6 with aperture,
When steam condensation is fallen filtration paper cylinder 7 is equably instilled from lotus nozzle formula distributor 8.Thermometer 2 stretches into the one of extractor body 10
End is located at steam communicating pipe 9 and extractor junction, and the end steam communicating pipe 9 is located at 7 top of filtration paper cylinder, to detect solvent
Steam temperature.Cooling water is connected in condenser 1, the cooling water temperature is 15 DEG C -20 DEG C.
Stainless billet 6 is placed in 7 bottom of filtration paper cylinder, highly concordant with siphon pipe top edge, so increases hot solvent and sample
The reflux frequency of effective contact area and control extracting of the product when washing away and impregnating, can quickly and easily isolate containing solid weight
Solid, asphalitine and oil in oil.
Specific implementation step：
Flask is placed in heating mantle 5 before experiment, extractor and condenser 1 are connected in series, and extractor steam siphunculus goes out
Mouth adjacent upper part is inserted into a thermometer 2, inserts the stainless billet 6 highly consistent with siphon pipe in extracting filter device.
After the recirculated cooling water of proper temperature is accessed this extraction device.It will weigh and be put into filter paper containing solid heavy oil sample after a certain amount of dehydration
7 bottoms of cylinder and a certain amount of normal heptane solvent are placed on together in extracting filter device, open 4 He of heated at constant temperature controlling and regulating system
Adjust the valve 3 on siphon pipe, increase in a short time effective contact area when washing away and impregnating of hot solvent and sample and
The reflux frequency of extracting is controlled, until the liquid clear, colorless of siphon pipe again.Directly change into a certain amount of toluene solvant after
Continuous extracting filtering, treats solution clear, colorless in siphon pipe, obtains solid and the solution with toluene.To carrying consolidating for filtration paper cylinder 7
Soma is dry, cooling, and the quality that filtration paper cylinder 7 is removed after constant weight obtains the solid content of mink cell focus；The solution vacuum for carrying toluene is done
It is dry, the asphalt content containing solid heavy oil is obtained, the oil containing normal heptane solvent is rotated, removal normal heptane solvent obtains
Oil quality is converted into oil content.
Finally it should be noted that above example is only to illustrate the technical solution of the utility model rather than to this reality
With the limitation of novel protected scope, although being explained in detail with reference to preferred embodiment to the utility model, this field it is general
Lead to it will be appreciated by the skilled person that can be modified or replaced equivalently to the technical solution of the utility model, without departing from this
The implementation of utility model technical solution and scope.
Claims (5)
1. a kind of quick analysis measurement device containing solid heavy oil, including constant temperature heating device and extraction device, the heated at constant temperature
Device includes heating mantle（5）Be connected to heating mantle（5）On heated at constant temperature controlling and regulating system（4）；
The extraction device includes the condenser being sequentially connected（1）, extractor and flask, the flask be located at heating mantle（5）It is interior,
And heating mantle is stretched out in openend（5）；A siphon pipe is provided on the extractor, valve is provided on the siphon pipe（3）；
It is characterized in that, the extractor includes extractor body（10）With steam communicating pipe（9）, the extractor body（10）
Inside it is provided with a stainless billet（6）, the stainless billet（6）On be provided with several through holes, the stainless billet（6）
On be additionally provided with a filtration paper cylinder（7）；
The steam communicating pipe（9）Both ends with extractor body（10）It is connected, and one end is located at stainless billet（6）Under
Portion, the other end are located at filtration paper cylinder（7）Top；
The extractor body（10）Top is provided with a thermometer（2）, and thermometer（2）One end stretch into extractor body
（10）In.
2. the quick analysis measurement device containing solid heavy oil as described in claim 1, which is characterized in that the stainless billet（6）
In extractor body（10）On height and siphon pipe export in extractor body（10）On height it is identical.
3. the quick analysis measurement device containing solid heavy oil as claimed in claim 1 or 2, which is characterized in that the condenser（1）With
Extractor body（10）Connected end set has lotus nozzle formula distributor（8）, the lotus nozzle formula distributor（8）On be provided with
Several discharge holes, number and the aperture and stainless billet of the discharge hole（6）The number of upper through hole is identical with aperture.
4. the quick analysis measurement device containing solid heavy oil as claimed in claim 3, which is characterized in that the thermometer（2）It stretches into
Extractor body（10）One end be located at steam communicating pipe（9）With extractor body（10）Junction, and the end steam communicating pipe
（9）Positioned at filtration paper cylinder（7）Top.
5. the quick analysis measurement device containing solid heavy oil as claimed in claim 4, which is characterized in that the condenser（1）It is interior logical
There is cooling water, the cooling water temperature is 15 DEG C -20 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721572935.2U CN207408264U (en) | 2017-11-22 | 2017-11-22 | Quick analysis measurement device containing solid heavy oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721572935.2U CN207408264U (en) | 2017-11-22 | 2017-11-22 | Quick analysis measurement device containing solid heavy oil |
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| Publication Number | Publication Date |
|---|---|
| CN207408264U true CN207408264U (en) | 2018-05-25 |
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ID=62316843
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| CN201721572935.2U Active CN207408264U (en) | 2017-11-22 | 2017-11-22 | Quick analysis measurement device containing solid heavy oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109932269A (en) * | 2019-03-16 | 2019-06-25 | 天能电池集团股份有限公司 | A kind of test method of lead powder oil content |
| CN114563486A (en) * | 2022-03-16 | 2022-05-31 | 珠海格力电工有限公司 | Solid content testing method for insulating paint |
-
2017
- 2017-11-22 CN CN201721572935.2U patent/CN207408264U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109932269A (en) * | 2019-03-16 | 2019-06-25 | 天能电池集团股份有限公司 | A kind of test method of lead powder oil content |
| CN114563486A (en) * | 2022-03-16 | 2022-05-31 | 珠海格力电工有限公司 | Solid content testing method for insulating paint |
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